scholarly journals Imaging Luminescence Thermometry to 750 °C for the Heat Treatment of Common Engineering Alloys and Comparison with Thermal Imaging

2022 ◽  
Vol 43 (3) ◽  
Author(s):  
Gavin Sutton ◽  
Sofia Korniliou ◽  
Aurik Andreu ◽  
David Wilson

AbstractAccurate temperature measurements are critical in manufacturing, affecting both product quality and energy consumption. At elevated temperatures, non-contact thermometers are often the only option. However, such instruments require prior knowledge of the surface emissivity, which is often unknown or difficult to determine, leading to large errors. Here we present a novel imaging luminescence thermometer based on the intensity ratio technique using magnesium fluorogermanate phosphor, with the potential to overcome this limitation. We describe measurements performed on a number of engineering alloys undergoing heat treatment at temperatures of up to 750 °C and compare these measurements against a traditional contact thermocouple and thermal imager system. Agreement between the luminescence and embedded thermocouple temperatures was found to be better than 45 °C at all temperatures. However, the thermal imager measurement on the bare metal samples, with the instrument emissivity set to 1.0, showed differences of up to 500 °C at 750 °C, a factor of 10 larger. In an effort to improve the thermal imager accuracy, its instrument emissivity was adjusted until its temperature agreed with that of the thermocouple. When measuring on the bare metal, the effective emissivity was strongly sample dependent, with mean values ranging from 0.205 to 0.784. Since the phosphor derived temperatures exhibited substantially smaller errors compared to the thermal imager, it is suggested that this method can be used to compliment the thermal imaging technique, by providing a robust mechanism for adjustment of the instrument emissivity until agreement between the thermal imager and phosphor thermometer is obtained.

2014 ◽  
Vol 511-512 ◽  
pp. 425-428
Author(s):  
Jie Jiang ◽  
Wen Da Zhu ◽  
Gong Sheng Yang ◽  
Jing Peng Yan ◽  
Nan Jin Gao ◽  
...  

Liquefied natural gas (LNG) is obtained by cooling the gas temperature to -162 degree. Problems with the steel cans, the insulation layer or the concrete tank of the LNG tank can lead to changes of the temperature, local temperature decreases, and the safety of the tank is threatening. Through the combination of many sets of infrared thermal imager to monitor the temperature of the LNG storage tank’s sidewall, analyze the heat imagine, establish the corresponding relationship between the locations on the sidewall of the LNG tank and on the heat imagine, determine the position of the temperature point on the tank wall. Infrared thermal imaging technique for the sidewall of LNG storage tank can find out the heat abnormal conditions and fixing the temperature drop area in time, and provide powerful guarantee for the safe storage of the liquefied natural gas.


2020 ◽  
Vol 12 (21) ◽  
pp. 3591
Author(s):  
Matheus Gabriel Acorsi ◽  
Leandro Maria Gimenez ◽  
Maurício Martello

The development of low-cost miniaturized thermal cameras has expanded the use of remotely sensed surface temperature and promoted advances in applications involving proximal and aerial data acquisition. However, deriving accurate temperature readings from these cameras is often challenging due to the sensitivity of the sensor, which changes according to the internal temperature. Moreover, the photogrammetry processing required to produce orthomosaics from aerial images can also be problematic and introduce errors to the temperature readings. In this study, we assessed the performance of the FLIR Lepton 3.5 camera in both proximal and aerial conditions based on precision and accuracy indices derived from reference temperature measurements. The aerial analysis was conducted using three flight altitudes replicated along the day, exploring the effect of the distance between the camera and the target, and the blending mode configuration used to create orthomosaics. During the tests, the camera was able to deliver results within the accuracy reported by the manufacturer when using factory calibration, with a root mean square error (RMSE) of 1.08 °C for proximal condition and ≤3.18 °C during aerial missions. Results among different flight altitudes revealed that the overall precision remained stable (R² = 0.94–0.96), contrasting with the accuracy results, decreasing towards higher flight altitudes due to atmospheric attenuation, which is not accounted by factory calibration (RMSE = 2.63–3.18 °C). The blending modes tested also influenced the final accuracy, with the best results obtained with the average (RMSE = 3.14 °C) and disabled mode (RMSE = 3.08 °C). Furthermore, empirical line calibration models using ground reference targets were tested, reducing the errors on temperature measurements by up to 1.83 °C, with a final accuracy better than 2 °C. Other important results include a simplified co-registering method developed to overcome alignment issues encountered during orthomosaic creation using non-geotagged thermal images, and a set of insights and recommendations to reduce errors when deriving temperature readings from aerial thermal imaging.


Author(s):  
M. Larsen ◽  
R.G. Rowe ◽  
D.W. Skelly

Microlaminate composites consisting of alternating layers of a high temperature intermetallic compound for elevated temperature strength and a ductile refractory metal for toughening may have uses in aircraft engine turbines. Microstructural stability at elevated temperatures is a crucial requirement for these composites. A microlaminate composite consisting of alternating layers of Cr2Nb and Nb(Cr) was produced by vapor phase deposition. The stability of the layers at elevated temperatures was investigated by cross-sectional TEM.The as-deposited composite consists of layers of a Nb(Cr) solid solution with a composition in atomic percent of 91% Nb and 9% Cr. It has a bcc structure with highly elongated grains. Alternating with this Nb(Cr) layer is the Cr2Nb layer. However, this layer has deposited as a fine grain Cr(Nb) solid solution with a metastable bcc structure and a lattice parameter about half way between that of pure Nb and pure Cr. The atomic composition of this layer is 60% Cr and 40% Nb. The interface between the layers in the as-deposited condition appears very flat (figure 1). After a two hour, 1200 °C heat treatment, the metastable Cr(Nb) layer transforms to the Cr2Nb phase with the C15 cubic structure. Grain coarsening occurs in the Nb(Cr) layer and the interface between the layers roughen. The roughening of the interface is a prelude to an instability of the interface at higher heat treatment temperatures with perturbations of the Cr2Nb grains penetrating into the Nb(Cr) layer.


2009 ◽  
Vol 5 (1) ◽  
pp. 31-35
Author(s):  
F.F. Sizov ◽  
◽  
V.V. Zabudsky ◽  
A.G. Golenkov ◽  
S.L. Kravchenko ◽  
...  

2019 ◽  
Vol 4 (1) ◽  
pp. 286-294
Author(s):  
László Tóth ◽  
Réka Fábián

The X153CrMoV12 ledeburitic chromium steel characteristically has high abrasive wear resistance, due to their high carbon and high chromium contents with a large volume of carbides in the microstructure. This steel quality has high compression strength, excellent deep hardenability and toughness properties, dimensional stability during heat treatment, high resistance to softening at elevated temperatures. The higher hardness of cryogenic treated samples in comparison with conventional quenched samples mean lower quantity of retained austenite as at samples quenched to room temperature and tempered in similar condition. In the microstructure of samples were observed that the primary carbide did not dissolve at 1070°C and their net structure have not been changed during to heat treatment. During to tempering at high temperature the primary carbides have become more and more rounded. After low tempering temperature in martensite were observed some small rounded carbides also, increasing the tempering temperature the quantity of finely dispersed carbides increased, which result higher hardness. The important issues in heat treatment of this steels are the reduction or elimination of retained austenite due to cryogenic treatment.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 539
Author(s):  
Gonçalo M. Gorito ◽  
Aida B. Moreira ◽  
Pedro Lacerda ◽  
Manuel F. Vieira ◽  
Laura M. M. Ribeiro

Cast Ni-Si-B alloys have the potential for high-temperature applications because of their high resistance to wear, impact, corrosion, and oxidation at elevated temperatures due to an appropriate balance of hard phases and austenite that ensures a good compromise between toughness and hardness. In this work, NiSi3B2 specimens, fabricated by the lost-wax casting process, were investigated. Given the complex multiphase cast microstructure, a differential scanning calorimeter (DSC-TGA) analysis was employed to characterize the reactions that occur during solidification and the resulting phases were characterized using scanning electron microscopy (SEM), with energy-dispersive microanalysis (EDS) and backscattered electron (BSE) image and X-ray diffraction (XRD). Due to the presence of hard phases, machining of the Ni-Si-B components can pose additional difficulties. Therefore, the conditions of the solution heat treatment, which might lead to the homogenization of the microstructure, consequently improving its machinability, were also investigated. The results of the heat-treated samples indicated that the dissolution of the eutectic constituent is accompanied by a significant decrease in the hardness (approximately 17%). It is important to emphasize that the solution heat treatments carried out reduced the hardness without affecting the percentage of borides, which will allow improving the machinability without adversely affecting the alloy performance in service.


2015 ◽  
Vol 651-653 ◽  
pp. 677-682 ◽  
Author(s):  
Anatoliy Popovich ◽  
Vadim Sufiiarov ◽  
Evgenii Borisov ◽  
Igor Polozov

The article presents results of a study of phase composition and microstructure of initial material and samples obtained by selective laser melting of titanium-based alloy, as well as samples after heat treatment. The effect of heat treatment on microstructure and mechanical properties of specimens was shown. It was studied mechanical behavior of manufactured specimens before and after heat treatment at room and elevated temperatures as well. The heat treatment allows obtaining sufficient mechanical properties of material at room and elevated temperatures such as increase in ductility of material. The fractography of samples showed that they feature ductile fracture with brittle elements.


2014 ◽  
Vol 937 ◽  
pp. 154-157 ◽  
Author(s):  
Rong Wang ◽  
Ya Juan Jin

Wetting and spreading ability of Ag-Cu-Zn filler and Ag-Cu-P filler on copper surface under heat treatment furnace was studied. The microstructures of brazed joints of Ag-Cu-Zn and Ag-Cu-P filler under the same parameter were also observed. The microstructure shows that the wetting ability of Ag-Cu-Zn filler on the copper surface is better than Ag-Cu-P and its structure is uniformed and regulated. It is founded that there were obvious dissolution and diffusion between base metal and filler for the copper/Ag-Cu-Zn/copper joint, there were white and black eutectic structure formed in the joint interface.


2014 ◽  
Vol 989-994 ◽  
pp. 212-215
Author(s):  
J. Liu ◽  
G. Zhu ◽  
W. Mao

The effect of volume fraction of ferrite on the mechanical properties including strength, plasticity and wok hardening was systematically investigated in X80 pipeline steel in order to improve the plasticity. The microstructures with different volume fraction of ferrite and bainite were obtained by heat-treatment processing and the mechanical properties were tested. The work hardening behavior was analyzed by C-J method. The results show that the small amount of ferrite could effectively improve the plasticity. The work hardening ability and the ratio of yield/tensile strength with two phases of ferrite/bainite would be obviously better than that with single phase of bainite. The improvement of plasticity could be attributed to the ferrite in which more plastic deformation was afforded.


2000 ◽  
Author(s):  
Li Shi ◽  
Sergei Plyasunov ◽  
Adrian Bachtold ◽  
Paul L. McEuen ◽  
Arunava Majumdar

Abstract This paper reports the use of scanning thermal microscopy (SThM) for studying heat dissipation and phonon transport in nanoelectronic circuits consisting of carbon nanotubes (CNs). Thermally designed and batch fabricated SThM probes were used to resolve the phonon temperature distribution in the CN circuits with a spatial resolution of 50 nm. Heat dissipation at poor metal-CN contacts could be readily found by the thermal imaging technique. Important questions regarding energy transport in nanoelectronic circuits, such as where is heat dissipated, whether the electrons and phonons are in equilibrium, how phonons are transported, and what are the effects of mechanical deformation on the transport and dissipation properties, are addressed in this work.


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