scholarly journals Rapid test for detecting artificial colorants in wine products

2021 ◽  
Vol 25 (2) ◽  
pp. 126-133
Author(s):  
N. S. Anikina ◽  
◽  
N. V. Gnilomedova ◽  
S. N. Cherviak ◽  
A. V. Vesiutova ◽  
...  

The problem of wine color adulteration is relevant all over the world, and, therefore, establishing or refuting the fact of the colorant presence is an integral part of the techno-chemical control. There are many methods for determining artificial colorants (AC) in the alcoholic beverages with various levels of sensitivity and selectivity of detection as well as the promptness in generating the results and the cost of studying one sample. Current work is devoted to the development of a rapid test for detecting the artificial colorants in wines. It is based on the method of the International Organization of Vine and Wine, the principle of which is to fixate the acidic artificial colorants on a specially prepared woolen thread when boiling the sample of wine. The modification of analytical procedure included the reduction of the test sample aliquot, the number of operations and the examination time without compromising the reliability of the conclusion. In order to imitate the color of red wines, Azorubine (E122), Allura Red AC (E129) and Indigo Carmine (E132) food colorants were used. The objects of the research were: model systems based on wine, white and red wines, counterfeit wines provided by the controlling authorities, and concentrated grape must. It was shown that in the genuine wines, depending on the color saturation of the test sample caused by natural anthocyanins, the woolen thread was discoloring from light to dark beige; its color was enhancing from pale pink to deep ruby with the increase in the content of AC in wine. The sensitivity of the proposed method made it possible to determine the presence of AC at the rate of 0.1-0.2 mg/dm3 in wines. The method did not require expensive equipment and could be used in the laboratories of winemaking industry or by the controlling authorities for establishing the fact of adulteration of alcoholic and juice products.

2021 ◽  
pp. 1-10
Author(s):  
Peter Bjerregaard ◽  
Christina Viskum Lytken Larsen

Abstract Objective: Dietary transition, obesity and risky use of alcohol and tobacco are challenges to public health among indigenous peoples. The aim of the article was to explore the role of social position in dietary patterns and expenditures on food and other commodities. Design: Countrywide population health survey. Setting: Greenland. Participants: 2436 Inuit aged 15+ years. Results: Less than half of the expenditures on commodities (43 %) were used to buy nutritious food, and the remaining to buy non-nutritious food (21 %), alcoholic beverages (18 %) and tobacco (18 %). Participants were classified according to five dietary patterns. The cost of a balanced diet and an unhealthy diet was similar, but the cost per 1000 kJ was higher and the energy consumption was lower for the balanced diet. Participants with low social position chose the unhealthy pattern more often than those with high social position (40 % v. 24 %; P < 0·0001), whereas those with high social position more often chose the balanced alternative. Participants with low social position spent less money on the total food basket than those with high social position but more on non-nutritious food, alcohol and tobacco. Conclusions: Cost seems to be less important than other mechanisms in the shaping of social dietary patterns and the use of alcohol and tobacco among the Inuit in Greenland. Rather than increasing the price of non-nutritious food or subsidising nutritious food, socially targeted interventions and public health promotion regarding food choice and prevention of excessive alcohol use and smoking are needed to change the purchase patterns.


Molecules ◽  
2021 ◽  
Vol 26 (4) ◽  
pp. 815
Author(s):  
Francesca Coppola ◽  
Luigi Picariello ◽  
Martino Forino ◽  
Luigi Moio ◽  
Angelita Gambuti

Background: Three accelerated oxidation tests were proposed to simulate red wine oxidation thus providing information useful to correctly manage moderate oxygen exposure of wine during aging in regard to phenolic composition and wine color. Since the results of the tests have never been compared on wines with different initial composition, the aim of this study was to find a suitable method to simulate oxidation of any still red wine. Methods: Aglianico, Barbera, Gaglioppo, Magliocco, and Nerello wines were treated with (1) three cycles of air saturation, (2) the addition of hydrogen peroxide, and (3) the addition of acetaldehyde. Changes in chromatic characteristics and phenolic composition were determined by spectrophotometric and HPLC methods. Results: Important differences in the behavior of the different wines were detected: the highest formation of polymeric pigments was observed in Barbera and Aglianico wines. In contrast, Gaglioppo and Magliocco wines showed a lower variability before and after the oxidation probably due to the lower anthocyanin/tannin ratio. Among the accelerated oxidation tests applied, no significant differences in color parameters and phenolic composition were detected in samples treated with the addition of H2O2 and the air saturation method. Conclusion: The study demonstrated that H2O2 addition is a successful tool to predict the evolution of different phenolic compounds during the air saturation treatment of wines.


2021 ◽  
Vol 23 (1) ◽  
Author(s):  
Shunichi Yokota ◽  
Keita Sakamoto ◽  
Yukie Shimizu ◽  
Tsuyoshi Asano ◽  
Daisuke Takahashi ◽  
...  

Abstract Background This study aimed to investigate the ability of whole-body bone scintigraphy (WB-BS) in the detection of multifocal osteonecrosis (ON) compared to whole-body magnetic resonance imaging (WB-MRI) and to clarify the characteristics of patients with multifocal ON among those with ON of the femoral head (ONFH) using WB-MRI. Methods Forty-six patients who had symptomatic ONFH and underwent surgery in our hospital from April 2019 to October 2020 were included in the study. Data on patient demographics, including age, sex, body mass index (BMI), history of corticosteroid intake, alcohol abuse, smoking, and symptomatic joints, were collected from their medical records. All patients underwent WB-MRI and WB-BS before surgery. Results The agreement in the detection of ON by WB-MRI vs the uptake lesions by WB-BS in the hip joints was moderate (κ = 0.584), while that in other joints was low (κ < 0.40). Among the 152 joints with ON detected by WB-MRI, 92 joints (60.5%) were symptomatic, and 60 joints (39.5%) were asymptomatic. Twelve out of the 46 (26.0%) patients had multifocal (three or more distinct anatomical sites) ON. Nonetheless, while WB-BS detected symptomatic ON detected by WB-MRI as uptake lesions in 82.6% (76/92) of the joints, asymptomatic ON detected by WB-MRI was detected as uptake lesions in 21.7% (13/60) of the joints. All patients with multifocal ON had a history of steroid therapy, which was significantly higher than that in patients with oligofocal ON (P = 0.035). The patients with a hematologic disease had multifocal ON at a higher rate (P = 0.015). Conclusions It might be difficult for WB-BS to detect the asymptomatic ON detected by WB-MRI compared to symptomatic ON. Considering the cost, examination time, and radiation exposure, WB-MRI might be useful for evaluating multifocal ON. Larger longitudinal studies evaluating the benefits of WB-MRI for detecting the risk factors for multifocal ON are required.


2019 ◽  
Vol 131 (3) ◽  
pp. 941-948
Author(s):  
Eric S. Nussbaum ◽  
Kevin Kallmes ◽  
Jodi Lowary ◽  
Leslie A. Nussbaum

OBJECTIVEUndiagnosed hepatitis C virus (HCV) and HIV in patients present risks of transmission of bloodborne infections to surgeons intraoperatively. Presurgical screening has been suggested as a protocol to protect surgical staff from these pathogens. The authors sought to determine the incidence of HCV and HIV infection in elective craniotomy patients and analyze the cost-effectiveness of universal and risk factor–specific screening for protection of the surgical staff.METHODSAll patients undergoing elective craniotomy between July 2009 and July 2016 at the National Brain Aneurysm Center who did not refuse screening were included in this study. The authors utilized rapid HCV and HIV tests to screen patients prior to elective surgery, and for each patient who tested positive using the rapid HCV or HIV test, qualitative nucleic acid testing was used to confirm active viral load, and risk factor information was collected. Patients scheduled for nonurgent surgery who were found to be HCV positive were referred to a hepatologist for preoperative treatment. The authors compared risk factors between patients who tested positive on rapid tests, patients with active viral loads, and a random sample of patients who tested negative. The authors also tracked the clinical and material costs of HCV and HIV rapid test screening per patient for cost-effectiveness analysis and calculated the cost per positive result of screening all patients and of screening based on all patient risk factors that differed significantly between patients with and those without positive HCV test results.RESULTSThe study population of patients scheduled for elective craniotomy included 1461 patients, of whom 22 (1.5%) refused the screening. Of the 1439 patients screened, 15 (1.0%) tested positive for HCV using rapid HCV screening; 9 (60%) of these patients had active viral loads. No patient (0%) tested positive for HIV. Seven (77.8%) of the 9 patients with active viral loads underwent treatment with a hepatologist and were referred back for surgery 3–6 months after sustained virologic response to treatment, but the remaining 2 patients (22.2%) required urgent surgery. Of the 9 patients with active viral loads, 1 patient (11%) had a history of both intravenous drug abuse and tattoos. Two of the 9 patients (22%) had tattoos, and 3 (33%) were born within the age-screening bracket (born 1945–1965) recommended by the Centers for Disease Control and Prevention. Rates of smoking differed significantly (p < 0.001) between patients who had active viral loads of HCV and patients who were HCV negative, and rates of smoking (p < 0.001) and IV drug abuse (p < 0.01) differed significantly between patients who were HCV rapid-test positive and those who were HCV negative. Total screening costs (95% CI) per positive result were $3,877.33 ($2,348.05–$11,119.28) for all patients undergoing HCV rapid screening, $226.29 ($93.54–$312.68) for patients with a history of smoking, and $72.00 ($29.15–$619.39) for patients with a history of IV drug abuse.CONCLUSIONSThe rate of undiagnosed HCV infection in this patient population was commensurate with national levels. While the cost of universal screening was considerable, screening patients based on a history of smoking or IV drug abuse would likely reduce costs per positive result greatly and potentially provide cost-effective identification and treatment of HCV patients and surgical staff protection. HIV screening found no infected patients and was not cost-effective.


Author(s):  
S. Korniienko ◽  
I. Korniienko ◽  
D. Kamak ◽  
S. Kaznachey ◽  
O. Zhyrna

Today, the problem of reducing the cost of resources and time during planning and conducting tests remains relevant. This problem is especially acute in qualified testing agencies, where testing prototypes at different stages of the life cycle is the main functional task. Automation of planning processes and optimization of testing processes will significantly reduce such costs and improve the overall quality of testing. The article considers the theoretical issues of forming quantitative plans for testing samples of armaments and military equipment (AME) in obtaining zonal estimates of stochastic parameters and characteristics. The need for zonal estimates arises to confirm the quality of the sample for a given stochastic characteristic in the range from the allowable probabilistic value to the maximum (minimum) possible. The authors propose an approach to obtaining zonal estimates of the parameters of the armament and military equipment test sample, which theoretically meet the requirements of a given accuracy and reliability. The approach is based on the use of a flexible test plan, which is terminated when statistical confirmation of the probabilistic value not worse than specified by the developer is obtained. Ensuring the quality of evaluation is carried out by virtue of the minimum required number of repetitions of the experiment and the balance of the number of successful to the total number of experiments. It is shown that a flexible test plan can significantly reduce the total number of experiments, which will to some extent reduce the resource and time costs of testing samples of armament and military equipment. For the practical application of the approach of obtaining zonal estimates of the AME sample quality, its formalization and algorithmics is required. It is assumed that the developed approach will be implemented in the form of a functional module as а part of the subsystem of automated planning and quality management of AME sample tests.


2020 ◽  
Vol 1 (2) ◽  
pp. 1-27
Author(s):  
Yang Wang ◽  
Xingfu Zou

Motivated by a recent field study [Nat. Commun. 7(2016), 10698] on the impact of fear of large carnivores on the populations in a cascading ecosystem of food chain type with the large carnivores as the top predator, in this paper we propose two model systems in the form of ordinary differential equations to mechanistically explore the cascade of such a fear effect. The models are of the Lotka-Volterra type, one is three imensional and the other four dimensional. The 3-D model only considers the cost of the anti-predation response reflected in the decrease of the production, while the 4-D model considers also the benefit of the response in reducing the predation rate, in addition to the cost by reducing the production. We perform a thorough analysis on the dynamics of the two models. The results reveal that the 3-D model and 4-model demonstrate opposite patterns for trophic cascade in terms of the dependence of population sizes for each species at the co-existence equilibrium on the anti-predation response level parameter, and such a difference is attributed to whether or not there is a benefit for the anti-predation response by the meso-carnivore species.


Author(s):  
Raffaele Cucciniello ◽  
Martino Forino ◽  
Luigi Picariello ◽  
Francesca Coppola ◽  
Luigi Moio ◽  
...  

AbstractAcetaldehyde is a key compound in determining wine color evolution and sensory properties. Major wine metabolites reactive to acetaldehyde are phenolic compounds, mainly flavan-3-ols and anthocyanins. Many studies have been conducted with the purpose of investigating acetaldehyde reactivity in model solutions, but very poor are the reports of its fate in real wines. By means of LC-HRESIMS and UV/Vis HPLC, red and white wines exposed to an excess of acetaldehyde were analyzed with a specific focus on low molecular weight phenolics. The chemical behavior of acetaldehyde turned out to be different in white and red wines. In white wines, it mainly mediated the formation of vinyl-flavan-3-ol derivatives, while in red wines it led to the formation of ethylidene-bridged red pigments. These latter positively enhanced the color properties of red wines. Conversely, in white wines, the formation of compounds, such as xanthylium ions, causing the undesired browning effects were not detected.


1980 ◽  
Vol 25 (92) ◽  
pp. 315-346 ◽  
Author(s):  
Charles Obled ◽  
Walter Good

AbstractDifferent statistical methods have been tested to answer the challenging problem of forecasting avalanche activity. For each approach, the theoretical background is briefly described, and the main advantages and drawbacks are discussed. The first method consists of a simple discriminant analysis applied to a sample of avalanche days against a sample of non-avalanche days. The second approach tries to take into account different types of avalanche phenomena associated with different types of snow and weather situations. It requires the development of an avalanche typology compatible with the available variables, and leads to a two-stage decision model. A given day is first allocated to a weather type, within which the proper model avalanche-non-avalanche is then processed. A third method, a local non-parametric one, consists of drawing, for the day under study and in an appropriate predictor space, its nearest neighbours from the sample file in order to get an estimate of the probability of avalanche occurrence. For each approach, the explanatory variables may be processed directly as quantitative continuous data or as qualitative categorized data. This removes the problems associated with the very asymmetric distribution of half of them, at the cost of a moderate loss of information. As a rule, the methods were calibrated and then applied to the winters 1972–73 and 1973–74 used as a test sample, thus allowing comparison of their respective potentials in operational forecast.


2021 ◽  
Author(s):  
Peter Bjerregaard ◽  
Ingelise Olesen ◽  
Christina Larsen

Abstract Background Amongst the indigenous Greenlandic Inuit, the experience of food insecurity has been attributed to a lack of money to buy enough food of sufficient quality to sustain a family, although a preference for alcohol and tobacco over food has also been cited. The purpose of the article was to compare dietary patterns and expenditure on food, alcoholic beverages and tobacco between survey participants who reported food insecurity and those who did not.Methods Countrywide cross-sectional health survey among 1886 adult Greenlandic Inuit in 2018. Diet was estimated by a food frequency questionnaire. Food insecurity status was based on the household hunger scale. Analyses were carried out by univariate general linear models adjusted for age, sex and social position. ResultsNine percent of the participants reported food insecurity. Food insecurity was unevenly distributed according to age, sex and social position. Food insecure participants more often chose an unhealthy dietary pattern (43% vs. 32%) and they reported a higher energy intake. The food insecure spent the same amount of money on food as other participants but less on nutritious food and more on non-nutritious food. The cost per kJ of the food of the food insecure was lower than that of the food secure (DKK 8.0 and 9.0 per 1000 kJ, respectively). The food insecure participants also spent considerably more on alcohol and tobacco. Conclusions The results suggest that it is not only unemployment and lack of money that creates food insecurity and unhealthy dietary patterns in Greenland but probably also social inequality, lack of resources for planning, prioritising, living one’s daily life and limited knowledge about food. There seems to be at least two population subgroups in Greenland with poverty and substance use, respectively, as the immediate determinants for food insecurity, but behind these causes is a web of underlying social causes. The results are important for the design of interventions against food insecurity and unhealthy dietary patterns.


2021 ◽  
Vol 293 ◽  
pp. 02042
Author(s):  
Jin Bai ◽  
Jingnan Gao ◽  
Wei Ma ◽  
Qingqing Yan ◽  
Xiaodi Wang ◽  
...  

In order to improve the scientificity and efficiency of quality inspection of navigation electronic map, and save the cost of quality inspection, it is necessary to establish the national navigation electronic map quality inspection sample database. In this paper, the construction goal, data acquisition technology process, and database construction method of navigation electronic map quality inspection sample database are described in detail, and the construction content and technical indicators are discussed. The quality test is carried out by combining the in-house verification with the field comparison of the navigation electronic map quality test sample database, and the test results are analyzed and evaluated. The effective application of the sample database in the quality test and evaluation of the internet navigation electronic map in the pilot area is carried out. At the same time, the application of navigation electronic map quality inspection sample database in the research of urban fine management and solid waste recycling economy ecological park planning is prospected.


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