Thermal Annealing Dependence of High-Frequency Magnetoimpedance in Amorphous and Nanocrystalline FeSiBCuNb Ribbons

2008 ◽  
Vol 8 (6) ◽  
pp. 2873-2882 ◽  
Author(s):  
B. Hernando ◽  
V. M. Prida ◽  
M. L. Sanchez ◽  
J. Olivera ◽  
C. Garcia ◽  
...  

The magnetoimpedance (MI) effect in Fe73.5Si13.5B9Nb3Cu1 melt-spun amorphous ribbons has been studied in the frequency range (1–500 MHz). Isothermal heating treatments in a furnace have been employed to nanocrystallize the ribbons (1 h at 565 °C in a vacuum of 10–3 mbar), while other samples were annealed at lower temperatures (400 and 475 °C during 1 h), in order to evaluate the influence of the annealing temperature on the MI effect. The high-frequency impedance was measured using a technique based on the reflection coefficient measurements of a specific transmission line by using a network analyzer. Frequency dependence of the MI ratio, ΔZ/Z, and both resistive, ΔR/R, and reactive, ΔX/X, components of magnetoimpedance were measured in the amorphous and annealed states, at different temperatures. A maximum value of the MI ratio of about 50% at a driving frequency of 18 MHz is obtained in the nanocrystalline (annealed at 565 °C) ribbon. Maxima for R/R of about 81% at 85 MHz and ΔX/X around 140% at 5 MHz were also achieved. It is revealed that the microstructural evolution in the nanocrystalline sample leads to a magnetic softening, an optimum domain structure and a permeability which is sensitive to frequency and applied magnetic field, generating a large MI response.

2007 ◽  
Vol 280-283 ◽  
pp. 919-924
Author(s):  
M.S. Jogad ◽  
V.K. Shrikhande ◽  
A.H. Dyama ◽  
L.A. Udachan ◽  
Govind P. Kothiyal

AC and DC conductivities have been measured by using the real (e¢) and imaginary (e¢¢) parts of the dielectric constant data of glass and glass-ceramics (GC) at different temperatures in the rage 297-642K and in the frequency range 100 Hz to 10 MHz. Using Anderson –Stuart model, we have calculated the activation energy, which is observed to be lower than that of the DC conductivity. The analysis for glass/glass-ceramics indicates that the conductivity variation with frequency exhibits an initial linear region followed by nonlinear region with a maximum in the high-frequency region. The observed frequency dependence of ionic conductivity has been analyzed within the extended Anderson–Stuart model considering both the electrostatic and elastic strain terms. In glass/glassceramic the calculations based on the Anderson-Stuart model agree with the experimental observations in the low frequency region but at higher frequencies there is departure from measured data.


2009 ◽  
Vol 155 ◽  
pp. 173-188
Author(s):  
Kanhaiya Lal Yadav

A simple citrate gel process was used to prepare nanocomposites of xCuFe2O4–(1−x)BiFeO3 (henceforth, CFBF) and xNi0.75Co0.25Fe2O4-(1-x)BiFeO3 (henceforth, NCFBF) with x=0.1, 0.2, 0.3 and 0.4. The phase was found to be formed at 500 °C and 700 °C for CFBF and NCFBF respectively. TEM observation showed that the average particles size is around 40 nm. The variation of the dielectric constant and the dielectric loss with frequency showed dispersion in the low frequency range. All the samples exhibit strong magnetic characteristics. The coercivity and squareness increased with the increase in annealing temperature and were maximum for samples annealed at 500°C and 700°C for CFBF and NCFBF nanocomposites, respectively, and further decrease in coercivity is attributed to decrease in aspect ratio and pinning effects in the nanocrysatllites. The ME coefficient αE showed strong dependence on HBias and maximum value of ME coefficients were 303 and 309 mV/cm Oe at magnetic field frequency of 50 kHz for CFBF and NCFBF nanocomposites respectively. The large values of ME coefficients are attributed to low coercivity, large magnetization and small crystallite size of constituent phases.


2016 ◽  
Vol 23 (03) ◽  
pp. 1650002 ◽  
Author(s):  
VALI DALOUJI ◽  
SMOHAMMAD ELAHI

In this work, the microstructure and magnetic properties of carbon–nickel (C–Ni) composite films annealed at different temperatures (300–1000[Formula: see text]C) were investigated. The films were grown by radio frequency magnetron sputtering on quartz substrates at room temperature. The nickel concentration in the films are affected by changing of the value of evaporation nickel atoms and measured by Rutherford backscattering spectroscopy (RBS). Values of coercive field were measured under both increasing and decreasing applied magnetic field. It is shown that the coercive field of films strongly dependent on the annealing temperature and at 500[Formula: see text]C films has maximum value of 93.67[Formula: see text]Oe. The difference in the coercive fields increased for films annealed from 300 to 500[Formula: see text]C and then decreased from 500 to 1000[Formula: see text]C. The ID/IG ratio of Raman spectra would indicate the presence of higher sp2 bonded carbon in the films annealed at 800[Formula: see text]C.


1971 ◽  
Vol 36 (4) ◽  
pp. 527-537 ◽  
Author(s):  
Norman P. Erber

Two types of special hearing aid have been developed recently to improve the reception of speech by profoundly deaf children. In a different way, each special system provides greater low-frequency acoustic stimulation to deaf ears than does a conventional hearing aid. One of the devices extends the low-frequency limit of amplification; the other shifts high-frequency energy to a lower frequency range. In general, previous evaluations of these special hearing aids have obtained inconsistent or inconclusive results. This paper reviews most of the published research on the use of special hearing aids by deaf children, summarizes several unpublished studies, and suggests a set of guidelines for future evaluations of special and conventional amplification systems.


2017 ◽  
Vol 76 (10) ◽  
pp. 929-940 ◽  
Author(s):  
Yu. S. Kovshov ◽  
S. S. Ponomarenko ◽  
S. A. Kishko ◽  
A. A. Likhachev ◽  
S. A. Vlasenko ◽  
...  

2016 ◽  
Vol 12 (2) ◽  
pp. 4204-4212 ◽  
Author(s):  
Maheshwar Sharon ◽  
Ritesh Vishwakarma ◽  
Abhijeet Rajendra Phatak ◽  
Golap Kalita ◽  
Nallin Sharma ◽  
...  

Corn cob, an agricultural waste, is paralyzed at different temperatures (700oC, 800oC and 900oC). Microwave absorption of carbon in the frequency range of 2 GHz to 8 GHz is reported. Carbon activated  with 5%  nickel nitrate showed more than 90% absorption of microwave in the frequency range from 6 GHz to 8 GHz, while carbon activated  with 10% Nickel nitrate treated corn cob showed 90% absorption  in the frequency range of 2.5 GHz to 5 GHz. Carbon showing the best absorption are characterized by XRD, Raman spectra and SEM . It is suggested that corn cob treatment   alone with KOH did not improve the microwave absorption, whereas treatment along with nickel nitrate improved the absorption property much better. It is proposed that treatment with nickel nitrate helps in creating suitable pores in carbon   which improved the absorption behavior because while treating carbon with 1N HCl helps to leach out nickel creating equivalent amount of pores in the carbon.


2021 ◽  
Vol 11 (12) ◽  
pp. 5415
Author(s):  
Aleksandr Gorst ◽  
Kseniya Zavyalova ◽  
Aleksandr Mironchev ◽  
Andrey Zapasnoy ◽  
Andrey Klokov

The article investigates the near-field probe of a special design to account for changes in glucose concentration. The probe is designed in such a way that it emits radiation in both directions from its plane. In this paper, it was proposed to modernize this design and consider the unidirectional emission of the probe in order to maximize the signal and reduce energy loss. We have done extensive research for both bidirectional and unidirectional probe designs. Numerical simulations and field experiments were carried out to determine different concentrations of glucose (0, 4, 5.3, 7.5 mmol/L). Numerical modeling of a unidirectional probe showed that the interaction of radiation generated by such a probe with a multilayer structure simulating a human hand showed a better result and high sensitivity compared to a bidirectional probe. Further, based on the simulation results, a phantom (physical model) of a human hand was recreated from layers with dielectric properties as close as possible to the properties of materials during simulation. The probe was constructed from a copper tube and matched both the geometric and physical parameters of the model. The experimental measurement was carried out using a vector network analyzer in the frequency range 2–10 GHz. The experimental measurement was carried out using a vector network analyzer in the frequency range 2–10 GHz for the unidirectional and bidirectional probes. Further, the results of the experiment were compared with the results of numerical simulation. According to the results of multiple experiments, it was found that the average deviation between the concentrations was 2 dB for a unidirectional probe and 0.4 dB for a bidirectional probe. Thus, the sensitivity of the unidirectional probe was 1.5 dB/(mmol/L) for the bidirectional one 0.3 dB/(mmol/L). Thus, the improved design of the near-field probe can be used to record glucose concentrations.


Nanomaterials ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 1097
Author(s):  
Luran Zhang ◽  
Xinchen Du ◽  
Hongjie Lu ◽  
Dandan Gao ◽  
Huan Liu ◽  
...  

L10 ordered FePt and FePtCu nanoparticles (NPs) with a good dispersion were successfully fabricated by a simple, green, one-step solid-phase reduction method. Fe (acac)3, Pt (acac)2, and CuO as the precursors were dispersed in NaCl and annealed at different temperatures with an H2-containing atmosphere. As the annealing temperature increased, the chemical order parameter (S), average particle size (D), coercivity (Hc), and saturation magnetization (Ms) of FePt and FePtCu NPs increased and the size distribution range of the particles became wider. The ordered degree, D, Hc, and Ms of FePt NPs were greatly improved by adding 5% Cu. The highest S, D, Hc, and Ms were obtained when FePtCu NPs annealed at 750 °C, which were 0.91, 4.87 nm, 12,200 Oe, and 23.38 emu/g, respectively. The structure and magnetic properties of FePt and FePtCu NPs at different annealing temperatures were investigated and the formation mechanism of FePt and FePtCu NPs were discussed in detail.


2021 ◽  
Vol 11 (4) ◽  
pp. 1932
Author(s):  
Weixuan Wang ◽  
Qinyan Xing ◽  
Qinghao Yang

Based on the newly proposed generalized Galerkin weak form (GGW) method, a two-step time integration method with controllable numerical dissipation is presented. In the first sub-step, the GGW method is used, and in the second sub-step, a new parameter is introduced by using the idea of a trapezoidal integral. According to the numerical analysis, it can be concluded that this method is unconditionally stable and its numerical damping is controllable with the change in introduced parameters. Compared with the GGW method, this two-step scheme avoids the fast numerical dissipation in a low-frequency range. To highlight the performance of the proposed method, some numerical problems are presented and illustrated which show that this method possesses superior accuracy, stability and efficiency compared with conventional trapezoidal rule, the Wilson method, and the Bathe method. High accuracy in a low-frequency range and controllable numerical dissipation in a high-frequency range are both the merits of the method.


Nanomaterials ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1802
Author(s):  
Dan Liu ◽  
Peng Shi ◽  
Yantao Liu ◽  
Yijun Zhang ◽  
Bian Tian ◽  
...  

La0.8Sr0.2CrO3 (0.2LSCO) thin films were prepared via the RF sputtering method to fabricate thin-film thermocouples (TFTCs), and post-annealing processes were employed to optimize their properties to sense high temperatures. The XRD patterns of the 0.2LSCO thin films showed a pure phase, and their crystallinities increased with the post-annealing temperature from 800 °C to 1000 °C, while some impurity phases of Cr2O3 and SrCr2O7 were observed above 1000 °C. The surface images indicated that the grain size increased first and then decreased, and the maximum size was 0.71 μm at 1100 °C. The cross-sectional images showed that the thickness of the 0.2LSCO thin films decreased significantly above 1000 °C, which was mainly due to the evaporation of Sr2+ and Cr3+. At the same time, the maximum conductivity was achieved for the film annealed at 1000 °C, which was 6.25 × 10−2 S/cm. When the thin films post-annealed at different temperatures were coupled with Pt reference electrodes to form TFTCs, the trend of output voltage to first increase and then decrease was observed, and the maximum average Seebeck coefficient of 167.8 µV/°C was obtained for the 0.2LSCO thin film post-annealed at 1100 °C. Through post-annealing optimization, the best post-annealing temperature was 1000 °C, which made the 0.2LSCO thin film more stable to monitor the temperatures of turbine engines for a long period of time.


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