scholarly journals Исследование влияния технологических факторов на неопределенность результатов измерения теплопроводности методом лазерной вспышки

2022 ◽  
Vol 56 (2) ◽  
pp. 173
Author(s):  
Е.С. Макарова ◽  
А.В. Асач ◽  
И.Л. Тхоржевский ◽  
В.Е. Фомин ◽  
А.В. Новотельнова ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Sharp Increase ◽  
Laser Flash ◽  
Comsol Multiphysics ◽  
Flash Method ◽  
Software Environment ◽  
Conductive Materials ◽  
Measurement Results ◽  
Thermally Conductive ◽  
Graphite Coating

The estimation of the deviation in the measurements of thermal conductivity by the laser flash method for materials with different thermal conductivity coefficients, arising due to the presence of a graphite coating on the sample and the small thickness of the sample, is carried out. A computer model of the method was created in the Comsol Multiphysics software environment. For bulk samples with a graphite coating thickness of 20 μm, the deviation is 5.5 %. The thickness of bulk samples does not affect the measurement results. For materials with low thermal conductivity, a sharp increase in the deviation is observed, reaching 60%. For thermally conductive materials, the deviation is 16-18%. For thin samples less than 10 μm thick, the thickness of the graphite coating does not affect the measurement results. The decisive factor is the duration of the laser pulse.

scholarly journals XVI Международная конференция "Термоэлектрики и их применения --- 2018" (ISCTA 2018), Санкт-Петербург, 8-12 октября 2018 г. Влияние неидеальности геометрической формы образца на неопределенность измерений теплопроводности методом лазерной вспышки

2019 ◽  
Vol 53 (6) ◽  
pp. 731
Author(s):  
А.В. Асач ◽  
Г.Н. Исаченко ◽  
А.В. Новотельнова ◽  
В.Е. Фомин ◽  
К.Л. Самусевич ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Measurement Uncertainty ◽  
Conductivity Measurement ◽  
Laser Flash ◽  
Comsol Multiphysics ◽  
Flash Method ◽  
Cylindrical Shape ◽  
Plane Parallel ◽  
Coefficient Of Thermal Conductivity ◽  
Truncated Cylinder

The influence of the geometric shape of the samples on the uncertainty of the coefficient of thermal conductivity measurement of materials by the method of a laser flash has been studied. Using a method of mathematical modeling in the Comsol Multiphysics software, a model that simulates the process of measuring the coefficient of thermal conductivity of samples made of graphite, Mg2Si0.4Sn0.6 and bismuth telluride using a laser flash method has been created. Samples of cylindrical shape with plane-parallel sides and samples in the form of a truncated cylinder, as well as samples in the form of a parallelepiped with a square base, were investigated. It is shown that the measurement uncertainty of samples with plane-parallel sides and sizes up to 12.7 mm, does not exceed 2%. For samples in the form of a truncated cylinder with a diameter of 3 mm and at an angle of ϕ= 1.5°, the measurement uncertainty does not exceed 3%. With an increase in the sample diameter and the ϕ angle, the measurement uncertainty increases significantly.

Study on Thermal Conductivity of Polyetheretherketone/Thermally Conductive Filler Composites

2007 ◽  
Vol 124-126 ◽  
pp. 1079-1082 ◽  
Author(s):  
Sung Ryong Kim ◽  
Dae Hoon Kim ◽  
Dong Ju Kim ◽  
Min Hyung Kim ◽  
Joung Man Park
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Carbon Fiber ◽  
Conductive Filler ◽  
Laser Flash ◽  
Flash Method ◽  
Phase System ◽  
Two Phase ◽  
Nielsen Theory ◽  
Thermally Conductive

Thermal properties of PEEK/silicon carbide(SiC) and PEEK/carbon fiber(CF) were investigated from ambient temperature up to 200°C measured by laser flash method. Thermal conductivity was increased from 0.29W/m-K without filler up to 2.4 W/m-K with at 50 volume % SiC and 3.1W/m-K with 40 volume % carbon fiber. Values from Nielsen theory that predicts thermal conductivity of two-phase system were compared to those obtained from experiment.

Highly thermally conductive UHMWPE/NG composites with the segregated structure and their application for heat spreader

2020 ◽  
pp. 089270572096564
Author(s):  
Xiao Wang ◽  
Hui Lu ◽  
Jun Chen
Keyword(s):  
Thermal Conductivity ◽  
Laser Flash ◽  
Heating Process ◽  
X Ray Diffraction ◽  
Heat Spreader ◽  
Conductive Composites ◽  
Compression Direction ◽  
Thermal Analyzer ◽  
Thermally Conductive ◽  
Plane Direction

In this work, ultra-high molecular weight polyethylene (UHMWPE)/natural flake graphite (NG) polymer composites with the extraordinary high thermal conductivity were prepared by a facile mixed-heating powder method. Morphology observation and X-ray diffraction (XRD) tests revealed that the NG flakes could be more tightly coated on the surface of UHMWPE granules by mixed-heating process and align horizontally (perpendicular to the hot compression direction of composites). Laser flash thermal analyzer (LFA) demonstrated that the thermal conductivity (TC) of composites with 21.6 vol% of NG reached 19.87 W/(m·K) and 10.67 W/(m·K) in the in-plane and through-plane direction, respectively. Application experiment further demonstrated that UHMWPE/NG composites had strong capability to dissipate the heat as heat spreader. The obtained results provided a valuable basis for fabricating high thermal conductive composites which can act as advanced thermal management materials.

Laser flash method for measuring thermal conductivity of liquids. Application to molten salts

1981 ◽  
Vol 20 (4) ◽  
pp. 333-336 ◽  
Author(s):  
Yutaka Tada ◽  
Makoto Harada ◽  
Masataka Tanigaki ◽  
Wataru Eguchi
Keyword(s):  
Thermal Conductivity ◽  
Molten Salts ◽  
Laser Flash ◽  
Laser Flash Method ◽  
Flash Method

scholarly journals Nano liquid metal for the preparation of a thermally conductive and electrically insulating material with high stability

RSC Advances ◽  
2018 ◽  
Vol 8 (29) ◽  
pp. 16232-16242 ◽  
Author(s):  
P. Fan ◽  
Z. Sun ◽  
Y. Wang ◽  
H. Chang ◽  
P. Zhang ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Liquid Metal ◽  
High Stability ◽  
Insulating Material ◽  
Conductive Materials ◽  
Thermally Conductive ◽  
Base Polymer

Compared to liquid metal (LM) microdroplets based thermally conductive materials (micro-LM-THEMs), nano LM-THEMs (nLM-THEMs) presents a more stable electric insulating property even upon stress, achieving ~50-fold thermal conductivity over base polymer.

Thermoelectric Properties of Phase Separated Composite of Ln-Doped SrTiO3 and TiO2 Micro Crystals

2007 ◽  
Vol 1044 ◽  
Author(s):  
Kiyoshi Fuda ◽  
Kenji Murakami ◽  
Shigeaki Sugiyama
Keyword(s):  
Thermal Conductivity ◽  
High Performance ◽  
Fine Particles ◽  
Bulk Material ◽  
Laser Flash ◽  
Flash Method ◽  
Helium Atmosphere ◽  
Low Thermal Conductivity ◽  
Seebeck Coefficients ◽  
Thermal Diffusivities

AbstractIt seems that no satisfactory TE property has been found in n-type oxide bulk materials even though Al-doped ZnO and La-doped SrTiO3 have high thermoelectric (TE) responses. Difficulty in developing high-performance TE materials seems to lie in finding low thermal conductivity in such oxides. The purpose of this study is to find a possibility to make an n-type TE oxide bulk material having low thermal conductivity and excellent TE properties as well. For this purpose, we fabricated and examined a series of composites constructed of TiO2 and Ln-doped SrTiO3 fine crystals. The composites were prepared via two processing steps: (1) precursor oxide preparation by wet processes; (2) sintering by using spark plasma sintering (SPS) apparatus. The microscopic structure was examined by using scanning electron microscope (SEM; HITACHI S-4500 model) attached with an energy dispersive x-ray spectroscopy. The electrical conductivities and the Seebeck coefficients were measured simultaneously using an ULVAC ZEM-1 instrument in helium atmosphere. The thermal diffusivities were measured by a laser flash method in vacuum. The composites obtained here were found to commonly have a mosaic type texture constructed of TiO2 and SrTiO3 fine particles with a typical size of 500 nm. The thermal conductivity values measured for three samples with different contents are ranged between 3 and 4 Wm-1K-1 in the temperature range from room temperature to 800 C. The values are apparently lower than the value for single crystal SrTiO3 samples presented in literature. Taking account the other TE data, e.g. Seebeck coefficient and electrical conductivity, we calculated dimensionless figure of merit, ZT, to be at maximum 0.15 at 800°C.

scholarly journals Determination of the effective thermal conductivity of solid fuels by the laser flash method

2014 ◽  
Vol 35 (3) ◽  
pp. 3-16 ◽  
Author(s):  
Monika Kosowska-Golachowska ◽  
Władysław Gajewski ◽  
Tomasz Musiał
Keyword(s):  
Thermal Conductivity ◽  
Room Temperature ◽  
Laser Flash ◽  
Physical Structure ◽  
Solid Fuels ◽  
Flash Method ◽  
Hard Coal ◽  
Coal Rank ◽  
Dominant Effect

Abstract In this study, a new laser flash system was proposed for the determination of the thermal conductivity of brown coal, hard coal and anthracite. The main objective of the investigation was to determine the effect of coal rank, composition, physical structure and temperature on thermal conductivity. The solid fuels tested were medium conductors of heat whose determined thermal conductivities were in the range of 0.09 to 0.23W/(mK) at room temperature. The thermal conductivity of the solid fuels tested typically increased with the rank of coal and the measurement temperature. The results of this study show that the physical structure of solid fuels and temperature have a dominant effect on the fuels’ thermal conductivity.

scholarly journals The difference in the thermal conductivity of nanofluids measured by different methods and its rationalization

2016 ◽  
Vol 7 ◽  
pp. 2037-2044 ◽  
Author(s):  
Aparna Zagabathuni ◽  
Sudipto Ghosh ◽  
Shyamal Kumar Pabi
Keyword(s):  
Heat Transfer ◽  
Thermal Conductivity ◽  
Laser Flash ◽  
Flash Method ◽  
Transfer Model ◽  
Measuring Methods ◽  
Order Of Magnitude ◽  
Wire Method ◽  
The Difference ◽  
First Time

A suspension of particles below 100 nm in size, usually termed as nanofluid, often shows a notable enhancement in thermal conductivity, when measured by the transient hot-wire method. In contrast, when the conductivity of the same nanofluid is measured by the laser flash method, the enhancement reported is about one order of magnitude lower. This difference has been quantitatively resolved for the first time on the basis of the collision-mediated heat transfer model for nanofluids proposed earlier by our research group. Based on the continuum simulation coupled with stochastic analysis, the present theoretical prediction agrees well with the experimental observations from different measuring methods reported in the literature, and fully accounts for the different results from the two measuring methods mentioned above. This analysis also gives an indication that the nanofluids are unlikely to be effective for heat transfer in microchannels.

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