One-pot Solvothermal Synthesis of lotus-leaf like Ni7S6/CoNi2S4 Hybrid on Carbon Fabric towards Comprehensive High-performance Flexible Non-Enzymatic Glucose Sensor and Supercapacitor

Author(s):  
hong zhao ◽  
Liping Tang ◽  
Man Zhou ◽  
Kai Li ◽  
Jinguang Hu ◽  
...  

Due to increased attentions on diabetes mellitus, flexible and multifunctional electrodes toward glucose detection have been desired for the construction of a wearable glucose self-monitoring system (WGSS). Herein, bifunctional Ni-Co-S...

The Analyst ◽  
2020 ◽  
Vol 145 (24) ◽  
pp. 7898-7906
Author(s):  
Victor Vinoth ◽  
Nalenthiran Pugazhenthiran ◽  
Ramalinga Viswanathan Mangalaraja ◽  
Asad Syed ◽  
Najat Marraiki ◽  
...  

The huge demand for the clinical diagnosis of diabetes mellitus has prompted the development of great-performance sensing platforms for glucose detection.


2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Jie Zhang ◽  
Yudong Sun ◽  
Xianchun Li ◽  
Jiasheng Xu

AbstractIn this work, porous NiMn2O4 nanosheet arrays on nickel foam (NiMn2O4 NSs@NF) was successfully fabricated by a simple hydrothermal step followed by a heat treatment. Porous NiMn2O4 NSs@NF is directly used as a sensor electrode for electrochemical detecting glucose. The NiMn2O4 nanosheet arrays are uniformly grown and packed on nickel foam to forming sensor electrode. The porous NiMn2O4 NSs@NF electrode not only provides the abundant accessible active sites and the effective ion-transport pathways, but also offers the efficient electron transport pathways for the electrochemical catalytic reaction by the high conductive nickel foam. This synergy effect endows porous NiMn2O4 NSs@NF with excellent electrochemical behaviors for glucose detection. The electrochemical measurements are used to investigate the performances of glucose detection. Porous NiMn2O4 NSs@NF for detecting glucose exhibits the high sensitivity of 12.2 mA mM−1 cm−2 at the window concentrations of 0.99–67.30 μM (correlation coefficient = 0.9982) and 12.3 mA mM−1 cm−2 at the window concentrations of 0.115–0.661 mM (correlation coefficient = 0.9908). In addition, porous NiMn2O4 NSs@NF also exhibits a fast response of 2 s and a low LOD of 0.24 µM. The combination of porous NiMn2O4 nanosheet arrays and nickel foam is a meaningful strategy to fabricate high performance non-enzymatic glucose sensor. These excellent properties reveal its potential application in the clinical detection of glucose.


2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Jiasheng Xu ◽  
Yuting Sun ◽  
Jie Zhang

Abstract Ferroferric oxide (Fe3O4) nanospheres have been synthesized via a facile solvothermal procedure to serve as an electrode material for high performance non-enzymatic glucose sensor. The as-synthesized Fe3O4 nanospheres with a uniform size from 16 to 18 nm, which can increase the reaction contact area and the active sites in the process of glucose detection. Benefiting from the particular nanoscale structure, the Fe3O4 nanospheres obviously enhanced the activity of electrocatalytic oxidation towards glucose. When the Fe3O4 nanospheres material was used for non-enzymatic glucose sensor, several electrochemical properties including the high sensitivity 6560 μA mM−1 cm−2 (0.1–1.1 mM), limit of detection 33 μM (S/N = 3) and good long-term stability were well demonstrated. Furthermore, Fe3O4 nanospheres electrode confirmed the excellent performance of selectivity in glucose detection with the interfering substances existed such as urea, citric acid, ascorbic acid, and NaCl. Due to the excellent electrocatalytic activity in alkaline solution, the Fe3O4 nanospheres material can be considered as a promising candidate in blood glucose monitoring.


2016 ◽  
Vol 52 (100) ◽  
pp. 14438-14441 ◽  
Author(s):  
Zao Wang ◽  
Xiaoqin Cao ◽  
Danni Liu ◽  
Shuai Hao ◽  
Gu Du ◽  
...  

NiCoP nanosheet array acts as a high-active catalyst electrode for glucose electro-oxidation in alkaline media. As a non-enzyme electrochemical glucose sensor, it shows a low detection limit of 0.13 μM (S/N = 3) and a high sensitivity of 14 586 μA mM−1 cm−2.


2014 ◽  
Vol 2 (8) ◽  
pp. 1381-1385 ◽  
Author(s):  
Ziming He ◽  
Jing Liu ◽  
Jianwei Miao ◽  
Bin Liu ◽  
Timothy Thatt Yang Tan

A simple solvothermal strategy is presented to prepare morphology-tunable hierarchical TiO2 microspheres, and the microsphere-based photoanode exhibited a power conversion efficiency of 7.95%.


2021 ◽  
Vol 27 (2) ◽  
pp. 51-68
Author(s):  
Muhd Alwi Muhd Helmi ◽  
Norsa'adah Bachok ◽  
Suhaimi Hussain

Objectives: The primary and secondary objectives were to compare the glycaemic control and frequency of hypoglycaemia between continuous glucose monitoring system (CGMS) and self-monitoring blood glucose (SMBG). Methods: A single centre, randomised, parallel-group controlled trial was conducted involving twenty-two type one Diabetes Mellitus (T1DM) patients with the mean age of 13.8 years assigned to either intervention or control group. All respondents wore the CGMS device at the beginning of the study. Intervention group (n=11) had their insulin adjusted based on the CGMS data, while the control group (n=11) was based on SMBG. Monthly average blood sugar level (BSL) and monthly mean hypoglycemic events per week (HE/wk) were measured at baseline, first month, second month, and third month. HbA1c levels were measured at baseline and in the third month. Results: The baseline characteristics were similar. The data were analysed using repeated measure analysis of variance (ANOVA). The mean difference of HbA1c within the group was not statistically significant with p=0.322. There were significant differences in the monthly mean HE/wk within and between groups, p=0.004, and p=0.037. Conclusion: In conclusion, CGMS is equivalent to SMBG in optimising glycaemic control but is more effective in detecting hypoglycaemia in children.  


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