scholarly journals In-Situ Reduction of Mo-Based Composite Particles during Laser Powder Bed Fusion

Crystals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 702
Author(s):  
Suxia Guo ◽  
Weiwei Zhou ◽  
Zhenxing Zhou ◽  
Yuchi Fan ◽  
Wei Luo ◽  
...  

Raw powders are processed in water during the freeze-dry pulsated orifice ejection method (FD-POEM), leading to the inclusion of oxygen impurities. This study proposes a strategy for removing the oxygen content and enhancing the mechanical performance of laser powder bed fusion (L-PBF) builds from powders using carbon nanotubes (CNTs) and H2 reduction. Spherical 1.5 wt.% CNT/Mo composite powders with uniform dispersion were fabricated via FD-POEM. The quantity of MoO2 decreased significantly, and a hexagonally structured Mo2C phase was simultaneously formed in the L-PBF build. The Mo2C with network structure was distributed along the boundaries of equiaxed Mo grains, leading to an increased Vickers hardness of the matrix. This study demonstrates the feasibility of fabricating oxygen-free and high-strength refractory parts during L-PBF for ultrahigh-temperature applications.

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 144
Author(s):  
Eslam M. Fayed ◽  
Mohammad Saadati ◽  
Davood Shahriari ◽  
Vladimir Brailovski ◽  
Mohammad Jahazi ◽  
...  

In the present study, multi-objective optimization is employed to develop the optimum heat treatments that can achieve both high-mechanical performance and non-distinctive crystallographic texture of 3D printed Inconel 718 (IN718) fabricated by laser powder bed fusion (LPBF). Heat treatments including homogenization at different soaking times (2, 2.5, 3, 3.5 and 4 h) at 1080 °C, followed by a 1 h solution treatment at 980 °C and the standard aging have been employed. 2.5 h is found to be the homogenization treatment threshold after which there is a depletion of hardening precipitate constituents (Nb and Ti) from the γ-matrix. However, a significant number of columnar grains with a high fraction (37.8%) of low-angle grain boundaries (LAGBs) have still been retained after the 2.5 h homogenization treatment. After a 4 h homogenization treatment, a fully recrystallized IN718 with a high fraction of annealing twins (87.1%) is obtained. 2.5 and 4 h homogenization treatments result in tensile properties exceeding those of the wrought IN718 at both RT and 650 °C. However, considering the texture requirements, it is found that the 4 h homogenization treatment offers the optimum treatment, which can be used to produce IN718 components offering a balanced combination of high mechanical properties and adequate microstructural isotropy.


Materialia ◽  
2021 ◽  
Vol 16 ◽  
pp. 101067
Author(s):  
Holden Hyer ◽  
Le Zhou ◽  
Qingyang Liu ◽  
Dazhong Wu ◽  
Shutao Song ◽  
...  

2017 ◽  
Vol 16 ◽  
pp. 35-48 ◽  
Author(s):  
Giulia Repossini ◽  
Vittorio Laguzza ◽  
Marco Grasso ◽  
Bianca Maria Colosimo

JOM ◽  
2017 ◽  
Vol 69 (12) ◽  
pp. 2725-2730 ◽  
Author(s):  
I. Yadroitsev ◽  
P. Krakhmalev ◽  
I. Yadroitsava

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