scholarly journals Parent grain reconstruction from partially or fully transformed microstructures in MTEX

2022 ◽  
Vol 55 (1) ◽  
Author(s):  
Frank Niessen ◽  
Tuomo Nyyssönen ◽  
Azdiar A. Gazder ◽  
Ralf Hielscher

A versatile generic framework for parent grain reconstruction from fully or partially transformed child microstructures has been integrated into the open-source crystallographic toolbox MTEX. The framework extends traditional parent grain reconstruction, phase transformation and variant analysis to all parent–child crystal symmetry combinations. The inherent versatility of the universally applicable parent grain reconstruction methods and the ability to conduct in-depth variant analysis are showcased via example workflows that can be programmatically modified by users to suit their specific applications. This is highlighted by three applications, namely α′-to-γ reconstruction in a lath martensitic steel, α-to-β reconstruction in a Ti alloy, and a two-step reconstruction from α′ to ɛ to γ in a twinning and transformation-induced plasticity steel. Advanced orientation relationship discovery and analysis options, including variant analysis, are demonstrated via the add-on function library ORTools.

2019 ◽  
Vol 743 ◽  
pp. 327-338 ◽  
Author(s):  
Xiaohui Bian ◽  
Ahmed A. Saleh ◽  
Peter A. Lynch ◽  
Christopher H.J. Davies ◽  
Elena V. Pereloma ◽  
...  

Author(s):  
Alexandra Roberts ◽  
John True ◽  
Nathan T. Jessurun ◽  
Dr. Navid Asadizanjani

Abstract Printed Circuit Boards (PCBs) play a critical role in everyday electronic systems, therefore the quality and assurance of the functionality for these systems is a topic of great interest to the government and industry. PCB manufacturing has been largely outsourced to cut manufacturing costs in comparison with the designing and testing of PCBs which still retains a large presence domestically. This offshoring of manufacturing has created a surge in the supply chain vulnerability for potential adversaries to garner access and attack a device via a malicious modification. Current hardware assurance and verification methods are based on electrical and optical tests. These tests are limited in the detection of malicious hardware modifications, otherwise known as Hardware Trojans. For PCB manufacturing there has been an increase in the use of automated X-ray inspection. These inspections can validate a PCB’s functionality during production. Such inspections mitigate process errors in real time but are unable to perform highresolution characterization on multi-layer fully assembled PCBs. In this paper, several X-ray reconstruction methods, ranging from proprietary to open-source, are compared. The high-fidelity, commercial NRecon software for SkyScan 2211 Multi-scale X-ray micro-Tomography system is compared to various methods from the ASTRA Toolbox. The latter is an open-source, transparent approach to reconstruction via analytical and iterative methods. The toolbox is based on C++ and MEX file functions with MATLAB and Python wrappers for analysis of PCB samples. In addition, the differences in required imaging parameters and the resultant artifacts generated by planar PCBs are compared to the imaging of cylindrical biological samples. Finally, recommendations are made for improving the ASTRA Toolbox reconstruction results and guidance is given on the appropriate scenarios for each algorithm in the context of hardware assurance for PCBs.


Materials ◽  
2019 ◽  
Vol 12 (22) ◽  
pp. 3781
Author(s):  
Zhongping He ◽  
Huachu Liu ◽  
Zhenyu Zhu ◽  
Weisen Zheng ◽  
Yanlin He ◽  
...  

Transformation Induced Plasticity (TRIP) steels with silicon–manganese (Si–Mn) as the main element have attracted a lot of attention and great interest from steel companies due to their low price, high strength, and high plasticity. Retained austenite is of primary importance as the source of high strength and high plasticity in Si–Mn TRIP steels. In this work, the cold rolled sheets of Si–Mn low carbon steel were treated with TRIP and Dual Phase (DP) treatment respectively. Then, the microstructure and composition of the Si–Mn low carbon steel were observed and tested. The static tensile test of TRIP steel and DP steel was carried out by a CMT5305 electronic universal testing machine. The self-built true stress–strain curve model of TRIP steel was verified. The simulation results were in good agreement with the experimental results. In addition, the phase transformation energy of retained austenite and the work borne by austenite in the sample during static stretching were calculated. The work done by austenite was 14.5 J, which was negligible compared with the total work of 217.8 J. The phase transformation energy absorption of retained austenite in the sample was 9.12 J. The role of retained austenite in TRIP steel is the absorption of excess energy at the key place where the fracture will occur, thereby increasing the elongation, so that the ferrite and bainite in the TRIP steel can absorb energy for a longer time and withstand more energy.


2010 ◽  
Vol 89-91 ◽  
pp. 359-364 ◽  
Author(s):  
Loïc Malet ◽  
Pascal J. Jacques ◽  
Stéphane Godet

The orientation relationships that apply to the fcc (γ) – bcc (α) phase transformation in high-performance hot-rolled TRIP-aided steels were characterised by EBSD techniques. A statistical treatment of the experimental data allows the mean orientation relationship to be determined. This mean orientation relationship was compared to the models commonly proposed in the literature and confronted qualitatively to the predictions of the phenomenological theory of martensite crystallography (PTMC). The variant selection phenomenon was also characterized quantitatively at the level of individual austenite grains. The reconstruction of the EBSD maps evidences that bainite grows by packets in which the bainite laths share a common {111}γ plane in the austenite. This growth mechanism is not influenced by the prior hot deformation of the austenite. The hot deformation has a critical influence on the number of packets that forms. The analysis of the crystallographic features of the bainite packets reveals that all possible variants are formed in a packet, though in different proportions.


2005 ◽  
Vol 495-497 ◽  
pp. 447-452 ◽  
Author(s):  
I. Lischewski ◽  
Günter Gottstein

The ferrite to austenite phase transformation in microalloyed steel was studied, with a special focus on the orientation relationship between prior ferrite and subsequent austenite. Also the role of growth selection and preferred nucleation was investigated in this context. Their effects were examined at partial phase transformation.


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