In this research, an alloy with a nanostructure was prepared using a metallurgical technique. To prepare an ideal alloy, three nanoscale powders were used (70 percent Ni, 25 percent Cu, and 5 percent V). The dried alloy was stored under 8 Tons of cold pressing at 80°C for 30 minutes. After that, a surface treatment of the prepared alloys with different laser energies (0, 200, 260, 300) mJ was carried out with a pulse time (10 seconds) at a distance of (100 cm). and hardness (Rockwell method) is studied. By immersing samples in a solution (3.5 percent NaCl) for different periods (3, 5, 7, 9, 11) days, the effect of laser surface treatment on the corrosion resistance of the alloy was investigated. Results show that porosity, water absorption ratio decreases after laser surface treatment with rising hardness values. Additionally, the wear resistance decreases as laser energy increases. Atomic force microscope images show that grain sizes increase as laser energy increases, and by increasing the laser energy, the surface of the nanoparticles is more homogeneous. Easy architecture and high nanostructure alloy consistency play a key role in improving the mechanical and physical properties.