Preparation and characterization of graft copolymerized Cannabis indica L. fiber-reinforced unsaturated polyester matrix-based biocomposites

2012 ◽  
Vol 31 (22) ◽  
pp. 1538-1553 ◽  
Author(s):  
Amar S Singha ◽  
Ashvinder K Rana
Keyword(s):  
Unsaturated Polyester ◽  
Fiber Reinforced ◽  
Polyester Matrix ◽  
Cannabis Indica

scholarly journals Characterization of Polyester Nanocomposites Reinforced with Conifer Fiber Cellulose Nanocrystals

Polymers ◽  
2020 ◽  
Vol 12 (12) ◽  
pp. 2838
Author(s):  
Grazielle da Silva Maradini ◽  
Michel Picanço Oliveira ◽  
Gabriel Madeira da Silva Guanaes ◽  
Gabriel Zuqui Passamani ◽  
Lilian Gasparelli Carreira ◽  
...  
Keyword(s):  
Cellulose Nanocrystals ◽  
Unsaturated Polyester ◽  
Cost Effective ◽  
Bending Test ◽  
X Ray Diffraction ◽  
Xrd Pattern ◽  
Glass Fiber Composites ◽  
Superior Mechanical Properties ◽  
Polyester Matrix

The application of cellulose nanocrystal has lately been investigated as polymer composites reinforcement owing to favorable characteristics of biodegradability and cost effectiveness as well as superior mechanical properties. In the present work novel nanocomposites of unsaturated polyester matrix reinforced with low amount of 1, 2, and 3 wt% of cellulose nanocrystals obtained from conifer fiber (CNC) were characterized. The polyester matrix and nanocomposites were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), bending test, and thermogravimetric analysis (TGA). The result showed that the addition of only 2 wt% CNC increased the nanocomposite flexural strength by 159%, the ductility by 500% and the toughness by 1420%. Fracture analyses by SEM revealed a uniform participation of the CNC in the polyester microstructure. The resistance to thermal degradation of the CNC reinforced nanocomposites was improved in more than 20 °C as compared to neat polyester. No significant changes were detected in the water absorptions and XRD pattern of the neat polyester with incorporations up to 3 wt% CNC. These results reveal that the 2 wt% CNC nanocomposite might be a promising more ductile, lightweight and cost-effective substitute for conventional glass fiber composites in engineering applications.

scholarly journals Characterization of Ceramic Waste Filled Unsaturated Polyester Resin

2020 ◽  
Vol 57 (3) ◽  
pp. 52-60
Author(s):  
Mohamed Farsane ◽  
Abdellah Anouar ◽  
Souad Chah ◽  
Miloud Bouzziri
Keyword(s):  
Water Absorption ◽  
Polyester Resin ◽  
Filler Content ◽  
Unsaturated Polyester ◽  
Unsaturated Polyester Resin ◽  
Ceramic Waste ◽  
The Matrix ◽  
Polyester Matrix ◽  
Resin Formulation

In this study, the composites of ceramic waste filler polyester were produced with ceramic waste as the filler and unsaturated polyester resin as the matrix. Various weight of filler loads (particle size [180 �m) were used; 0, 28.5, 41 and 50 wt% in view to better understand the effect of filler content on the mechanical, thermal properties and water absorption of the composites. Additionally, Fourier transform infrared spectroscopy was used to characterize the samples, from the findings, it is noticed an increase in the level of porcelain powder decreased the flexural strength and Hardness and increased the density. The results of water absorption have shown the composites absorbs fewer water. Thermal degradation indicates that the composite is more resistant to temperature than unsaturated polyester matrix due to the effect of porcelain powder incorporated. Moreover, the results reveal an opportunity for using the ceramic waste as filler in unsaturated polyester resin formulation.

Jute Fiber Reinforced Polymeric Composites With Flexible Interphase

2012 ◽  
Author(s):  
Tetsushi Koshino ◽  
Mohamed S. Aly-Hassan ◽  
Hiroyuki Hamada
Keyword(s):  
Unsaturated Polyester ◽  
Weight Ratio ◽  
Matrix Cracking ◽  
Jute Fiber ◽  
Matrix Composites ◽  
Fiber Reinforced ◽  
Jute Fibers ◽  
Jute Cloth ◽  
Polyester Matrix ◽  
The Impact

In this research, the flexible interphase concept was introduced to enhance the poor mechanical properties of jute fiber reinforced unsaturated polyester matrix composites. The jute cloth reinforcement was obtained from recycled coffee bags. These jute cloths after washing by water and drying were soaked in mixture of Polybutadiene Epoxydied as flexible resin and acetone for 10 seconds. Several mixtures consist of 0, 2, 3.5, 5 and 8 wt% of Polybutadiene Epoxydied and 100, 98, 96.5, 95 and 92 wt% of acetone, respectively, to form flexible interface around the jute fibers. Jute cloth reinforced unsaturated polyester matrix composites with different flexible interphase incremental weight ((Wa-Wb)/Wb) ratios were fabricated by hand lay-up method and examined by a series of mechanical tests. The mechanical testing including tensile, bending, Izod strength impact and drop impact was carried out for these composites to evaluate the effect of the flexible interphase and acetone on the jute cloth composites. The flexible interphase succeed to control the mechanical properties of jute fiber reinforced unsaturated polyester matrix composites. Inserting flexible interphase between unsaturated polyester matrix and jute fibers leads to smooth fluctuation, less matrix cracking, in the second part after the knee point of each stress-strain curve as exhibited in composites with higher flexible interphase incremental weight ratio. This means not only the brittle matrix but also interface/interphase dominates the multiple matrix cracking behavior in jute cloth reinforced unsaturated polyester matrix composites. Inserting flexible interphase between unsaturated polyester matrix and jute fibers leads to less number of multiple cracking as shown in the second portion of flexural stress-displacement curve. This means the number of multiple cracking are dominated by flexible interphase. The impact strength of jute cloth reinforced unsaturated polyester matrix composites with flexible interphase incremental weight ratio of 1.2% is higher than that of jute cloth reinforced unsaturated polyester matrix composites without flexible interphase by about 45%. The impact energy after maximum load has increased significantly with all flexible interphase incremental weight ratios.

Studies on the Mechanical Characterization of Jute Fiber Reinforced Unsaturated Polyester Resin Based Composites: Effect of Weave Structure and Yarn Density

2019 ◽  
Vol 1156 ◽  
pp. 69-78
Author(s):  
Kamrun N. Keya ◽  
Nasrin A. Kona ◽  
Ruhul A. Khan
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Polyester Resin ◽  
Mechanical Characterization ◽  
Unsaturated Polyester ◽  
Unsaturated Polyester Resin ◽  
Degradation Behavior ◽  
Fiber Reinforced ◽  
Weave Structure

This paper represents a comparative study of the different weave structures of jute woven fiber reinforced unsaturated polyester resin (UPR) composites. The weave structures were selected as plain (1/1), twill (2/1), twill (3/1) and basket (2/2). Composites (50% fiber by wt.) were prepared by using hand lay-up technique. The mechanical properties such as tensile strength (TS), bending strength (BS) and impact strength (IS) of the composites were evaluated and compared. It was found that basket weave/UPR based composite showed the highest mechanical properties. The optimum value of TS, BS, TM, BM and IS of the composite were found to be 47 MPa, 80 MPa, 1.4 GPa, 4.8 GPa and 27 KJ/m2.To find out the effect of yarn density on mechanical properties of the composites, 2/1 twill structure was selected and found significant improvement in the mechanical properties with the increase of Ends/Inch (EPI) and Picks/Inch (PPI) in the fabric. Water uptake and degradation behavior in aqueous medium of the composites was also observed.

TEM characterization of reaction zone in a SiC fiber-reinforced titanium alloy

1988 ◽  
Vol 46 ◽  
pp. 738-739
Author(s):  
G. Das ◽  
R. E. Omlor
Keyword(s):  
Titanium Alloys ◽  
Reaction Zone ◽  
Carbon Layer ◽  
Fiber Reinforced ◽  
Reaction Products ◽  
Sic Fibers ◽  
Sic Fiber ◽  
The Matrix ◽  
Immense Potential

Fiber reinforced titanium alloys hold immense potential for applications in the aerospace industry. However, chemical reaction between the fibers and the titanium alloys at fabrication temperatures leads to the formation of brittle reaction products which limits their development. In the present study, coated SiC fibers have been used to evaluate the effects of surface coating on the reaction zone in the SiC/IMI829 system.IMI829 (Ti-5.5A1-3.5Sn-3.0Zr-0.3Mo-1Nb-0.3Si), a near alpha alloy, in the form of PREP powder (-35 mesh), was used a茸 the matrix. CVD grown AVCO SCS-6 SiC fibers were used as discontinuous reinforcements. These fibers of 142μm diameter contained an overlayer with high Si/C ratio on top of an amorphous carbon layer, the thickness of the coating being ∽ 1μm. SCS-6 fibers, broken into ∽ 2mm lengths, were mixed with IMI829 powder (representing < 0.1vol%) and the mixture was consolidated by HIP'ing at 871°C/0. 28GPa/4h.

Characterization of interfaces in CVD-coated nicalon fiber-reinforced SiC

1989 ◽  
Vol 47 ◽  
pp. 556-557
Author(s):  
K.L. More ◽  
R.A. Lowden
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Chemical Vapor ◽  
Chemical Vapor Infiltration ◽  
Frictional Stress ◽  
Fiber Reinforced ◽  
Pull Out ◽  
Carbon Coated ◽  
Fiber Matrix

The mechanical properties of fiber-reinforced composites are directly related to the nature of the fiber-matrix bond. Fracture toughness is improved when debonding, crack deflection, and fiber pull-out occur which in turn depend on a weak interfacial bond. The interfacial characteristics of fiber-reinforced ceramics can be altered by applying thin coatings to the fibers prior to composite fabrication. In a previous study, Lowden and co-workers coated Nicalon fibers (Nippon Carbon Company) with silicon and carbon prior to chemical vapor infiltration with SiC and determined the influence of interfacial frictional stress on fracture phenomena. They found that the silicon-coated Nicalon fiber-reinforced SiC had low flexure strengths and brittle fracture whereas the composites containing carbon coated fibers exhibited improved strength and fracture toughness. In this study, coatings of boron or BN were applied to Nicalon fibers via chemical vapor deposition (CVD) and the fibers were subsequently incorporated in a SiC matrix. The fiber-matrix interfaces were characterized using transmission and scanning electron microscopy (TEM and SEM). Mechanical properties were determined and compared to those obtained for uncoated Nicalon fiber-reinforced SiC.

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