Development of Antimicrobial Gelatin-Based Edible Films by Incorporation of Trans-Anethole/β-Cyclodextrin Inclusion Complex

2017 ◽  
Vol 10 (10) ◽  
pp. 1844-1853 ◽  
Author(s):  
Youxin Ye ◽  
Mingjin Zhu ◽  
Keyan Miao ◽  
Xinying Li ◽  
Defu Li ◽  
...  
Keyword(s):  
Inclusion Complex ◽  
Edible Films ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex

Development and characterization of zein edible films incorporated with catechin/β-cyclodextrin inclusion complex nanoparticles

2021 ◽  
Vol 261 ◽  
pp. 117877
Author(s):  
Longwei Jiang ◽  
Fuguo Jia ◽  
Yanlong Han ◽  
Xiangyi Meng ◽  
Yawen Xiao ◽  
...  
Keyword(s):  
Inclusion Complex ◽  
Edible Films ◽  
Cyclodextrin Inclusion ◽  
Cyclodextrin Inclusion Complex

scholarly journals Comprehensive Characterisation of the Ketoprofen-β-Cyclodextrin Inclusion Complex Using X-ray Techniques and NMR Spectroscopy

Molecules ◽  
2021 ◽  
Vol 26 (13) ◽  
pp. 4089
Author(s):  
Katarzyna Betlejewska-Kielak ◽  
Elżbieta Bednarek ◽  
Armand Budzianowski ◽  
Katarzyna Michalska ◽  
Jan K. Maurin
Keyword(s):  
Nmr Spectroscopy ◽  
Inclusion Complex ◽  
Crystal And Molecular Structure ◽  
Binding Constants ◽  
Nmr Studies ◽  
X Ray ◽  
Cyclodextrin Inclusion ◽  
Powder Samples ◽  
Cyclodextrin Inclusion Complex ◽  
Co Precipitation

Racemic ketoprofen (KP) and β-cyclodextrin (β-CD) powder samples from co-precipitation (1), evaporation (2), and heating-under-reflux (3) were analysed using X-ray techniques and nuclear magnetic resonance (NMR) spectroscopy. On the basis of NMR studies carried out in an aqueous solution, it was found that in the samples obtained by methods 1 and 2, there were large excesses of β-CD in relation to KP, 10 and 75 times, respectively, while the sample obtained by method 3 contained equimolar amounts of β-CD and KP. NMR results indicated that KP/β-CD inclusion complexes were formed and the estimated binding constants were approximately 2400 M−1, showing that KP is quite strongly associated with β-CD. On the other hand, the X-ray single-crystal technique in the solid state revealed that the (S)-KP/β-CD inclusion complex with a stoichiometry of 2:2 was obtained as a result of heating-under-reflux, for which the crystal and molecular structure were examined. Among the methods used for the preparation of the KP/β-CD complex, only method 3 is suitable.

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