Chromatographic characterization of molecularly imprinted microspheres for the separation and determination of trimethoprim in aqueous buffers

2002 ◽  
Vol 372 (2) ◽  
pp. 391-396 ◽  
Author(s):  
Jia-Ping Lai ◽  
Xian-Feng Cao ◽  
Xiu-Ling Wang ◽  
Xi-Wen He
Keyword(s):  
Molecularly Imprinted ◽  
Chromatographic Characterization ◽  
Molecularly Imprinted Microspheres

Synthesis and characterization of molecularly imprinted polymers with modified rosin as a cross-linker and selective SPE-HPLC detection of basic orange II in foods

2014 ◽  
Vol 6 (16) ◽  
pp. 6397-6406 ◽  
Author(s):  
Xiaoyan Li ◽  
Mei Li ◽  
Junjie Li ◽  
Fuhou Lei ◽  
Xiaomeng Su ◽  
...  
Keyword(s):  
Molecularly Imprinted Polymers ◽  
Solid Phase ◽  
Selective Extraction ◽  
Synthesis And Characterization ◽  
Orange Ii ◽  
Molecularly Imprinted ◽  
Imprinted Polymers ◽  
Cross Linker

A novel sample clean-up technique, i.e., molecularly imprinted solid-phase extraction (MISPE) combined with HPLC, was developed and validated for the selective extraction and determination of basic orange II in foods.

Chiral Recognition of L-Carnitine Using Surface Molecularly Imprinted Microspheres via RAFT Polymerization

2014 ◽  
Vol 884-885 ◽  
pp. 33-36 ◽  
Author(s):  
Lin Tong Hou ◽  
Jiao Jiao Chen ◽  
Hong Jun Fu ◽  
Xin Lei Fu
Keyword(s):  
Experimental Data ◽  
Chiral Recognition ◽  
Chain Transfer ◽  
Raft Polymerization ◽  
Isothermal Adsorption ◽  
Molecularly Imprinted ◽  
Reversible Addition ◽  
Ft Ir ◽  
Molecularly Imprinted Microspheres

A molecularly imprinted microsphere (MIPs) was prepared successfullyviasurface-initiated reversible addition-fragmentation chain transfer (RAFT) polymerization. Characterization of the obtained MIPs was achieved by FT-IR and TGA. The isothermal adsorption and chiral separation experiments of MIPs on L-Carnitine were investigated. Compared with non-imprinted microsphere (NMIPs) adsorbent, MIPs showed faster adsorption rate and stronger adsorption capacity for L-Carnitine. Equilibrium experimental data of MIPs fitted the Langmuir isotherm better. Furthermore, the MIPs also exhibited enantioselectivity for L-Carnitine through the resolution experiment.

Separation and determination of astaxanthin from microalgal and yeast samples by molecularly imprinted microspheres

2004 ◽  
Vol 804 (1) ◽  
pp. 25-30 ◽  
Author(s):  
Jia-Ping Lai ◽  
Yue Jiang ◽  
Xi-Wen He ◽  
Jun-Chao Huang ◽  
Feng Chen
Keyword(s):  
Molecularly Imprinted ◽  
Molecularly Imprinted Microspheres

Inverse gas chromatographic characterization of Porapak Q as an extractant of pollutants from aqueous media

2009 ◽  
Vol 63 (3) ◽  
Author(s):  
Nagy Moustafa ◽  
Doaa El-Desouki
Keyword(s):  
Gas Chromatography ◽  
Chemical Structure ◽  
Inverse Gas Chromatography ◽  
Aqueous Media ◽  
Lewis Acidity ◽  
Porapak Q ◽  
Chromatographic Characterization ◽  
Surface Lewis Acidity

AbstractThe surface of Porapak Q was characterized by inverse gas chromatography (IGC) carried out by the determination of dispersive and specific adsorption components of Porapak Q surface, calculating γsd and -ΔH as parameters, respectively. An interpretation was given based on the chemical structure of Porapak Q. The obtained results were confirmed through the surface Lewis acidity and basicity constants, K a and K b, respectively, correlating well with the determined thermodynamic parameters.

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