scholarly journals Alkylation of in situ generated fluorinated alkoxides: novel synthesis of partially fluorinated ethers

ARKIVOC ◽  
2003 ◽  
Vol 2003 (3) ◽  
pp. 104-119 ◽  
Author(s):  
G. K. Surya Prakash ◽  
Jinbo Hu ◽  
George A. Olah
Synlett ◽  
2018 ◽  
Vol 29 (07) ◽  
pp. 912-917 ◽  
Author(s):  
Parviz Ranjbar ◽  
Narjes Rezaei ◽  
Ehsan Sheikhi

A metal-free oxidative C(sp3)–N coupling process has been developed for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones. The reaction between primary amines, isatoic anhydride, and benzylic alcohols in the presence of HBr in DMSO at 80 °C affords 2,3-dihydroquinazolin-4(1H)-ones in excellent yields. Under these reaction conditions, benzylic alcohols react with in situ generated bromodimethylsulfonium bromide to form alkoxysulfonium intermediates. These intermediates undergo an oxidative cyclization reaction with primary amines and isatoic anhydride to produce the title products.


2015 ◽  
Vol 3 (32) ◽  
pp. 16513-16519 ◽  
Author(s):  
Liyuan Zhang ◽  
Hui Huang ◽  
Hailin Yin ◽  
Yang Xia ◽  
Jianmin Luo ◽  
...  

A novel synthesis of graphene–sulfur composites is designed by electrolytic exfoliation of graphite coupled with in situ electrodeposition of sulfur.


2007 ◽  
Vol 48 (7) ◽  
pp. 1281-1285 ◽  
Author(s):  
Ramendra Pratap ◽  
Abhijeet Deb Roy ◽  
Raja Roy ◽  
Vishnu Ji Ram
Keyword(s):  

ChemInform ◽  
2007 ◽  
Vol 38 (21) ◽  
Author(s):  
Ramendra Pratap ◽  
Abhijeet Dep Roy ◽  
Raja Roy ◽  
Vishnu Ji Ram
Keyword(s):  

Sign in / Sign up

Export Citation Format

Share Document