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Author(s):  
A. P. Nechiporenko ◽  
O. S. Vezo ◽  
U. Yu. Nechiporenko ◽  
L. V. Plotnikova ◽  
V. E. Sitnikova ◽  
...  

115 samples of honey of various botanical types, geographical origin and harvest year (2019– 2021) were analysed using attenuated total reflection infrared spectroscopy of impaired total reflection, refractometry and biochemical analysis. Initial honey samples in liquid and crystallised states were investigated. Crystalline D-glucopyranose (glucose), D-fructopyranose (fructose), their 40% solutions and invert sugar were used as auxiliary substances. Biochemical analysis was used to determine the glucose content in honey samples. Based on the obtained data, a relationship between the results of biochemical analysis and refractometry (refractive index, the content of invert sugars, humidity) was established. We deduced equations that allow the content of glucose and fructose in honey to be evaluated by the refractive index. Studying honey by IR spectroscopy showed that all investigated samples, regardless of the botanical and geographical origins, can be classified into three groups dominated by: I – glucose, II – fructose and III – mixed, with a close content of two monosaccharides. This allowed the bands characteristic of α- and β-pyranose forms of glucose and fructose to be identified, as well as the nature of their changes depending on the ratio of both monosaccharides in honey as a result of their crystallisation to be assessed. It is noted that the ratio of monosaccharides determines not only the stability of the liquid crystal structure and crystallisation rate in honey but also their optical, biochemical and nutritional properties, which are important for the preferred use of honey in medical and pharmacopoeial practice, dietetics and cosmetology.


Foods ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 104
Author(s):  
Carina Pedrosa Costa ◽  
Samuel Patinha ◽  
Alisa Rudnitskaya ◽  
Sónia A. O. Santos ◽  
Armando J. D. Silvestre ◽  
...  

Improvement of dietary and ecological biodiversity, namely by exploring autochthonous varieties, is a key point to the construction of a more sustainable food system and planetary health. However, the environmental sustainability continues to face huge challenges, reflecting the importance of achieving a better understanding about the functional role of biodiversity in ecosystems. Thus, the main objective of this research is to contribute to the sustainable valorization of Sambucus nigra L. berries through a comprehensive approach to evaluate the effects of elderberry’s cultivar, harvest year, and plantation field on the physicochemical berry composition. Moreover, the nutritional value of elderberry juice and respective dried pomace was determined. This complementary information is of huge utility for the rational and, as much as possible, integral use of elderberries. The harvest year, followed by field and the interaction of harvest × field, accounted for the highest impact on the berry’s physicochemical parameters, indicating the importance of the combined impact of the macro- and mesoclimate conditions on plant metabolism. Elderberry juice and dried pomace are a good source of carbohydrates (ca. 12 and 82%, respectively) and have low amounts of fat (≤2.5%), making them low-energy foods. Dried pomace may also represent a potential alternative source of vegetal protein (ca. 6%).


2021 ◽  
pp. 004051752110620
Author(s):  
Yu Li ◽  
Jiajia Fu ◽  
Hongbo Wang ◽  
Weidong Gao

Bamboo fiber bundles were successfully extracted from bamboo culms using water-retting, taking advantage of enzymes secreted by microorganisms in the retting liquid. The harvest year and place of origin of the bamboo and the source of water impacted the products of the retting process. One-month-old bamboo was decomposed completely, whereas the one-year-old sample was hardly changed after 24-day retting. Moisture regain and crystallinity varied with the different origins of the bamboo. However, all samples resulted in similar chemical structures and thermal properties. The best operational conditions for water-retting were 3-month-old bamboo from Wuxi incubated in deionized water. Enzyme activities, including cellulase, xylanase, pectinase, and ligninolytic enzymes (lignin peroxidase, manganese peroxidase, and laccase) were monitored during a 24-day retting. Manganese peroxidase was the primary enzyme used to degrade lignin, resulting in absorbance at 294 nm of UV-Vis spectra. In addition, xylanase played a leading role in hydrolyzing hemicellulose, which was consistent with the change in reducing sugar yield. In addition, variations in dissolved oxygen and pH values were also recorded, indicating the changes in bacterial strains and the enzymatic system. The wastewater from bamboo retting showed good biodegradability but a lack of nitrogen and phosphorus. Overall, a manganese peroxidase–xylanase combined enzyme-retting treatment would offer a more environmentally friendly approach for extracting bamboo fibers.


Agronomy ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 2227
Author(s):  
Oluwakorede Olugbenle ◽  
Priscila Pinto ◽  
Valentin D. Picasso

Intermediate wheatgrass (IWG) is a new perennial dual-use crop for grain and forage with growing interest among farmers. Intercropping IWG with red clover may increase yield and nutritive value through nitrogen transfer. IWG and red clover planting timing can affect grain and forage yield, and there has not been previous research on this management practice. At two locations (Arlington and Lancaster, WI, USA) a factorial experiment was established two years with two factors: (1) IWG planting date (August through October, and April) and (2) red clover planting season (in the fall with IWG or frost seeded in the next spring). Yield data were collected for two subsequent years. Grain yield was maximized at 515 kg ha−1 and 423 kg ha−1 at Arlington and Lancaster when planted by 26 August and 13 September, respectively. Planting date influenced grain yields in the first harvest year but not in the second. Seeding red clover in the spring increased IWG and red clover biomass compared to seeding it in the fall. In Wisconsin, planting IWG by early September at the latest and planting red clover in the spring is recommended to maximize grain yield.


2021 ◽  
Vol 99 (Supplement_3) ◽  
pp. 36-37
Author(s):  
Paige N Gott ◽  
Erin Schwandt ◽  
Shelby M Ramirez ◽  
Ursula Hofstetter ◽  
Raj Murugesan

Abstract Mycotoxins are fungal metabolites that limit animal health and performance through various negative effects including reduced feed intake, diarrhea, and compromised immune function. These toxic metabolites have been detected in a broad range of feedstuffs worldwide. This study investigated mycotoxin occurrence and contamination levels in U.S. corn grain samples marked as 2020 harvest year and corn by-product feed samples submitted since October 2020. Samples were screened via LC-MS/MS for six major mycotoxin groups including: aflatoxins, type A trichothecenes, type B trichothecenes (B-Trich), fumonisins (FUM), zearalenone (ZEN), and ochratoxin A. Results from samples that were above the limit of detection for each respective mycotoxin group were analyzed using the GLIMMIX procedure (SAS 9.4, Cary, NC) to test the effect of harvest year on mean contamination level. Results are presented in Table 1. Occurrence levels of B-Trich, ZEN, and FUM in 2020 corn grain are numerically lower than those from 2019. Mean B-Trich level (parts per billion, ppb) for corn grain samples harvested in 2020 was similar to 2019 crop year. Contamination levels of FUM and ZEN were similar for 2020 crop as compared to prior harvest years. Mycotoxin occurrence in corn by-product feeds continued to be high at 99, 85, and 95% for B-Trich, ZEN, and FUM, respectively. Mean B-Trich and ZEN levels in 2020 corn by-products were similar to respective contamination levels in 2018, but were lower than 2019 samples. Mean FUM contamination in corn by-products has been similar across reported years. Preliminary results of the 2020 corn grain survey indicate mean mycotoxin contamination levels are similar to those observed the past two crop years while levels of B-Trich and ZEN in corn by-product feeds are reduced from 2019. Corn-based feed ingredients may present challenges to producers due to the presence of mycotoxin contamination, therefore, continued monitoring is warranted.


2021 ◽  
Vol 99 (Supplement_3) ◽  
pp. 183-184
Author(s):  
Erin Schwandt ◽  
Paige N Gott ◽  
Shelby M Ramirez ◽  
Ursula Hofstetter ◽  
Raj Murugesan

Abstract Mycotoxins are harmful secondary fungal metabolites which limit animal health and performance through various negative effects such as reduced feed intake, diarrhea, and compromised immune and reproductive function. These metabolites are found in a variety of feedstuffs worldwide. This study monitored mycotoxin occurrence and contamination levels in fresh pasture grasses and harvested dry hay from across the US. Samples were screened for six major mycotoxin groups: aflatoxins, type A trichothecenes (A-Trich), type B trichothecenes (B-Trich), fumonisins (FUM), zearalenone (ZEN), and ochratoxin A via LC-MS/MS. Samples that were above the limit of detection for each mycotoxin group were analyzed using the GLIMMIX procedure of SAS (SAS 9.4, Cary, NC) to test the effect of harvest year on average contamination level. Results are presented in Table 1. Zearalenone and B-Trich contamination prevalence for fresh grass samples was lower in 2020 compared to the previous two years. A-Trich tested positive in 34% of samples which was greater in 2020 compared to 2018 and 2019. Mean concentration levels (parts per billion, ppb) for B-Trich, ZEN, A-Trich were not different in 2020 compared to the previous two years. Prevalence of mycotoxin contamination for dry harvested hay samples for B-Trich and ZEN decreased in 2020 compared to the previous two years, but 64 and 28% of samples tested positive, respectively. A-Trich prevalence was greater than the last two years and resulted in 17% of samples testing positive compared to 0 and 6% in 2018 and 2019, respectively. Mean B-Trich levels in 2020 were similar to levels seen in 2018 and lower than 2019 (P = 0.005). Mean ZEN and A-Trich concentration levels averaged 1,612 ppb and 796 ppb, respectively. Mycotoxin analysis of pasture grasses and harvested hay forages is warranted to identify potential sources of mycotoxin contamination in ruminant diets.


2021 ◽  
Vol 99 (Supplement_3) ◽  
pp. 37-38
Author(s):  
Paige N Gott ◽  
Erin Schwandt ◽  
Shelby M Ramirez ◽  
Ursula Hofstetter ◽  
Raj Murugesan

Abstract Mycotoxins are fungal metabolites which have been identified in many feed ingredients and ruminants have an increased risk of exposure due to the complex nature of their diets. Despite varying degrees of natural detoxification in the rumen, cattle health, productivity, and reproduction can be compromised by mycotoxins. This study investigated mycotoxin occurrence and contamination levels in 2020 U.S. corn silage and dairy total mixed ration (TMR) samples. Samples were screened via LC-MS/MS for six major mycotoxin groups including: aflatoxins, type A trichothecenes (A-Trich), type B trichothecenes (B-Trich), fumonisins (FUM), zearalenone (ZEN), and ochratoxin A. Information was collected with each submission including state of origin and whether or not clinical health or performance concerns were present. Contamination levels were analyzed using the GLIMMIX procedure (SAS 9.4, Cary, NC) to investigate the interaction of clinical concern (yes/no) and harvest year. No interaction was statistically significant for each of the toxin groups, so main effects of harvest year are presented in Table 1. Type B trichothecenes have been identified most frequently in 2020 corn silage. Although not often detected, A-Trich occurrence has increased ten percentage points from 2019 crop year. Among 236 TMR samples analyzed, B-Trich have been detected in a high percentage of samples. Mean contamination levels (parts per billion, ppb) are presented on a dry matter basis and within each data set were similar in 2020 compared to 2019 for respective toxin groups. Preliminary survey results indicate B-Trich occur frequently in both U.S. corn silage and TMR samples. Despite less frequent detection, other mycotoxin groups do occur including ZEN, FUM, and A-Trich, so the potential risk from toxin interactions due to co-contamination should be considered.


AppliedChem ◽  
2021 ◽  
Vol 1 (1) ◽  
pp. 62-74
Author(s):  
Lydia Valasi ◽  
Christos S. Pappas

Food quality is a topic of utmost importance as more and more emphasis is placed on quality rather than quantity of products. Previous studies have pointed out the interaction of quality with the harvest year. In this study, 22 Pistacia vera (Greek ‘Aegina’ variety) samples (11 from 2017 and 11 from 2018) were differentiated using Fourier transform infrared spectroscopy (FTIR) and (a) diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) and (b) KBr/sample disk techniques. In both years, the pistachios trees’ growing followed standard cultivation methods and similar agronomic conditions. Two chemometric models were developed using partial least squares-discrimination analysis (PLS-DA). DRIFTS proved unable to statistically differentiate the samples (R2 = 0.96266, Q2 = 0.63152). On the contrary, the disk technique completely differentiated the pistachio samples (R2 = 0.99705, Q2 = 0.97719). The 1720–1800 cm−1 region mostly contributed to the discrimination. The disk-FTIR chemometric model is fast, robust, economical, and environmentally friendly for determining pistachio matrix quality.


2021 ◽  
Vol 9 (3) ◽  
pp. 303
Author(s):  
Edilza Martins da Silva ◽  
Priscila Pigatto Gasparin ◽  
Alex Paludo ◽  
Willyan Ronaldo Becker ◽  
Luciana Pagliosa Carvalho Guedes ◽  
...  

Climate change can affect the development of soybean cultivation, impacting your productivity. Thus, agrometeorological information is essential in order to improve productivity strategies. The objective of the paper was to analyze the influence and occurrence of seasonality of the following agrometeorological variables on soybean productivity: mean air temperature [TMean] (ºC), accumulated rainfall value [Rain] (mm), global solar radiation [Sr] (MJ m-2 day-1), and potential evapotranspiration [ETp] (mm), in ten-day variations of the the maximum vegetative development date (MVDD), in the 2011/2012 and 2013/2014 harvest years in the state of Paraná. The study was based on spatial distribution of variables, using univariate and bivariate Global Moran’s Indexes, and multivariate clustering analysis. To verify seasonality in the time distribution of the agrometeorological variables in the ten-day variations close to soybean MVDD, we used the circular statistics, through the mean vector length (R). Result it was identified regions of the state that have higher and lower rainfall and seasonality, also have higher and lowest productivity, respectively. That the variation in soybean productivity between harvest years was correlated with the agrometeorological variables, and rainfall volume is an important factor in productivity. The other agrometeorological variables occurred uniformly, especially in 2011/2012 harvest year, in the Northwest, Central-northern and West mesoregions. Furthermore, there was clustering of regions with similar spatial distribution of the evapotranspiration and rainfall variables in 2aDMDV2d in the 2011/2012 and 2013/2014 harvest year, showed the same spatial distribution of the agrometeorological variables and the productivity variable.


2021 ◽  
Author(s):  
Yi Zheng ◽  
Ana Cláudia dos Santos Luciano ◽  
Jie Dong ◽  
Wenping Yuan

Abstract. Sugarcane is the most important source of sugar, and its cultivation area has undergone rapid expansion, replacing other crops, pastures, and forests. Brazil is the world's largest sugarcane producer and contributed to approximately 38.6 % of the world's total production in 2019. Sugarcane in Brazil can be harvested from April to December in south-central area and from September to April in northeast area. The flexible phenology and harvest conditions of sugarcane in Brazil make it difficult to identify the harvest area at state to country scales. In this study, we developed a phenology-based method to identify the harvest area of sugarcane in Brazil by incorporating the multiple phenology conditions into a time-weighted dynamic time warping method (TWDTW). Then, we produced annual 30-m spatial resolution sugarcane harvest maps (2016–2019) for 14 states in Brazil (over 98 % of the harvest area) based on the proposed method by using Landsat-7/8 and Sentinel-2 optical data. The proposed method performed well in identifying sugarcane harvest area with limited training sample data. Validations for the 2018 harvest year displayed high accuracy, with user's, producer's, and overall accuracies of 97.00 %, 88.08 %, and 92.99 % in Brazil, respectively. In addition, the identified harvest area of sugarcane exhibited good correlations with the agricultural statistical data provided by the Brazilian Institute of Geography and Statistics (IBGE) at the municipality, microregion, and mesoregion levels. The 30-m Brazil sugarcane harvest maps can be obtained at https://doi.org/10.6084/m9.figshare.14213909 (Zheng et al., 2021).


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