Trace Determination of Rhodium in Coating Wastewater by Vortex Assisted Magnetic Nanoparticle Based Solid Phase Microextraction (MNP-SPME) Combined with Slotted Quartz Tube–Flame Atomic Absorption Spectrometry (SQT-FAAS) with Matrix Matching Calibration

2022 ◽  
pp. 1-13
Author(s):  
Hakan Serbest ◽  
Sezgin Bakırdere ◽  
Seyfullah Keyf
2017 ◽  
Vol 32 (12) ◽  
pp. 2433-2438 ◽  
Author(s):  
Erhan Akkaya ◽  
Nursu Aylin Kasa ◽  
Gülten Çetin ◽  
Sezgin Bakirdere

A combination of slotted quartz tube attached flame atomic absorption spectrometry (SQT-FAAS) and stearic acid coated magnetite nanoparticle based solid phase microextraction (SPME-MNP) was used for the determination of ultratrace amounts of cadmium.


2014 ◽  
Vol 29 (9) ◽  
pp. 1692-1697 ◽  
Author(s):  
Jianping Zou ◽  
Xiaoguo Ma ◽  
Yongfeng Dang ◽  
Yuan Chen

A sensitive and reliable method for trace determination of Cd(ii) and Cu(ii) based on solid-phase extraction using a novel sorbent coupled with flame atomic absorption spectrometry.


2007 ◽  
Vol 72 (6) ◽  
pp. 585-590 ◽  
Author(s):  
Morteza Talebi ◽  
Homeyra Safigholi

Arapid, simple, and sensitive procedure based on modified solid phase extraction was developed for the pre-concentration and determination of trace amount of lead in water resources. Lead was reacted with ammonium pyrrolidinedithiocarbamate (APDC) to make a complex. The complex was then collected in a column packed with surfactant-coated alumina. The parameters affecting the collection efficiency and desorption rate of the lead complexes from the column were investigated and optimized. The collection efficiency of the lead complex on the adsorbent was excellent under the optimized conditions. The results obtained from the recovery test showed the capability and reliability of the method for the analysis of trace amounts of lead. The proposed pre-concentration procedure made it possible to apply conventional flame atomic absorption spectrometry (FAAS) for the sensitive determination of trace amounts of lead in water resources. .


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