Voids in Quenched Nickel

1968 ◽  
Vol 26 ◽  
pp. 266-267
Author(s):  
J. J. Laidler
Keyword(s):  
Electron Beam ◽  
Ambient Temperature ◽  
Cooling Rate ◽  
Three Dimensional ◽  
Cooling Curve ◽  
Polycrystalline Nickel ◽  
Quenching Temperature ◽  
Long Tail ◽  
Diffusion Pump

The presence of three-dimensional voids in quenched metals has long been suspected, and voids have indeed been observed directly in a number of metals. These include aluminum, platinum, and copper, silver and gold. Attempts at the production of observable quenched-in defects in nickel have been generally unsuccessful, so the present work was initiated in order to establish the conditions under which such defects may be formed.Electron beam zone-melted polycrystalline nickel foils, 99.997% pure, were quenched from 1420°C in an evacuated chamber into a bath containing a silicone diffusion pump fluid . The pressure in the chamber at the quenching temperature was less than 10-5 Torr . With an oil quench such as this, the cooling rate is approximately 5,000°C/second above 400°C; below 400°C, the cooling curve has a long tail. Therefore, the quenched specimens are aged in place for several seconds at a temperature which continuously approaches the ambient temperature of the system.

Nanoscale Self-Assembly Using Ion and Electron Beam Techniques: A Rapid Review

MRS Advances ◽  
2020 ◽  
Vol 5 (64) ◽  
pp. 3507-3520
Author(s):  
Chunhui Dai ◽  
Kriti Agarwal ◽  
Jeong-Hyun Cho
Keyword(s):  
Electron Beam ◽  
Self Assembly ◽  
Ion Beam ◽  
Three Dimensional ◽  
The Self ◽  
Stress Generation ◽  
Rapid Review ◽  
High Yield ◽  
3D Nanostructures ◽  
Self Assembled

AbstractNanoscale self-assembly, as a technique to transform two-dimensional (2D) planar patterns into three-dimensional (3D) nanoscale architectures, has achieved tremendous success in the past decade. However, an assembly process at nanoscale is easily affected by small unavoidable variations in sample conditions and reaction environment, resulting in a low yield. Recently, in-situ monitored self-assembly based on ion and electron irradiation has stood out as a promising candidate to overcome this limitation. The usage of ion and electron beam allows stress generation and real-time observation simultaneously, which significantly enhances the controllability of self-assembly. This enables the realization of various complex 3D nanostructures with a high yield. The additional dimension of the self-assembled 3D nanostructures opens the possibility to explore novel properties that cannot be demonstrated in 2D planar patterns. Here, we present a rapid review on the recent achievements and challenges in nanoscale self-assembly using electron and ion beam techniques, followed by a discussion of the novel optical properties achieved in the self-assembled 3D nanostructures.

scholarly journals Comparison of Phase Characteristics and Residual Stresses in Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion (L-PBF) and Electron Beam Powder Bed Fusion (EB-PBF) Techniques

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 796
Author(s):  
Aya Takase ◽  
Takuya Ishimoto ◽  
Naotaka Morita ◽  
Naoko Ikeo ◽  
Takayoshi Nakano
Keyword(s):  
Electron Beam ◽  
Residual Stresses ◽  
Cooling Rate ◽  
Process Parameters ◽  
Phase Evolution ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Solidification Temperature ◽  
Powder Bed ◽  
Β Phase

Ti-6Al-4V alloy fabricated by laser powder bed fusion (L-PBF) and electron beam powder bed fusion (EB-PBF) techniques have been studied for applications ranging from medicine to aviation. The fabrication technique is often selected based on the part size and fabrication speed, while less attention is paid to the differences in the physicochemical properties. Especially, the relationship between the evolution of α, α’, and β phases in as-grown parts and the fabrication techniques is unclear. This work systematically and quantitatively investigates how L-PBF and EB-PBF and their process parameters affect the phase evolution of Ti-6Al-4V and residual stresses in the final parts. This is the first report demonstrating the correlations among measured parameters, indicating the lattice strain reduces, and c/a increases, shifting from an α’ to α+β or α structure as the crystallite size of the α or α’ phase increases. The experimental results combined with heat-transfer simulation indicate the cooling rate near the β transus temperature dictates the resulting phase characteristics, whereas the residual stress depends on the cooling rate immediately below the solidification temperature. This study provides new insights into the previously unknown differences in the α, α’, and β phase evolution between L-PBF and EB-PBF and their process parameters.

scholarly journals Online Measurement of Deposit Surface in Electron Beam Freeform Fabrication

Sensors ◽  
2019 ◽  
Vol 19 (18) ◽  
pp. 4001 ◽  
Author(s):  
Shuhe Chang ◽  
Haoyu Zhang ◽  
Haiying Xu ◽  
Xinghua Sang ◽  
Li Wang ◽  
...  
Keyword(s):  
Electron Beam ◽  
3D Reconstruction ◽  
Three Dimensional ◽  
Thermal Conditions ◽  
Online Measurement ◽  
Three Dimensional Reconstruction ◽  
Continuous Change ◽  
Position Information ◽  
Freeform Fabrication ◽  
Dimensional Reconstruction

In the process of electron beam freeform fabrication (EBF3), due to the continuous change of thermal conditions and variability in wire feeding in the deposition process, geometric deviations are generated in the deposition of each layer. In order to prevent the layer-by-layer accumulation of the deviation, it is necessary to perform online geometry measurement for each deposition layer, based on which the error compensation can be done for the previous deposition layer in the next deposition layer. However, the traditional three-dimensional reconstruction method that employs structured laser cannot meet the requirements of long-term stable operation in the manufacturing process of EBF3. Therefore, this paper proposes a method to measure the deposit surfaces based on the position information of electron beam speckle, in which an electron beam is used to bombard the surface of the deposit to generate the speckle. Based on the structured information of the electron beam in the vacuum chamber, the three-dimensional reconstruction of the surface of the deposited parts is realized without need of additional structured laser sensor. In order to improve the detection accuracy, the detection error is theoretically analyzed and compensated. The absolute error after compensation is smaller than 0.1 mm, and the precision can reach 0.1%, which satisfies the requirements of 3D reconstruction of the deposited parts. An online measurement system is built for the surface of deposited parts in the process of electron beam freeform fabrication, which realizes the online 3D reconstruction of the surface of the deposited layer. In addition, in order to improve the detection stability of the whole system, the image processing algorithm suitable for this scene is designed. The reliability and speed of the algorithm are improved by ROI extraction, threshold segmentation, and expansion corrosion. In addition, the speckle size information can also reflect the thermal conditions of the surface of the deposited parts. Hence, it can be used for online detection of defects such as infusion and voids.

scholarly journals A three-dimensional steady state thermal fluid model of jumbo ingot casting during electron beam re-melting of Ti–6Al–4V

2014 ◽  
Vol 38 (14) ◽  
pp. 3607-3623 ◽  
Author(s):  
X. Zhao ◽  
C. Reilly ◽  
L. Yao ◽  
D.M. Maijer ◽  
S.L. Cockcroft ◽  
...  
Keyword(s):  
Electron Beam ◽  
Steady State ◽  
Fluid Model ◽  
Three Dimensional ◽  
Ingot Casting

Numerical Simulation on Quenching Temperature Field of 40Cr Steel

2010 ◽  
Vol 154-155 ◽  
pp. 417-420
Author(s):  
Di Cui ◽  
He Liang
Keyword(s):  
Field Work ◽  
Cooling Curve ◽  
Work Piece ◽  
Security Assessment ◽  
Quenching Temperature ◽  
Temperature Changes ◽  
Complex Process ◽  
Medium Flow ◽  
Quenching Process ◽  
40Cr Steel

The quenching process is a complex process, which involves quenching medium flow field, work piece temperature and stress field. In this paper, the 40Cr steel belt wheel is chosen for the sample of finite element method to simulate the quenching process. The temperature changes with time at any position in the work piece are directly reflected in the actual quenching process. The cooling curves of center and general surface are obtained after simulation. Combined with cooling curve of transformation of under cooled austenite, it is easy to predict whether the technological results meet the performance of organization, and conduct a security assessment of the work piece.

On the Construction of Analytical Cooling Curves from ASTM D6200 Data Using Multi-Variable Gradient Descent Method

2021 ◽  
Author(s):  
James Jan ◽  
D. Scott MacKenzie
Keyword(s):  
Cooling Rate ◽  
Oil Quality ◽  
Standard Test ◽  
Descent Method ◽  
Test Method ◽  
Cooling Curve ◽  
Gradient Descent Method ◽  
Mathematical Function ◽  
Current Standard ◽  
Characteristic Points

Abstract ASTM D6200 is a standard test method to evaluate cooling characteristics of quench oils. The test produces six discrete numbers representing the cooling characteristics: three temporal scales (time to cool to 600°C, 400°C, and 200°C), two cooling rates (max cooling rate and cooling rate at 300°C), and one temperature scale (at max cooling rate). One of the main purposes of ASTM D6200 is to monitor the oil quality to ensure gears are properly quenched. The current standard only includes specifications for gear quenching oil and its applications are limited to physical testing. The intent of this research is to explore the possibility of broadening the support for more quenchants and extending applications to virtual engineering. This research includes two parts. The first part is the development of a systematic method to identify the characteristic points of a cooling curve. The second part is the construction of an analytical cooling curve based on the characteristic points. The analytical cooling curve is a mathematical function of temperature versus time that can provide temperature at any given time in the quenching process. In addition, the curve is differentiable to provide the cooling rate information at any given time as well.

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