Effect of annealing temperature on TiO2 structured films by the glancing angle deposition with incline spinning substrate on rotating holder method

Author(s):  
Vatcharinkorn Mekla ◽  
Supakorn Pukird ◽  
Supanit Porntheerapat ◽  
Jiti Nukeaw
2020 ◽  
Vol 20 (8) ◽  
pp. 5006-5013
Author(s):  
Peerasil Charoenyuenyao ◽  
Nathaporn Promros ◽  
Rawiwan Chaleawpong ◽  
Pitoon Noymaliwan ◽  
Nattakorn Borwornpornmetee ◽  
...  

In the present study, indium tin oxide (ITO) nanorod films were produced by usage of ion-assisted electron-beam evaporation with a glancing angle deposition technique. The as-produced ITO nanorod films were annealed in the temperature range of 100–500 °C for two hours in a vacuum atmosphere. The as-produced ITO nanorod films exhibited (222) and (611) preferred orientations from the X-ray diffraction pattern. After vacuum annealing at 500 °C, the ITO nanorod films demonstrated many preferred orientations and the improvement of film crystallinity. The sheet resistance of the as-produced ITO nanorod films was 11.92 Ω/ and was found to be 13.63 Ω/ by annealing at 500 °C. The as-produced and annealed ITO nanorod films had a rod diameter of around 80 nm and transmittance in a visible zone of around 90%. The root mean square roughness of the as-produced ITO nanorod film’s surface was 5.49 nm, which increased to 13.77 nm at an annealing temperature of 500 °C. The contact angle of the as-produced ITO nanorod films was 110.9° and increased to 116.5° after annealing at 500 °C.


2020 ◽  
Vol 20 (5) ◽  
pp. 3274-3282 ◽  
Author(s):  
Rajshree Rajkumari ◽  
Naorem Khelchand Singh

In this article, vertically aligned WO3 nanowires were synthesized by employing the glancing angle deposition technique. The significant improvement in the crystallinity and surface morphology of the synthesized WO3 nanowires were observed for 500 °C annealed samples and beyond that temperature it starts degrading. The X-ray diffraction confirmed the different phase transition after annealing. Increase in crystallite size from 68.93 nm to 77.41 nm was observed with the increase in annealing temperature from 300 °C to 500 °C. Upon 250 nm excitation, a broad blue emission aroused by near band edge emission is observed. Also, other emission peaks were observed due to the localized states of oxygen vacancies in the conduction band of WO3. Fourier transform infrared result shows the bonding of WO3 nanowires and intensity were greatly enhanced as the annealing temperature increases up to 500 °C. These enhancements in the properties could be applicable for the development of WO3 based nanodevices.


2021 ◽  
pp. 2100071
Author(s):  
Fernando Fresno ◽  
María U. González ◽  
Lidia Martínez ◽  
Marcial Fernández‐Castro ◽  
Mariam Barawi ◽  
...  

2012 ◽  
Vol 258 (24) ◽  
pp. 9762-9769 ◽  
Author(s):  
C. Khare ◽  
J.W. Gerlach ◽  
T. Höche ◽  
B. Fuhrmann ◽  
H.S. Leipner ◽  
...  

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