Micropollutants pre-concentration using adsorption-desorption cycles: application to chlorinated paraffins and alkyl-phenol derivatives

2016 ◽  
Vol 92 (5) ◽  
pp. 1076-1084 ◽  
Author(s):  
Yolanda Patiño ◽  
Eva Díaz ◽  
Salvador Ordóñez

1971 ◽  
Vol 68 ◽  
pp. 29-33 ◽  
Author(s):  
Bernard Weber ◽  
Albert Cassuto


1983 ◽  
Vol 139 (4) ◽  
pp. 736
Author(s):  
V.N. Ageev ◽  
E.Ya. Zandberg ◽  
N.I. Ionov ◽  
A.Ya. Tontegode


2015 ◽  
Vol 14 (1) ◽  
pp. 66-72 ◽  
Author(s):  
Seo-Hyun Pak ◽  
◽  
Myung-Seop Shin ◽  
Hyun-Jung Kim ◽  
Yong-Woo Jeon


1960 ◽  
Vol XXXV (I) ◽  
pp. 34-48 ◽  
Author(s):  
Gerd Ittrich

ABSTRACT A series of organic solvents and phenol derivatives have been examined for the extraction of the pink Kober-colour complex. Optimal results could be achieved for fluorimetry by a solution of 2 % (w/v) p-nitrophenol and 1 % (v/v) ethanol in acetylenetetrabromide, when the green mercury line (546 mμ was used as primary light. The sensitivity, stability and specificity have been improved, compared with the previously described reaction. By changing the sequence of purification steps and by reducing the volume of the urine sample (5 ml) the method for the determination of total oestrogens has been simplified. Approximately 10 determinations can be done within 3–4 hours by one person. Recovery experiments and comparative determinations with a previously described method have been carried out. The excretion of total oestrogens in a complete menstrual cycle is determined with the described method.



2020 ◽  
Author(s):  
Baojian Xiong ◽  
Yue Li ◽  
Yin Wei ◽  
Søren Kramer ◽  
Zhong Lian

Cross-coupling between substrates that can be easily derived from phenols is highly attractive due to the abundance and low cost of phenols. Here, we report a dual nickel/palladium-catalyzed reductive cross-coupling between aryl tosylates and aryl triflates; both substrates can be accessed in just one step from readily available phenols. The reaction has a broad functional group tolerance and substrate scope (>60 examples). Furthermore, it displays low sensitivity to steric effects demonstrated by the synthesis of a 2,2’disubstituted biaryl and a fully substituted aryl product. The widespread presence of phenols in natural products and pharmaceuticals allow for straightforward late-stage functionalization, illustrated with examples such as Ezetimibe and tyrosine. NMR spectroscopy and DFT calculations indicate that the nickel catalyst is responsible for activating the aryl triflate, while the palladium catalyst preferentially reacts with the aryl tosylate.



2011 ◽  
Vol 26 (2) ◽  
pp. 149-154 ◽  
Author(s):  
Fei XIE ◽  
Yan Li WANG ◽  
Liang ZHAN ◽  
Ming GE ◽  
Xiao-Yi LIANG ◽  
...  


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