Synthesis and characterization of square-planar platinum(II) and palladium(II) complexes with pyridine-2,6-dicarboxylic acid (H2dipic). X-ray crystal structure of trans-Na2[Pt(dipic)2]·6H2O and K[Pt(dipic)I]·1/2H2O

1991 ◽  
Vol 185 (2) ◽  
pp. 201-210 ◽  
Author(s):  
Gavino Chessa ◽  
Giampaolo Marangoni ◽  
Bruno Pitteri ◽  
Valerio Bertolasi ◽  
Gastone Gilli ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Dicarboxylic Acid ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Square Planar

scholarly journals Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complexes with 2’-[1-(2-pyridinyl)- ethylidene]oxamohydrazide: The crystal structure of biss2'-[1-(2-pyridinyl)ethylidene]oxa

2004 ◽  
Vol 69 (8-9) ◽  
pp. 651-660 ◽  
Author(s):  
Katarina Andjelkovic ◽  
Gordana Jakovljevic ◽  
Mario Zlatovic ◽  
Zivoslav Tesic ◽  
Dusan Sladic ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Nmr Spectroscopy ◽  
13C Nmr ◽  
Neutral Type ◽  
13C Nmr Spectroscopy ◽  
Octahedral Geometry ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Square Planar

Complexes of Zn(II), Pd(II) and Pt(II) with 2?-[1-(2-pyridinyl)ethylidene ]oxamohydrazide (Hapsox) were synthesized and their structures were determined. All the complexes are of a neutral type with two apsox ligands coordinated to Zn(II) and one apsox ligand coordinated to Pd(II) or Pt(II). In each case, the polydentate was coordinated via pyridine and hydrazone nitrogens and ?-oxyazine oxygen, forming an octahedral geometry around Zn(II), and a square planar one around Pd(II) and Pt(II). The structure determination was performed by IR, 1H-NMR and 13C-NMR spectroscopy, and for the Zn(II) complex by X-ray structure analysis.

Darstellung und Charakterisierung von Rubidiumhydrogencyanamid/Synthesis and Characterization of Rubidium Hydrogen Cyanamide

1999 ◽  
Vol 54 (11) ◽  
pp. 1375-1378 ◽  
Author(s):  
Michael Becker ◽  
Martin Jansen
Keyword(s):  
Crystal Structure ◽  
Liquid Ammonia ◽  
Synthesis And Characterization ◽  
Hydrogen Cyanamide ◽  
X Ray ◽  
Bond Lengths

The synthesis of RbHCN2 was carried out by reaction of cyanamide with rubidium amide in liquid ammonia. The crystal structure has been determinedo by x-ray powder methods (orthorhombic, P21,21,21, a = 7.299(1), b = 9.435(1), c = 9.420(1) Å; Z = 8). The anion is slightly bent (174°) and exhibits two different bond lengths (C-N: 1.17, HN-C: 1.31 Å).

The synthesis and characterization of a cationic technetium(V) phenylimido complex. The X-ray crystal structure of [TcCl2(NPh)(PMe2Ph)3](BPh4)

1995 ◽  
Vol 230 (1-2) ◽  
pp. 205-208 ◽  
Author(s):  
Terrence Nicholson ◽  
Alan Davison ◽  
Jon A. Zubieta ◽  
Qin Chen ◽  
Alun G. Jones
Keyword(s):  
Crystal Structure ◽  
Synthesis And Characterization ◽  
X Ray
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