scholarly journals Strength of lime-strengthened ashand-slag materials study

2021 ◽  
Vol 18 (3) ◽  
pp. 330-341
Author(s):  
A. V. Zvyagintsev ◽  
A. А. Lunev ◽  
R. S. Katsarskiy ◽  
D. A. Shevchenko
Keyword(s):  
Water Resistance ◽  
Clay Soil ◽  
Water Saturation ◽  
Capillary Water ◽  
Pond Ash ◽  
Additional Layer ◽  
Subsequent Determination ◽  
Potential Possibility ◽  
Dry Soil

Introduction. The article studies the strength of hardened ash-soil materials, with different ratios of pond ash, natural clay soil and lime in various proportions when adding a stabilizing additive “Sattelit”.Materials and methods. As part of the study, tests were carried out to determine the maximum density of dry soil and the optimal mixture of ash-soil materials (100% ash-and-slag mixture, 25% ash-and-slag and 75% loam and 50% ash-and-slag and 50% loam), and the subsequent determination of the ultimate strength for uniaxial compression at age seven, twenty-eight and ninety days. The samples were gaining strength in the normal hardening chamber. The samples are placed in a device for capillary water saturation of the samples.Results. As a result of the study, a regularity of the increase in the strength of the soil-ash mixtrues was revealed, depending on the amount of binder, the proportion of materials and the age of the mixture. It was also revealed that with an increase in the dosage of clay soil in the pond ash, the strength of the obtained soil-ash mixtrues sharply increases.Discussion and conclusion. The results of the studies carried out show the potential possibility of using zoological soil materials fortified with lime when installing an additional layer of the base of highways with capital or lightweight pavement on roads in the I-V road-climatic zone. However, additional research is required to determine the frost resistance and water resistance of zoological soil composites reinforced with lime.

scholarly journals STUDY OF VOLUME CHANGES OF PLASTER WITH MINERAL ADDITIVES

2021 ◽  
pp. 6-15
Author(s):  
Artem Іefimenko
Keyword(s):  
Blast Furnace ◽  
Water Resistance ◽  
Water Saturation ◽  
Chemical Additives ◽  
Sodium Lignosulfonate ◽  
Mineral Supplement ◽  
Linear Character ◽  
Pre Treatment ◽  
Mineral Additives

Pre-treatment viznachaє infusion of mineral additives on the natural deformation of gypsum virob. The main reason for the low water resistance of the gypsum viruses is stated. The reason is є a wedge vise. Such a grip breaks out local contacts with crystals. Tsi cause one to dress up in a negative synergistic effect. A wide circle of naukovts is looked around. Fakhivtsi detect the inflow of mineral and chemical additives on the water resistance of the gypsum. Zokrem is honored that the power of materials on the basis of inorganic viscous accumulation of the manifestation of electrostatic interconnection of subordinate electric spheres of structural elements. Before it was confirmed, the value of the biological deformation of the gypsum should be deposited instead of a mineral supplement. Uwagu zoseredzheno on slag blast-furnace granulated chalk.The meta of the statistic was the determination of the degree of determination of the indicator of the uniform lineal deformation of the water saturation (swelling) ew at m / m. Such an indicator can be used with a supplementary indicator of water resistance. In the experimental preliminaries, we used G-10 grade G-10 industrial gypsum, Zaporizhstal blast-furnace granulation slag, and a plasticizing additive - sodium lignosulfonate in a 2% mixture of gipsuFor further development, the skin with three eyes was placed vertically near the vessel. A steel overlay was placed on top of the zrazok. Before the overlay, an indicator of the year-old type was set, fastened to a laboratory stand. The distance was fixed to the cob to show the indicator. The deformation took 3–5 years to develop. In the meantime, having reached the maximum value and mayzhe, the odra was repaired to decrease. At the same time, there will be a projection of the addition of a supplementary indicator of water resistance to the water consumDue to the increase in the amount of slag, the deformation will decrease. The price decrease did not demonstrate a linear character. The character is sickly. This deposit is analogous to that of the deposits of the mines and water from the slag. Minimal deformation is more favorable for a piece gypsum stone with a removable slag W / (H + W) 0.05–0.1 and ponad 0.27. Tse pіdtverzhu podpuschennya about injections at low water resistance gіpsu ozklinuvalnogo inlet water. The wedge-shaped inflow of water is drawn through the contacts between the crystals and particles in the structures of the hypers. The values of the natural deformations of a piece gypsum stone are projected according to the parameters of the water resistance.

Sorption of Se (IV) from aqueous solutions with subsequent determination by X-ray fluorescence analysis

2020 ◽  
Vol 86 (10) ◽  
pp. 5-9
Author(s):  
D. G. Filatova ◽  
A. A. Arkhipenko ◽  
M. A. Statkus ◽  
V. V. Es’kina ◽  
V. B. Baranovskaya ◽  
...  
Keyword(s):  
Inductively Coupled Plasma ◽  
Fluorescence Analysis ◽  
Standard Samples ◽  
Phase Contact Time ◽  
Sorbent Phase ◽  
X Ray ◽  
Fundamental Parameters ◽  
Inductively Coupled ◽  
Subsequent Determination

An approach to sorptive separation of Se (IV) from solutions on a novel S,N-containing sorbent with subsequent determination of the analyte in the sorbent phase by micro-x-ray fluorescence method is presented. The sorbent copolymethylenesulfide-N-alkyl-methylenamine (CMA) was synthesized using «snake in the cage» procedure and proven to be stable in acid solutions. Conditions for quantitative extraction of Se (IV) were determined: sorption in 5 M HCl or 0.05 M HNO3 solutions when heated to 60°C, phase contact time being 1 h. The residual selenium content in the solution was determined by inductively coupled plasma mass spectrometry (ICP-MS) using 82Se isotope. The absence of selenium losses is proved and the mechanism of sorption interaction under specified conditions is proposed. The method of micro-x-ray fluorescence analysis (micro-RFA) with mapping revealed a uniform distribution of selenium on the sorbent surface. The possibility of determining selenium in the sorbent phase by micro-RFA is shown. When comparing the obtained results with the results of calculations by the method of fundamental parameters, it is shown the necessity of using standard samples of sorbates to obtain correct results of RFA determination of selenium in the sorbent phase.

scholarly journals Indirect spectrophotometric determination of gentamicin and vancomycin antibiotics based on their oxidation by potassium permanganate

2006 ◽  
Vol 4 (4) ◽  
pp. 708-722 ◽  
Author(s):  
Akram El-Didamony ◽  
Alaa Amin ◽  
Ahmed Ghoneim ◽  
Ayman Telebany
Keyword(s):  
Acid Medium ◽  
Potassium Permanganate ◽  
Pharmaceutical Formulations ◽  
Molar Absorptivity ◽  
Reaction Conditions ◽  
Subsequent Determination ◽  
Optimum Reaction ◽  
Acid Orange Ii ◽  
Sulphuric Acid Medium

AbstractFour simple, accurate, sensitive and economical procedures (A–D) for the estimation of gentamicin sulphate and vancomycin hydrochloride, both in pure form and in pharmaceutical formulations have been developed. The methods are based on the oxidation of the studied drugs by a known excess of potassium permanganate in sulphuric acid medium and subsequent determination of unreacted oxidant by reacting it with amaranth dye (method A), acid orange II (method B), indigocarmine (method C) and methylene blue (method D), in the same acid medium at a suitable λmax=521, 485, 610 and 664 nm, respectively. The reacted oxidant corresponds to the drug content. Regression analysis of Beer-Lambert plots showed good correlations in the concentration ranges 4–8, 3–8, 4–9 and 5–9 µg ml−1 with gentamicin and 4–8, 1.5–4, 1.5–4 and 3.5–5.5 µg ml−1 with vancomycin for methods A, B, C, and D, respectively. The molar absorptivity, sandell sensitivity, detection and quantification limits were calculated. The stoichiometric ratios for the cited drugs were studied. The optimum reaction conditions and other analytical parameters were evaluated. The influence of the substance commonly employed as excipients with these drugs were studied. The proposed methods were applied to the determination of these drugs in pharmaceutical formulations. The results have demonstrated that the methods are equally accurate and reproducible as the official methods.

scholarly journals Effect of Fertilizer Management on NPKS Leaching Loss from Sandy Loam Soil under Alternate Wetting and Drying Condition

2016 ◽  
Vol 20 (1) ◽  
pp. 59-64
Author(s):  
MN Islam ◽  
MM Rahman ◽  
MJA Mian ◽  
MH Ali
Keyword(s):  
Sandy Loam ◽  
Foliar Spray ◽  
Sandy Loam Soil ◽  
Fertilizer Management ◽  
Wetting And Drying ◽  
Leaching Loss ◽  
Randomized Design ◽  
Loam Soil ◽  
Dry Soil

Leaching loss of nutrients hampers plant growth and contributes to environmental pollution. An experiment was conducted at the net house of Soil Science Department, Bangladesh Agricultural University, Mymensingh during January to May 2009 to find out the leaching loss of N, P, K and S from sandy loam soil. Each pot received 6.67 kg dry soil with an opening at the bottom for collecting leachates. Six treatments were used: T0 = control, T1 = NPKS (120, 25, 60 and 20 kg ha-1), T2 = NPKS (180, 37, 90 and 30 kg ha-1), T3 = NPKS (90, 5, 28 and 17 kg ha-1) + cowdung (2.5 t ha-1), T4 = NPKS (109, 25, 60 and 20 kg ha-1, N as USG) and T5 = as T1 but N applied as foliar spray. Treatments were arranged in a completely randomized design with three replications. Leachates were collected at 15 days interval for determination of NPKS. The total leaching loss of N, P, K and S due to different treatments ranged from 16.00 to 90.21, 0.07 to 0.29, 9.60 to 11.20 and 3.75 to 17.81 kg ha-1, respectively. Application of chemical fertilizer at higher rates resulted in greater loss of nutrients. Integrated fertilizer management with cowdung (T3) minimized such losses. Use of USG also reduced leaching loss of N, P, K and S. The application of cowdung and USG with recommended balanced fertilizer might be useful for minimizing N, P, K and S loss from wetland rice field.Bangladesh Rice j. 2016, 20(1): 59-64

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