Dynamic Behavior of Air Void during the Discharge of Cohesive Powder in a Hopper Using a Rubber Air Spring

An unstable discharge rate occurs during dry fine powder discharge from a hopper because of the significant two-phase solid/gas interactions that occur in powder flows. In addition, the air bubble phenomenon may occur in a silo during fine powder discharge. In this study, we conducted experiments using a semi-conical dual-structure hopper, and examined the effects on the hopper internal flow structure, cavity fluid pressure, pressure inside the airtight cavity section, and the powder discharge rate when changes are made in the position of the supplied air injection port and the solenoid valve open/close timing. From the experimental results, it was confirmed that an appropriate pressure supply port position exists, and the change in expansion/contraction of the flexible container due to air vibration is determined by the balance between the amount of air inserted and the amount of air discharged, and does not affect the presence or absence of powder so much. Furthermore, as the pressure value in the airtight void is directly related to the change in the expansion and contraction of the flexible container, the maximum amplitude value of the pressure in the airtight void can be kept high and constant at the time of opening and closing the solenoid valve.

The mixing of cohesive and flowable powder materials using a common laboratory powder mixer

This study presented the homogeneity obtained when mixing cohesive and flowable powder materials using a laboratory powder mixer. The mixing process parameters studied were the mixing time and the mixer rotational speed (20 rpm, 40 rpm and 60 rpm) at the different ratios (95%: 5%, 50%: 50% and 5%: 95%) of the cohesive cocoa and flowable mannitol powder materials. The homogeneity sampled at the powder bed surface showed that only at the highest rotational speed of 60 rpm used in this work yield acceptable homogeneity at the two extremes of the powder mass ratios; 95%: 5% and 5%: 95% of mannitol: cocoa for some of the locations on the powder bed surface, especially near the wall of the mixer. Other combinations of the experimental conditions did not yield acceptable mixture homogeneity. These results showed the difficulties in obtaining a homogeneous powder mix when mixing cohesive powder materials, especially in academic teaching and research laboratories using a simple powder mixer apparatus.

Conformal Coating of Powder by Initiated Chemical Vapor Deposition on Vibrating Substrate

Encapsulation of pharmaceutical powders within thin functional polymer films is a powerful and versatile method to modify drug release properties. Conformal coating over the complete surface of the particle via chemical vapor deposition techniques is a challenging task due to the compromised gas–solid contact. In this study, an initiated chemical vapor deposition reactor was adapted with speakers and vibration of particles was achieved by playing AC/DC’s song “Thunderstruck” to overcome the above-mentioned problem. To show the possibilities of this method, two types of powder of very different particle sizes were chosen, magnesium citrate (3–10 µm, cohesive powder) and aspirin (100–500 µm, good flowability), and coated with poly-ethylene-glycol-di-methacrylate. The release curve of coated magnesium citrate powder was retarded compared to uncoated powder. However, neither changing the thickness coating nor vibrating the powder during the deposition had influence on the release parameters, indicating, that cohesive powders cannot be coated conformally. The release of coated aspirin was as well retarded as compared to uncoated aspirin, especially in the case of the powder that vibrated during deposition. We attribute the enhancement of the retarded release to the formation of a conformal coating on the aspirin powder.

Maltodextrin on the flow properties of green coconut (Cocos nucifera L.) pulp powder

ABSTRACT The study of the flow properties and particle surfaces of a food powder is essential for predicting its behaviour during processing and commercialization. The objective of this work was to determine the powder flow properties of lyophilized green coconut pulp with different concentrations of maltodextrin. Samples containing 0, 5, 10 and 15% (m/m) maltodextrin were lyophilized, and the flow index (FI), wall friction angles and densities were determined. The microstructure of the powders was evaluated by scanning electron microscopy (SEM). The samples containing 0 and 5% maltodextrin showed 1.87 FI, classifying them as very cohesive powders, and those containing 10 and 15% cohesive powder showed 2.12 and 2.43 FI, respectively. The powder densities varied from 138.6 to 287.6 kg/m3, and the wall friction angle varied from 15.8 to 39.8°. The powder particles presented irregular shapes and rough surfaces, especially in powders containing 0, 5 and 10% maltodextrin. The powder containing 15% had smoother and less agglomerated surfaces. An increase in the amount of maltodextrin added to the pulp made the particles smoother and denser and improved the fluidity of the powder.