scholarly journals Effect of physical and chemical parameters on the β-Tricalcium phosphate synthesized by the wet chemical method

2018 ◽  
Vol 7 (3) ◽  
pp. 234-242
Author(s):  
Asmaa Massit ◽  
Majda Fathi ◽  
Ahmed El Yacoubi ◽  
Abdelilah Kholtei ◽  
Brahim Chafik El Idrissi
Keyword(s):  
Tricalcium Phosphate ◽  
Chemical Method ◽  
Calcium Nitrate ◽  
Calcium Nitrate Tetrahydrate ◽  
Wet Chemical Method ◽  
Nanosized Powders ◽  
Synthesis Conditions ◽  
Addition Rate ◽  
Wet Chemical ◽  
Physical And Chemical

In this paper, the synthesis of nanosized powders β -Tricalcium phosphate β -Ca3(PO4)2 was studied by the wet chemical method at different values of reaction temperature, initial concentration of diammonium hydrogen phosphate (NH4)2HPO4, calcium nitrate tetrahydrate Ca(NO3)2·4H2O addition rate, pH of reaction and aging time. All these parameters have a great impact on the properties of the resulting β-TCP nano powders. Analysis results of morphology, structure of TCP powder from infrared (IR) spectra, X-ray diffraction (XRD) and transmission electron microscopy (TEM) indicated that the synthesized TCP powder had spherical crystal shape with crystallite size, calculated by XRD method, less than 60 nm, mono and biphasic structure composed of βTCP with pyrophosphate calcium or hydroxyapatite. The variation of the synthesis conditions did not affect the morphology, but it affect the size of crystallites and particles.

scholarly journals Synthesis of plate-like β-tricalcium phosphate nanoparticles and their efficiency in remineralization of incipient enamel caries

2019 ◽  
Vol 8 (4) ◽  
pp. 261-276
Author(s):  
Roghayyeh Marefat Seyedlar ◽  
Mohammadbagher Rezvani ◽  
Samira Barari ◽  
Mohammad Imani ◽  
Azizollah Nodehi ◽  
...  
Keyword(s):  
Tricalcium Phosphate ◽  
Calcium Nitrate ◽  
Negative Control ◽  
Second Phase ◽  
Calcium Nitrate Tetrahydrate ◽  
Enamel Caries ◽  
Nitrate Tetrahydrate ◽  
Addition Rate ◽  
Post Hoc ◽  
Caries Lesions

AbstractThe purpose of this study was to synthesize nano-sized β-tricalcium phosphate (nano-TCP) particles and determine its concentration-dependent properties on incipient enamel caries lesions. Nano-TCP was synthesized as a wet chemical through a method using low concentration of precursors and low addition rate of calcium nitrate tetrahydrate as a second phase. Morphology and phase composition of the particles were analyzed by SEM, XRD, and EDXA techniques. Incipient enamel lesions were created in human premolars with an acidic buffer. The teeth were then incubated in aqueous dispersions of nano-TCP as remineralization solutions. Sodium fluoride solution and deionized water were used as positive and negative control groups, respectively. The quality and thickness of the remineralized layer on enamel were investigated using SEM. The data were statistically analyzed by analysis of variance (ANOVA) and post hoc Tukey’s test. The synthesized nano-TCP mostly consisted of porous platelet-like crystals of 50–100 nm thickness and pore diameters of 100–300 nm. SEM observation showed that a homogenous layer was formed on the surface of the enamels remineralized in nano-TCP solutions. The thickness of the mineralized layer was dependent on the incubation time and nano-TCP concentration.

Impact of LiTi2(PO4)3 coating on the electrochemical performance of Li1.2Ni0.13Mn0.54Co0.13O2 using a wet chemical method

Ionics ◽  
2021 ◽  
Vol 27 (4) ◽  
pp. 1465-1475
Author(s):  
Ning Zhang ◽  
Ying Li ◽  
Yadan Luo ◽  
Zhen Yang ◽  
Jiayao Lu
Keyword(s):  
Electrochemical Performance ◽  
Chemical Method ◽  
Wet Chemical Method ◽  
Wet Chemical

Hybrids of cobalt nanochains and polyvinylidene fluoride with enhanced microwave absorption performance

RSC Advances ◽  
2016 ◽  
Vol 6 (60) ◽  
pp. 55546-55551 ◽  
Author(s):  
Shu-Qing Lv ◽  
Ya-Fei Pan ◽  
Pei-Bo Yang ◽  
Guang-Sheng Wang
Keyword(s):  
Microwave Absorption ◽  
Polyvinylidene Fluoride ◽  
Chemical Method ◽  
Wet Chemical Method ◽  
Absorption Properties ◽  
Flexible Film ◽  
Absorption Performance ◽  
Wet Chemical ◽  
Microwave Absorption Performance

By using a simple wet chemical method and hot-molding procedure, a kind of flexible film with enhance absorption properties based on binary cobalt nanochains/polyvinylidene fluoride (PVDF) hybrids has been successfully fabricated.

Development of a wet chemical method for the synthesis of arrayed ZnO nanorods

2010 ◽  
Vol 500 (2) ◽  
pp. L17-L21 ◽  
Author(s):  
Shao-Hwa Hu ◽  
Yi-Chuan Chen ◽  
Chyi-Ching Hwang ◽  
Cheng-Hsiung Peng ◽  
Dah-Chuan Gong
Keyword(s):  
Chemical Method ◽  
Zno Nanorods ◽  
Wet Chemical Method ◽  
Wet Chemical

scholarly journals Characterization of ferrite nanoparticles for preparation of biocomposites

2017 ◽  
Vol 8 ◽  
pp. 1257-1265 ◽  
Author(s):  
Urszula Klekotka ◽  
Magdalena Rogowska ◽  
Dariusz Satuła ◽  
Beata Kalska-Szostko
Keyword(s):  
Chemical Method ◽  
Ferrite Nanoparticles ◽  
Chemical Activity ◽  
Nominal Composition ◽  
X Ray Diffraction ◽  
Wet Chemical Method ◽  
X Ray ◽  
Transmission Electron ◽  
Wet Chemical

Ferrite nanoparticles with nominal composition Me0.5Fe2.5O4 (Me = Co, Fe, Ni or Mn) have been successfully prepared by the wet chemical method. The obtained particles have a mean diameter of 11–16 ± 2 nm and were modified to improve their magnetic properties and chemical activity. The surface of the pristine nanoparticles was functionalized afterwards with –COOH and –NH2 groups to obtain a bioactive layer. To achieve our goal, two different modification approaches were realized. In the first one, glutaraldehyde was attached to the nanoparticles as a linker. In the second one, direct bonding of such nanoparticles with a bioparticle was studied. In subsequent steps, the nanoparticles were immobilized with enzymes such as albumin, glucose oxidase, lipase and trypsin as a test bioparticles. The characterization of the nanoparticles was acheived by transmission electron microscopy, X-ray diffraction, energy dispersive X-ray and Mössbauer spectroscopy. The effect of the obtained biocomposites was monitored by Fourier transform infrared spectroscopy. The obtained results show that in some cases the use of glutaraldehyde was crucial (albumin).

Wet chemical method for synthesis of superparamagnetic alloyed NiPd and NiPt nanomagnets in micelles

2003 ◽  
Vol 265 (1) ◽  
pp. 23-28 ◽  
Author(s):  
Madhuri Mandal ◽  
Subrata Kundu ◽  
Sujit Kumar Ghosh ◽  
Tapan K. Sau ◽  
S.M. Yusuf ◽  
...  
Keyword(s):  
Chemical Method ◽  
Wet Chemical Method ◽  
Wet Chemical

Controllable wet synthesis of multicomponent copper-based catalysts for Rochow reaction

RSC Advances ◽  
2015 ◽  
Vol 5 (89) ◽  
pp. 73011-73019 ◽  
Author(s):  
Yanzhao Zhai ◽  
Yongjun Ji ◽  
Guangna Wang ◽  
Yongxia Zhu ◽  
Hezhi Liu ◽  
...  
Keyword(s):  
Synergistic Effect ◽  
Chemical Method ◽  
Wet Chemical Method ◽  
Wet Chemical ◽  
Improved Performance ◽  
Wet Synthesis

Ternary CuO–Cu2O–Cu synthesized by a wet chemical method showed improved performance in the Rochow reaction due to the synergistic effect.

scholarly journals Studies on the control of ZnO nanostructures by wet chemical method and plausible mechanism

AIP Advances ◽  
2015 ◽  
Vol 5 (9) ◽  
pp. 097118 ◽  
Author(s):  
Amit Kumar Rana ◽  
Yogendra Kumar ◽  
Niharika Saxena ◽  
Rajasree Das ◽  
Somaditya Sen ◽  
...  
Keyword(s):  
Chemical Method ◽  
Zno Nanostructures ◽  
Wet Chemical Method ◽  
Plausible Mechanism ◽  
Wet Chemical
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