Deposition Tantalum Nitride on LDX 2101 Duplex Stainless Steel by Reactive Sputtering in Biomedical Applications

2022 ◽  
Vol 113 (2) ◽  
pp. 75-85
Author(s):  
J.M.S. Al-Murshdy

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Author(s):  
A. Redjaïmia ◽  
J.P. Morniroli ◽  
G. Metauer ◽  
M. Gantois

2D and especially 3D symmetry information required to determine the crystal structure of four intermetallic phases present as small particles (average size in the range 100-500nm) in a Fe.22Cr.5Ni.3Mo.0.03C duplex stainless steel is not present in most Convergent Beam Electron Diffraction (CBED) patterns. Nevertheless it is possible to deduce many crystal features and to identify unambiguously these four phases by means of microdiffraction patterns obtained with a nearly parallel beam focused on a very small area (50-100nm).From examinations of the whole pattern reduced (RS) and full (FS) symmetries the 7 crystal systems and the 11 Laue classes are distinguished without ambiguity (1). By considering the shifts and the periodicity differences between the ZOLZ and FOLZ reflection nets on specific Zone Axis Patterns (ZAP) which depend on the crystal system, the centering type of the cell and the glide planes are simultaneously identified (2). This identification is easily done by comparisons with the corresponding simulated diffraction patterns.


Author(s):  
Edgard Silva ◽  
Francisco Eduardo Mendes da Silva ◽  
Amanda Medeiros ◽  
Ana Paula Alves Pacheco ◽  
IZAURA VIEGAS ◽  
...  

2018 ◽  
Vol 60 (6) ◽  
pp. 577-582
Author(s):  
Sergii Krasnorutskyi ◽  
Christian Kipp ◽  
Jonas Hensel ◽  
Peter Kaestner ◽  
Sven Hartwig ◽  
...  

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