scholarly journals Langmuir Probe Diagnostics with Optical Emission Spectrometry (OES) for Coaxial Line Microwave Plasma

2020 ◽  
Vol 10 (22) ◽  
pp. 8117
Author(s):  
Chi Chen ◽  
Wenjie Fu ◽  
Chaoyang Zhang ◽  
Dun Lu ◽  
Meng Han ◽  
...  

The Langmuir probe is a feasible method to measure plasma parameters. However, as the reaction progresses in the discharged plasma, the contamination would be attached to the probe surface and lead to a higher incorrect electron temperature. Then, the electron density cannot be obtained. This paper reports a simple approach to combining the Langmuir probe and the optical emission spectrometry (OES), which can be used to obtain the electron temperature to solve this problem. Even the Langmuir probe is contaminative, the probe current–voltage (I–V) curve with the OES spectra also gives the approximate electron temperature and density. A homemade coaxial line microwave plasma source driven by a 2.45 GHz magnetron was adopted to verify this mothed, and the electron temperature and density in different pressure (40–80 Pa) and microwave power (400–800 W) were measured to verify that it is feasible.

2020 ◽  
Vol 35 (10) ◽  
pp. 2369-2377
Author(s):  
Helmar Wiltsche ◽  
Matthias Wolfgang

The MICAP is a microwave driven plasma source employing nitrogen as the plasma gas. In this work we compare LODs and LOQs obtained in axial viewing with those obtained by ICP-OES and evaluate the effect of air instead of nitrogen as the plasma gas.


2006 ◽  
Vol 8 (4) ◽  
pp. 461-463 ◽  
Author(s):  
Fu Yabo ◽  
Zhang Yuefei ◽  
Chen Qiang ◽  
Zhang Guangqiu ◽  
Gao Yuan ◽  
...  

1995 ◽  
Vol 49 (5) ◽  
pp. 616-622 ◽  
Author(s):  
Rosario Pereiro ◽  
Timothy K. Starn ◽  
Gary M. Hieftje

A new gas-sampling glow discharge (GSGD) is evaluated for the continuous determination of C, F, Cl, and S in molecular gases and organic vapors by optical emission spectrometry, with the use of helium as the discharge gas. Discrete aliquots of the sample are introduced into an exponential dilutor and carried by the support gas through a silica capillary tube and into the glow discharge. Radiation from the plasma source is viewed axially. The effects of plasma operating parameters such as power and pressure are studied, and emission lines of C, F, Cl, and S measured. Analytical performance is evaluated under conditions found to be optimal for each element, as well as under compromise conditions chosen for the simultaneous detection of all four elements. In both cases, detection limits in the low ng/s range, good precision (RSD < 5%), and dynamic ranges of 2–3 decades were observed for the four elements. The utility of this He–GSGD for the determination of elemental ratios in organic compounds is also investigated.


2020 ◽  
Vol 35 (10) ◽  
pp. 2113-2131 ◽  
Author(s):  
Alexandre Müller ◽  
Dirce Pozebon ◽  
Valderi L. Dressler

The N2-sustained microwave-induced plasma optical emission spectrometry (N2-MIP OES) has been increasingly applied for metals and non-metals determination in different fields.


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