scholarly journals Effect of Self-Generated Transfer Layer on the Tribological Properties of PTFE Composites Sliding against Steel

Coatings ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 399 ◽  
Author(s):  
Ting Xie ◽  
Shihao Feng ◽  
Yongheng Qi ◽  
Ailong Cui

Coatings are normally employed to meet some functional requirements. There is a kind of self-generated coating during use, such as the transfer layer during sliding, which may greatly affect the tribological behavior. Although the transfer layer has aroused much attention recently, the formation of the transfer layer closely depends on the service conditions, which need to be further studied. In this paper, the effects of sliding speed, normal load, and duration of wear test on the transfer layer thickness during friction of Ni/PTFE (Polytetrafluoroethylene) composites were experimentally investigated. The formation mechanism of transfer layer and the relationships between tribological properties and transfer layer thickness were analyzed in detail. It was found that the transfer layer thickness increased with increases of sliding speed and normal load; and after a period of wear test, the transfer layer thickness remained stable. The transfer layer thickness correlates linearly with the friction coefficient and wear volume of the PTFE composites. With the increase of the transfer layer thickness, the friction coefficient decreased, while the wear volume increased, which means that a uniform, thin, and stable transfer layer is beneficial for the reduction of friction and wear of the polymeric composites.

2010 ◽  
Vol 654-656 ◽  
pp. 2763-2766 ◽  
Author(s):  
Li Wen Mu ◽  
Xin Feng ◽  
Yi Jun Shi ◽  
Huai Yuan Wang ◽  
Xiao Hua Lu

The tribological properties of polyimide (PI) composites reinforced with graphite or MoS2 sliding in liquid alkali and water as well as dry friction were investigated using a ring-on-ring tester. The results show that the friction coefficient (μ) and wear rate (W) for both graphite/PI and MoS2/PI composites in different liquid mediums are μdry>μwater >μalkali and Wwater>Wdry >Walkali. Results also indicate that the friction coefficient and wear rate of the PI composites filled with different solid lubricants are μMoS2 >μgraphite and W MoS2 >Wgraphite in different liquid mediums. In addition, the hydrophobic inorganic fillers are fit for the reinforcement of polymer-based composites sliding in liquid mediums. It is also concluded from the authors’ work that the wear rate and friction coefficient of polymer-based (such as PI, PTFE) composites in the alkali lubricated conditions is lowest among all the friction conditions. This may be attributed to the ionic hydration in the alkaline solution.


2014 ◽  
Vol 81 (7) ◽  
Author(s):  
N. W. Khun ◽  
H. Zhang ◽  
C. Y. Yue ◽  
J. L. Yang

Self-lubricating and wear resistant epoxy composites were developed via incorporation of wax-containing microcapsules. The effects of microcapsule size and content and working parameters on the tribological properties of epoxy composites were systematically investigated. The incorporation of microcapsules dramatically decreased the friction and wear of the composites from those of the epoxy. The increased microcapsule content or the incorporation of larger microcapsules decreased the friction and wear of the epoxy composites due to the larger amount of released wax lubricant via the rupture of microcapsules during the wear test. The friction of the composites decreased with increased normal load as a result of the promoted wear of the composites and the increased release of the wax lubricant.


2018 ◽  
Vol 188 ◽  
pp. 02007
Author(s):  
Enbiya Türedi

There are plenty of methods for determining the wear volume after a wear test. Due to the geometrical assumptions, some of them could unfortunately lead to mistaken results. It has been shown that a novel method, the direct microscopic measurement, is able to calculate the wear volume on a specimen surface very precisely and accurately [1-2]. It is based on creating a series of line profiles perpendicular to the wear scar. This novel method, however, needs to be characterized in terms of measurement limitations and minimum detectable volume capability. For example, how small or how shallow a wear scar could be calculated or measured with this method, must be determined. For this purpose, it has been prepared a series of wear test specimens exposed to the different amounts of wear in a “pin-on-disk” type test rig. As specimens, two different non-ferrous mold materials, Al bronze alloys, were selected and prepared metallographically. Counterpart materials were inox steel and bearing steel balls with diameter of 6 mm. Normal load was set to 5 N. Test configurations were set to 1, 5, 10 and 100 m of sliding distance values, in turn. Wear tests were conducted in according to ASTM G99 standard. Wear volume results were determined both direct microscopic measurement and also a 3D optical microscope methods. Comparison results showed that the novel method could be successfully used for wear volume calculations even with small amounts of wear volume conditions.


2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Yu Su ◽  
Le Gong ◽  
Dandan Chen

This paper used graphite nanoparticles with the diameter of 35 and 80 nm and LB2000 vegetable based oil to prepare graphite oil-based nanofluids with different volume fractions by two-step method. The tribological properties of graphite nanoparticles as LB2000 vegetable based oil additive were investigated with a pin-on-disk friction and wear tester. Field emission scanning electron microscope (FE-SEM) and energy dispersive spectroscopy (EDS) were used to examine the morphology and the content of some typical elements of wear scar, respectively. Further, the lubrication mechanism of graphite nanoparticles was explored. It was found that graphite nanoparticles as vegetable based oil additive could remarkably improve friction-reducing and antiwear properties of pure oil. With the increase of volume fraction of graphite nanoparticles, the friction coefficient and the wear volume of disk decreased. At the same volume fraction, the smaller particles, the lower friction coefficient and wear volume. The main reason for the improvement in friction-reducing and antiwear properties of vegetable based oil using graphite nanoparticles was that graphite nanoparticles could form a physical deposition film on the friction surfaces.


2014 ◽  
Vol 693 ◽  
pp. 305-310 ◽  
Author(s):  
Eva Labašová

The coefficient of friction for the bronze material (CuZn25Al6) with insert graphite beds and other bronze material (CuSn12) are investigated in this paper. Friction coefficient was investigated experimentally by the testing machine Tribotestor`89 which uses the principle of the ring on ring method. The external fixed bushing was exposed to the normal load of the same size in all tests. Process of load was increased from level 50 N to 600 N during run up 300 s, after the run up the appropriate level of load was held. The internal bushing performed a rotational movement with constant sliding speed. The value of sliding speed was changed individually for every sample (v = 0.2 (0.3, 0.4) m.s-1). The forth test had a rectangular shape of sliding speed with direct current component 0.3 m.s-1 and the amplitude 0.1 m.s-1 period 300 s, the whole test took 2100 s. The obtained results reveal that friction coefficient increase with the increase of sliding speed.


2009 ◽  
Vol 60-61 ◽  
pp. 270-273
Author(s):  
Guang Gui Cheng ◽  
Jian Ning Ding ◽  
Biao Kan ◽  
Zhen Fan

In order to analyze the effect of proceeding on the mechanical and tribological properties of DLC films. Three DLC films samples on single silicon wafers were prepared by CVD method. The changed bias voltages were 300V, 350V, 450V separately. The structure and topography of prepared films were studied by Raman spectroscopy and atomic force microscopy (AFM), respectively. The hardness and elastic modulus together with friction coefficient of DLC films were measured by Tribolab system. According to the Raman spectra, the G and D peak shift to left with the increasing of bias voltage. Nano indent showed that the hardness (H) of the DLC films decreases from 19.63GPa to 18.12GPa with the increasing of bias voltages, and the value of elastic modulus (E) is also behaving the same trend as H from 157.95GPa to 146.95GPa. Friction coefficients of the three samples were measured by nano-scratch method under the constant normal load of 1000uN and the slide velocity of 3 um/sec, the corresponding friction coefficient is 0.0804 for DLC300, 0.0508for DLC350 and 0.0594 for DLC450 separately, which indicates that high hardness materials may not necessarily the perfect frictional material, but compound properties of hardness and elastic modulus


2013 ◽  
Vol 315 ◽  
pp. 951-955 ◽  
Author(s):  
Samion Syahrullail ◽  
Jazair Yahya Wira ◽  
W.B. Wan Nik ◽  
Chiong Ing Tiong

In this paper, the effect of sliding speed on the anti-friction of RBD palm olein was investigated using four-ball tribotester. The speeds were varied from 800 to 1400 rpm. The normal load was set to 40 kg and the test oil was heated up to 75 °C before the experiments. The result showed that palm olein has low friction coefficient compared to additive-free paraffinic mineral oil.


2012 ◽  
Vol 134 (1) ◽  
Author(s):  
G. Y. Li ◽  
Z. Y. Wang ◽  
M. K. Lei

A single high-nitrogen face-centered-cubic (f.c.c.) phase (γN) layer formed on the plasma source nitrided AISI 316 austenitic stainless steel at a nitriding temperature of 450 °C for a nitriding time of 6 h. An approximately 17 μm-thick γN layer has a peak nitrogen concentration of about 20 at. %. Tribological properties of the γN phase layer on a ball-on-disk tribometer against an Si3N4 ceramic counterface under a normal load of 2 and 6 N with a sliding speed of 0.15 to 0.29 m/s were investigated by friction coefficient and specific wear rate measurement. Worn surface morphology and wear debris were characterized using scanning electron microscopy (SEM) and transmission electron microscopy (TEM), respectively. The microhardness of the γN phase layer on the nitrided stainless steel was measured as about 15.1 GPa. The change in the friction coefficient of the γN phase layer on the stainless steel was dependent on the applied normal load, which was associated with that in the specific wear rate. Under a lower normal load of 2 N, the lower specific wear rate of the γN phase layer with a sliding speed of 0.15 m/s was obtained as 2.8 × 10−6 mm3/N m with a friction coefficient of 0.60. Under a higher normal load of 6 N, the lower specific wear rate with a sliding speed of 0.29 m/s was 7.9 × 10−6 mm3/N m with a friction coefficient of 0.80. When the applied load increased from 2 to 6 N, a transition of the wear mechanisms from oxidative to abrasive wear was found, which was derived from the oxidation reaction and the h.c.p. martensite phase transformation of the γN phase during the wear tests, respectively.


2016 ◽  
Vol 1137 ◽  
pp. 24-38
Author(s):  
Jasmaninder Singh Grewal ◽  
Buta Singh Sidhu ◽  
Satya Prakash

In the present work TiAlN coatings were deposited by plasma spray process as titanium aluminium based nitride (Ti, Al)N coatings possess excellent tribological behaviour with respect to metal cutting and polymer forming contacts. Three coatings of TiAlN were deposited on AISI-304 grade boiler steel substrate out of which two were thin nanocoatings deposited at different temperatures of 500°C and 200°C and one conventional coating was deposited by plasma spraying. The as sprayed coatings were characterized with relative to coating thickness, microhardness, porosity and microstructure. The optical microscopy (OM), the XRD analysis and field mission scanning electron microscope (FESEM with EDAX attachment) techniques have been used to identify various phases formed after coating deposited on the surface of the substrate. Subsequently the sliding wear behaviour of uncoated, PVD sprayed nanostructured thin TiAlN coatings deposited at 500°C and 200°C and plasma sprayed conventional coated AISI-304 grade boiler steel were investigated according to ASTM standard G99-03 using pin on disk wear test rig. Cumulative wear volume loss and coefficient of friction, μ were calculated for the coated as well as uncoated specimens for 0.5, 1 and 2 m/sec sliding velocities at a constant normal load of 10 N. The worn out samples were analysed with SEM/EDAX. Wear rates in terms of volumetric loss (mm3/g) for uncoated and coated alloys were compared. The nanostructured TiAlN coatings deposited at 500°C and 200°C has shown minimum wear rate as compared to conventional TiAlN coating and uncoated AISI-304 grade boiler steel. Nanostructured TiAlN coatings were found to be successful in retaining surface contact with the substrate after the wear tests.


2021 ◽  
pp. 1-19
Author(s):  
Temel Savaşkan ◽  
Ali Paşa Hekimoğlu ◽  
Zeki Azakli ◽  
Merve Çaliş

Abstract In order to determine the effect of working conditions on the lubricated wear behavior of Zn-40Al-2Cu-2Si alloy in the as cast and T6 heat-treated states, its tribological properties were studied at different oil flow rates, contact pressures, and sliding speeds in comparison with SAE 660 bronze. It was observed that the friction coefficient, temperature, and wear volume of both materials decrease, but their average surface roughness increase with increasing oil flow rate. As the pressure increased, the friction coefficient and average surface roughness of the experimental materials decreased, but their temperature and wear volume increased. It was also found that the working temperature of these materials increased, but their wear volume showed a decrement and a subsequent increment with increasing sliding speed. In addition, their wear volume and average surface roughness showed opposite changes with the sliding speed. The results of the lubricated friction and wear tests were discussed in terms of the microstructure and mechanical properties of the experimental materials and test conditions. Zn-40Al-2Cu-2Si alloy in both as cast and heat-treated conditions showed lower wear volume and friction coefficient than SAE 660 bronze. This indicates that Zn-40Al-2Cu-2Si alloy can be used to manufacture diesel engine crankshaft journal bearings.


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