scholarly journals Selective Laser Melting of Hydroxyapatite: Perspectives for 3D Printing of Bioresorbable Ceramic Implants

Materials ◽  
2021 ◽  
Vol 14 (18) ◽  
pp. 5425
Author(s):  
Natalia V. Bulina ◽  
Sergey G. Baev ◽  
Svetlana V. Makarova ◽  
Alexander M. Vorobyev ◽  
Alexander I. Titkov ◽  
...  
Keyword(s):  
3D Printing ◽  
Laser Treatment ◽  
Selective Laser Melting ◽  
Tooth Enamel ◽  
Calcium Phosphates ◽  
Scanning Speed ◽  
Powder Layer ◽  
Apatite Crystal ◽  
Layer By Layer ◽  
Laser Melting

Hydroxyapatite, being the major mineral component of tooth enamel and natural bones, is a good candidate for bone tissue engineering applications. One of the promising approaches for manufacturing of three-dimensional objects is selective laser sintering/melting which enables the creation of a dense structure directly during 3D printing by adding material layer-by-layer. The effect of laser irradiation with a wavelength of 10.6 μm on the behavior of mechanochemically synthesized hydroxyapatite under different treatment conditions was studied for the first time in this work. It was shown that, in contrast to laser treatment, the congruent melting is impossible under conditions of a relatively slow rate of heating in a furnace. Depending on the mode of laser treatment, hydroxyapatite can be sintered or melted, or partially decomposed into the more resorbable calcium phosphates. It was found that the congruent selective laser melting of hydroxyapatite can be achieved by treating the dense powder layer with a 0.2 mm laser spot at a power of 4 W and at a scanning speed of 700 mm/s. Melting was shown to be accompanied by the crystallization of a dense monolayer of oxyhydroxyapatite while preserving the initial apatite crystal lattice. The thickness of the melted layer, the presence of micron-sized pores, and the phase composition can be controlled by varying the scanning speed and laser power. This set of parameters permits the use of selective laser melting technology for the production of oxyhydroxyapatite biodegradable implants with acceptable properties by 3D printing.

scholarly journals Numerical Simulation of Moving Heat Flux during Selective Laser Melting of AlSi25 Alloy Powder

Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 877
Author(s):  
Cong Ma ◽  
Xianshun Wei ◽  
Biao Yan ◽  
Pengfei Yan
Keyword(s):  
Numerical Simulation ◽  
Selective Laser Melting ◽  
Process Parameters ◽  
Molten Pool ◽  
Laser Power ◽  
Scanning Speed ◽  
Powder Layer ◽  
Maximum Temperature ◽  
Three Dimensional Model ◽  
Laser Melting

A single-layer three-dimensional model was created to simulate multi-channel scanning of AlSi25 powder in selective laser melting (SLM) by the finite element method. Thermal behaviors of laser power and scanning speed in the procedure of SLM AlSi25 powder were studied. With the increase of laser power, the maximum temperature, size and cooling rate of the molten pool increase, while the scanning speed decreases. For an expected SLM process, a perfect molten pool can be generated using process parameters of laser power of 180 W and a scanning speed of 200 mm/s. The pool is greater than the width of the scanning interval, the depth of the molten pool is close to scan powder layer thickness, the temperature of the molten pool is higher than the melting point temperature of the powder and the parameters of the width and depth are the highest. To confirm the accuracy of the simulation results of forecasting excellent process parameters, the SLM experiment of forming AlSi25 powder was carried out. The surface morphology of the printed sample is intact without holes and defects, and a satisfactory metallurgical bond between adjacent scanning channels and adjacent scanning layers was achieved. Therefore, the development of numerical simulation in this paper provides an effective method to obtain the best process parameters, which can be used as a choice to further improve SLM process parameters. In the future, metallographic technology can also be implemented to obtain the width-to-depth ratio of the SLM sample molten pool, enhancing the connection between experiment and theory.

Numerical Study of Porosity Formation With Implementation of Laser Multiple Reflection in Selective Laser Melting

2019 ◽  
Author(s):  
Bo Cheng ◽  
Charles Tuffile
Keyword(s):  
Selective Laser Melting ◽  
Laser Scanning ◽  
Numerical Study ◽  
Fluid Model ◽  
Melting Process ◽  
Scanning Speed ◽  
Powder Layer ◽  
Cfd Model ◽  
Laser Melting ◽  
Porosity Formation

Abstract In selective laser melting (SLM) process, the build part quality is determined by process parameters such as laser scanning speed and power. The presence of porosity, a major printing defect that significantly affects part performance, may arise in laser melting process due to insufficient or excess energy input. The improvement of build quality heavily depends on fundamental understanding of porosity formation in the SLM process. In this study, the discrete element method (DEM) has been utilized to simulate the creation of a newly deposited powder layer. A computational fluid dynamics (CFD) model was developed to simulate the melting and solidification process of Ti-6Al-4V powders in the SLM process. The thermo-fluid model includes effect of surface tension and recoil pressure as well as laser ray multi-reflection in keyhole. The predictability of the developed CFD model has been validated against literature experimental data. It is found that the collapse of an unstable deep keyhole was responsible for the formation of pores. In addition, higher laser scanning speeds tend to form unstable melt pools, e.g., melt pool break-up.

Effect of processing parameters on forming defects during selective laser melting of AlSi10Mg powder

2020 ◽  
Vol 26 (5) ◽  
pp. 871-879 ◽  
Author(s):  
Haihua Wu ◽  
Junfeng Li ◽  
Zhengying Wei ◽  
Pei Wei
Keyword(s):  
Selective Laser Melting ◽  
Laser Power ◽  
Scanning Speed ◽  
Processing Parameters ◽  
Argon Pressure ◽  
Powder Layer ◽  
Laser Melting ◽  
Content Type ◽  
Scan Speed ◽  
Forming Defects

Purpose To fabricate a selective laser melting (SLM)-processed AlSi10Mg part with almost full density and free of any apparent pores, this study aims to investigate the effect of ambient argon pressure and laser scanning speed on the particles splash during the AlSi10Mg powder bed laser melting. Design/methodology/approach Based on the discrete element method (DEM), a 3D model of random distribution of powder particles was established, and the 3D free surface of SLM forming process was dynamically tracked by the volume of fluid, where a Gaussian laser beam acts as the energy source melting the powder bed. Through the numerical simulation and process experimental research, the effect of the applied laser power and scanning speed on the operating laser melting temperature was studied. Findings The process stability has a fundamental role in the porosity formation, which is process-dependent. The effect of the processing conditions on the process stability and the resultant forming defects were clarified. Research limitations/implications The results shows that the pores were the main defects present in the SLM-processed AlSi10Mg sample, which decreases the densification level of the sample. Practical implications The optimal processing parameters (argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm ) applied during laser melting can improve the quality of selective laser melting of AlSi10Mg, Social implications It can provide a technological support for 3D printing. Originality/value Based on the analysis of the pore and balling formation mechanisms, the optimal processing parameters have been obtained, which were argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm. Then, a near-fully dense sample free of any apparent pores on the cross-sectional microstructure was produced by SLM, wherein the relative density of the as-built samples is larger than 97.5%.

Effects of the Processing Parameters on the Forming Quality of Stainless Steel Parts by Selective Laser Melting

2011 ◽  
Vol 189-193 ◽  
pp. 3668-3671 ◽  
Author(s):  
Qing Song Wei ◽  
Xiao Zhao ◽  
Li Wang ◽  
Rui Di Li ◽  
Jie Liu ◽  
...  
Keyword(s):  
Layer Thickness ◽  
Selective Laser Melting ◽  
Molten Pool ◽  
Laser Power ◽  
Single Layer ◽  
Scanning Speed ◽  
Processing Parameters ◽  
Powder Layer ◽  
Laser Melting

Selective Laser Melting (SLM) can produce high-performance metal parts with complex structures. However, it’s difficult to control the processing parameters, because many factors involves. From the perspective of the molten pool, the study focuses on the effects of processing parameters, including scanning speed, laser power, scanning space, layer thickness, and scanning strategies, on the surface quality, the balling effect, the density of SLM parts, by conducting experiments of single track, single layer and block forming. The results show that the quality of the molten pool is affected by laser power and scanning speed. Scanning drove in the strategy of “jumping and turning”，a smooth surface and a less balling effect will be obtained. The thicker the powder layer is, the lower density will be obtained. The optimal parameters from series of experiments are: laser power of 98W; scanning speed of 90mm/s; scanning space of 0.07mm; layer thickness of 0.1mm; and scanning strategy of “jumping and turning”.

scholarly journals Modelling of Selective Laser Melting Process of Quartz Glass at Elevated Temperatures

2021 ◽  
Vol 248 ◽  
pp. 01001
Author(s):  
M.A. Gridnev ◽  
R.S. Khmyrov ◽  
A.V. Gusarov
Keyword(s):  
Selective Laser Melting ◽  
Quartz Glass ◽  
Elevated Temperatures ◽  
Melting Process ◽  
Coupled Processes ◽  
Powder Layer ◽  
Layer By Layer ◽  
Laser Melting ◽  
Material Quality ◽  
Powder Consolidation

Selective laser melting (SLM) to date is the method of additive manufacturing allowing fabricating products from powder layer-by-layer according to a 3D model. However, when applying this method to fragile materials, parts crack while fabricating due to high temperatures. Quartz glass is a promising material for fabricating products by SLM without cracks due to a low thermal expansion. However, quality of fabricated material differs from the fused cast ones. This article aims to test the method of SLM with preheating to improve the material quality. Experiments on single track formation in SLM are analysed by modelling the coupled processes of heat transfer and powder consolidation in the laser-interaction zone. The mathematical model is validated by the experiments. It is shown that the preheating can improve the material quality and increase the process productivity but overheating may result in undesirable crystallization.

Novel Development of Implant Elements Manufactured through Selective Laser Melting 3D Printing

2021 ◽  
pp. 2001488
Author(s):  
Piotr Kuryło ◽  
Małgorzata Cykowska-Błasik ◽  
Edward Tertel ◽  
Łukasz Pałka ◽  
Piotr Pruszyński ◽  
...  
Keyword(s):  
3D Printing ◽  
Selective Laser Melting ◽  
Laser Melting

Liquation and Crystallization Cracks in Aluminum Alloy AA2024 during Selective Laser Melting

2021 ◽  
Vol 410 ◽  
pp. 203-208
Author(s):  
I.S. Loginova ◽  
N.A. Popov ◽  
A.N. Solonin
Keyword(s):  
Aluminum Alloy ◽  
Selective Laser Melting ◽  
Laser Scanning ◽  
Scanning Speed ◽  
Melting Zone ◽  
Alloying Elements ◽  
Laser Melting ◽  
Laser Scanning Speed ◽  
Positive Effect

In this work we studied the microstructure and microhardness of standard AA2024 alloy and AA2024 alloy with the addition of 1.5% Y after pulsed laser melting (PLM) and selective laser melting (SLM). The SLM process was carried out with a 300 W power and 0.1 m/s laser scanning speed. A dispersed microstructure without the formation of crystallization cracks and low liquation of alloying elements was obtained in Y-modified AA2024 aluminum alloy. Eutectic Al3Y and Al8Cu4Y phases were detected in Y-modified AA2024 aluminum alloy. It is led to a decrease in the formation of crystallization cracks The uniform distribution of alloying elements in the yttrium-modified alloy had a positive effect on the quality of the laser melting zone (LMZ) and microhardness.

scholarly journals Fracture Toughness of Hybrid Components with Selective Laser Melting 18Ni300 Steel Parts

2018 ◽  
Vol 8 (10) ◽  
pp. 1879 ◽  
Author(s):  
Luis Santos ◽  
Joel de Jesus ◽  
José Ferreira ◽  
José Costa ◽  
Carlos Capela
Keyword(s):  
Fracture Toughness ◽  
Selective Laser Melting ◽  
Compact Tension ◽  
Powder Materials ◽  
Layer By Layer ◽  
Laser Melting ◽  
Conventional Steel ◽  
Scan Rate ◽  
Aisi H13 ◽  
3D Printed

Selective Laser Melting (SLM) is currently one of the more advanced manufacturing and prototyping processes, allowing the 3D-printing of complex parts through the layer-by-layer deposition of powder materials melted by laser. This work concerns the study of the fracture toughness of maraging AISI 18Ni300 steel implants by SLM built over two different conventional steels, AISI H13 and AISI 420, ranging the scan rate between 200 mm/s and 400 mm/s. The SLM process creates an interface zone between the conventional steel and the laser melted implant in the final form of compact tension (CT) samples, where the hardness is higher than the 3D-printed material but lower than the conventional steel. Both fully 3D-printed series and 3D-printed implants series produced at 200 mm/s of scan rate showed higher fracture toughness than the other series built at 400 mm/s of scan rate due to a lower level of internal defects. An inexpressive variation of fracture toughness was observed between the implanted series with the same parameters. The crack growth path for all samples occurred in the limit of interface/3D-printed material zone and occurred between laser melted layers.

Track evolution and surface characteristics of selective laser melting Ti6Al4V

2018 ◽  
Vol 24 (9) ◽  
pp. 1554-1562 ◽  
Author(s):  
Luo Zhang ◽  
Haihong Zhu ◽  
Jiahe Liu ◽  
Xiaoyan Zeng
Keyword(s):  
Surface Morphology ◽  
Selective Laser Melting ◽  
Surface Characteristics ◽  
Scanning Speed ◽  
Bulk Sample ◽  
Three Dimension ◽  
Single Track ◽  
Heat Accumulation ◽  
Laser Melting ◽  
Content Type

Purpose The purpose of this paper is to investigate the track evolution and surface characteristics of selective laser melting Ti6Al4V. Design/methodology/approach In the present paper, Ti6Al4V single-track, multi-track and bulk sample were formed at different scanning speed by selective laser melting (SLM). Then, the surface morphology, three-dimension profile and surface roughness were evaluated. The width of the single and multi-track was measured and compared. Findings The results showed that the heat accumulation played a great role on the evolution of tracks and surface characteristics from single-track to multi-track and to bulk. The surface morphology of the subsequent tracks became more regular when the single-track was irregular at the same high scanning speed. The width of last track Wn was always larger than that of the first track W1. The Ra of the top of the bulk increased with the increase of the scanning speed, this trend was as same as the Ra of the single-track, but the trend of Ra of the side was opposite. Originality/value The effect of heat accumulation on the track evolution and surface characteristics is obtained. The results can help to derive a smooth surface with a regular and continuous track in SLM.

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