scholarly journals Investigations for In-house prepared Biocompatible Feed Stock Filament of Fused Deposition Modelling: A Process Capability study

2019 ◽  
Vol 48 (1) ◽  
pp. 18-23
Author(s):  
Nishant Ranjan ◽  
Rupinder Singh ◽  
IPS Ahuja
Keyword(s):  
Control Charts ◽  
Low Cost ◽  
Process Capability ◽  
Dimensional Accuracy ◽  
Fused Deposition Modelling ◽  
Twin Screw Extrusion ◽  
Fused Deposition ◽  
Feed Stock ◽  
Screw Extrusion ◽  
Twin Screw

Fused deposition modelling (FDM) is one of the low cost additive manufacturing (AM) process. The feed stock filament of FDM is the only consumable in the process and by preparing (in-house) bio compatible feed stock filament the application domain can be increased. Some studies have reported the use of twin screw extrusion (TSE) process for preparation of bio compatible feed stock filament (comprising of polyvinyl chloride (PVC) and polypropylene (PP) and hydroxyapatite (HAp) particles) with improved mechanical, dimensional and thermal properties, for commercial FDM setup. But hitherto very less has been reported on process capability of in-house prepared biocompatible feed stock filament. In the present work statistical analysis (for tensile strength, hardness and dimensional accuracy) has been performed for investigations of process capability. The results have been also supported by control charts (X-chart and R-chart) based upon the best feedstock filament wire.

On synergistic effect of BaTiO3 and graphene reinforcement in polyvinyl diene fluoride matrix for four dimensional applications

2021 ◽  
pp. 095440622110157
Author(s):  
Ravinder Sharma ◽  
Rupinder Singh ◽  
Ajay Batish ◽  
Nishant Ranjan
Keyword(s):  
Synergistic Effect ◽  
Fused Deposition Modelling ◽  
Twin Screw Extrusion ◽  
3D Print ◽  
Fused Deposition ◽  
Β Phase ◽  
Pull Out ◽  
Screw Extrusion ◽  
Twin Screw ◽  
Pvdf Matrix

This work presents the synergistic effect of BaTiO3 and graphene (Gr) reinforcement in polyvinyl diene fluoride (PVDF) matrix by chemical-assisted mechanical blending (CAMB) for possible 4D applications. The PVDF matrix was prepared (in form of filament) by solvent casting followed by twin-screw extrusion (TSE) as CAMB process. The filament was used on fused deposition modelling (FDM) setup for preparing standard flexural and pull-out specimens. The mechanical testing revealed that the parts printed with 100% in-fill density (ID), 70 mm/s infill speed (IS), and 45° in-fill angle (IA) has shown better flexural strength (FS). For pull-out properties, part printed at IS 90 mm/s, 0° IA, and 100% ID have shown better results. Further optimized settings of FS were used to 3D print thin cylindrical discs followed by electric poling (for possible piezoelectric properties). The results of X-ray diffraction (XRD) and Fourier transmission infrared spectroscopy (FTIR) analysis show more β-phase formation in the electrically poled sample as compared to non-poled specimen. Moreover, XRD spectra show the homogenous dispersion of doped material in the PVDF matrix. The piezoelectric coefficient (d33) 30.2pC/N was observed on 3D printed specimen (prepared from filament processed with CAMB), suitable for 4D applications.

Graphene Reinforced Composites as Sensing Elements

2019 ◽  
Vol 826 ◽  
pp. 33-44
Author(s):  
Rupinder Singh ◽  
Ranvijay Kumar ◽  
A. Amendola ◽  
Ilenia Farina ◽  
Narinder Singh ◽  
...  
Keyword(s):  
Matrix Material ◽  
Fused Deposition Modelling ◽  
Mixed Solution ◽  
Reinforced Composites ◽  
Twin Screw Extrusion ◽  
Fused Deposition ◽  
Reinforced Composite ◽  
Chemical Exfoliation ◽  
Screw Extrusion ◽  
Twin Screw

The present study deals with the optimal design of a Graphene reinforced composite. The Graphene was prepared by chemical exfoliation process and was chemically blended with matrix material in acetone. Further chemically mixed solution was exposed to air for acetone vaporization. Next, this Graphene composite was extruded through twin screw extrusion (TSE) for preparation of feedstock filament with 1.75±0.05mm diameter via fused deposition modelling (FDM). The presented results suggest that statistically controlled Graphene reinforced functional prototypes can be usefully employed as sensors for bio-medical and engineering applications.

Investigations for partial denture casting by fused deposition modelling-assisted chemical vapour smoothing

2020 ◽  
Vol 40 (5) ◽  
pp. 745-754
Author(s):  
Gurpartap Singh ◽  
Rupinder Singh ◽  
S.S. Bal
Keyword(s):  
Ph Value ◽  
Low Cost ◽  
Chemical Vapour ◽  
Dimensional Accuracy ◽  
Acrylonitrile Butadiene Styrene ◽  
Fused Deposition Modelling ◽  
View Point ◽  
Content Type ◽  
Fused Deposition ◽  
Set Up

Purpose The purpose of this study is to investigate dimensional accuracy (Δd), surface roughness (Ra) and micro hardness (HV) of partial dentures (PD) prepared with synergic combination of fused deposition modelling (FDM) assisted chemical vapour smoothing (CVS) patterns and conventional dental casting (DC) from multi-factor optimization view point. Design/methodology/approach The master pattern for PD was prepared with acrylonitrile butadiene styrene (ABS) thermoplastic on FDM set-up (one of the low cost additive manufacturing process) followed by CVS process. The final PD as functional prototypes was casted with nickel–chromium-based (Ni-Cr) alloy by varying Ni% (Z). The other input parameters were powder to water ratio P/W (X) and pH value (Y) of water used. Findings The results of this study suggest that for controlling the Δd and Ra of the PD, most important factor is X, followed by Z. For hardness of PD, the most important factor is Z. But from overall optimization viewpoint, the best settings are X-100/12, Y-10 and Z-61% (in Ni-Cr alloy). Further, based upon X-bar chart (for HV), the FDM-assisted DC process used for preparation of PD is statistically controlled. Originality/value This study highlights that PD prepared with X-100/12, Y-10 and Z-61% gives overall better results from multi-factor optimization view point. Finally, X-bar chart has been plotted to understand the statistical nature of the synergic combination of FDM, CVS and DC.

A Low-Cost Method to Prepare Biocompatible Filaments with Enhanced Physico-mechanical Properties for FDM 3D Printing

2020 ◽  
Vol 18 ◽  
Author(s):  
Deck Khong Tan ◽  
Niko Münzenrieder ◽  
Mohammed Maniruzzaman ◽  
Ali Nokhodchi
Keyword(s):  
3D Printing ◽  
Low Cost ◽  
Fused Deposition Modelling ◽  
Processing Temperature ◽  
Melt Extrusion ◽  
Screw Extruder ◽  
Fused Deposition ◽  
Single Screw ◽  
Pharmaceutical Applications ◽  
Twin Screw

Background: Fused Deposition Modelling (FDM) 3D printing has received much interest as a fabrication method in the medical and pharmaceutical industry due to its accessibility and cost-effectiveness. A low-cost method to produce biocompatible and biodegradable filaments can improve the usability of FDM 3D printing for biomedical applications. Objectives: The feasibility of producing low-cost filaments suitable for FDM 3D printing via single screw and twin-screw hot melt extrusion was explored. Methods: A single-screw extruder and a twin-screw extruder were used to produce biocompatible filaments composed of varying concentrations of polyethylene glycol (PEG) at 10%, 20%, 30% w/w and polylactic acid (PLA) 90%, 80% and 70% w/w, respectively. DSC, TGA and FTIR were employed to investigate the effect of PEG on the PLA filaments. Results: The presence of PEG lowered the processing temperature of the formulation compositions via melt-extrusion, making it suitable for pharmaceutical applications. The use of PEG can lower the melting point of the PLA polymer to 170 °C, hence lowering the printing temperature. PEG can also improve the plasticity of the filaments, as the rupture strain of twinscrew extruded filaments increased up to 10-fold as compared to the commercial filaments. Advanced application of FTIR analysis confirmed the compatibility and miscibility of PEG with PLA. Conclusion: Twin-screw extrusion is more effective in producing a polymeric mixture of filaments as the mixing is more homogenous. The PEG/PLA filament is suitable to be used in 3D printing of medical or pharmaceutical applications such as medical implants, drug delivery systems, or personalised tablets.

Experimental investigations for preparation of biocompatible feedstock filament of fused deposition modeling (FDM) using twin screw extrusion process

2017 ◽  
Vol 31 (11) ◽  
pp. 1455-1469 ◽  
Author(s):  
Rupinder Singh ◽  
Nishant Ranjan
Keyword(s):  
Fused Deposition Modeling ◽  
Extrusion Process ◽  
Functionally Graded ◽  
Experimental Investigations ◽  
Twin Screw Extrusion ◽  
Fused Deposition ◽  
Screw Extrusion ◽  
Twin Screw ◽  
Deposition Modeling ◽  
Ceramic Fillers

Twin screw extrusion (TSE) is one of the commercially established processes for reinforcement of metallic/nonmetallic/ceramic fillers in polymer matrix for tailor-made applications. In this study, biocompatible feedstock filament has been prepared (in-house) for commercial fused deposition modeling (FDM) setup with biocompatible grade polymers, namely polyvinyl chloride and polypropylene which was reinforced with the hydroxyapatite particles. The process parameters (namely, material composition, rotational speed of TSE, die temperature of TSE, HAp particle grain size, and applied load on TSE) were optimized using Taguchi L18 orthogonal array. In this study, mechanical, thermal, and metallurgical properties have been established, and best-feedstock filament wire for development of partial/complete denture on the FDM with functionally graded surfaces properties has been recommended for future applications.

Process capability analysis of fused deposition modelling for plastic components

2014 ◽  
Vol 20 (1) ◽  
pp. 69-76 ◽  
Author(s):  
Rupinder Singh
Keyword(s):  
Process Capability ◽  
Dimensional Accuracy ◽  
Fused Deposition Modelling ◽  
Economic Point ◽  
Content Type ◽  
Process Capability Analysis ◽  
Fused Deposition ◽  
Capability Analysis ◽  
Measuring Machine ◽  
Plastic Components

Purpose – The purpose of the present study is process capability analysis of fused deposition modelling (FDM) process as rapid pattern making (RDPM) solutions for plastic components. Design/methodology/approach – Starting from the identification of component, prototypes with ABS plastic material were produced and dimensional measurements were made with coordinate measuring machine (CMM). Some important mechanical properties were also compared to verify the suitability of the components. Findings – The study highlighted the best settings of orientation, support material quantity for the selected component as a case study on FDM machine from dimensional accuracy and economic point of view as RDPM solution for plastic components. Practical implications – This process ensures rapid production of statistically controlled pre-series technological prototypes and proof of concept at less production cost and time. Final components produced are acceptable as per ISO standard UNI EN 20286-I and DIN16901. Originality/value – The results of the study suggest that FDM process lies in ±4.5 sigma (σ) limit in regard to dimensional accuracy of plastic component is concerned and may be gainfully employed as RDPM solution for bio-medical applications.

scholarly journals Improving the Oxygen Barrier of Polyamide Food Packaging by Using Nanoclay

2021 ◽  
Author(s):  
Tonis PAARA ◽  
Sven LANGE ◽  
Kristjan SAAL ◽  
Rünno LÕHMUS ◽  
Andres KRUMME ◽  
...  
Keyword(s):  
Food Packaging ◽  
Transmission Rate ◽  
Low Cost ◽  
Twin Screw Extrusion ◽  
Oxygen Transmission Rate ◽  
Industrial Grade ◽  
Screw Extrusion ◽  
Twin Screw ◽  
Polyamide Film ◽  
Film Making

The effect of nanoclay additive on polyamide film oxygen permeability is investigated from the perspective of possible use as a laminate component for low-cost food packaging material. Montmorillonite nanoclay was melt-mixed in an industrial grade polyamide by twin-screw extrusion and the mixture was hot-pressed to a ~50 µm thick film. The film with 10 wt.% of nanoclay loading showed a 17 % decrease in the oxygen transmission rate (OTR), as compared to the pristine polyamide film (72 and 87 cm3/m2∙24 h, respectively). Despite the relatively high loading of the filler the obtained OTR exceeds that of the food packaging preferred upper limit of 10 cm3/m2∙24 h. XRD measurements confirmed the near-complete exfoliation of the nanoclay platelets. The platelets were found to be at an average angle of 9.5 degrees relative to the film’s surface plane. To comply with the requirements for food packaging, this angle needs to be decreased down to 0.4 degrees. To achieve this, different film-making methods enabling better control over the filler particles’ orientation need to be explored. Nanoclay addition increased the films’ yield strength (23 % for 10 wt.% film) and stiffness, while not affecting the films’ optical appearance.

Evaluation of geometrical benchmark artifacts containing multiple overhang lengths fabricated using material extrusion technique

2020 ◽  
Vol 14 (3) ◽  
pp. 7296-7308
Author(s):  
Siti Nur Humaira Mazlan ◽  
Aini Zuhra Abdul Kadir ◽  
N. H. A. Ngadiman ◽  
M.R. Alkahari
Keyword(s):  
3D Model ◽  
Laser Scanner ◽  
Dimensional Accuracy ◽  
Fused Deposition Modelling ◽  
Layer By Layer ◽  
Fused Deposition ◽  
Layer Technique ◽  
Subtractive Manufacturing ◽  
Manufacturing Features ◽  
Layer Problem

Fused deposition modelling (FDM) is a process of joining materials based on material entrusion technique to produce objects from 3D model using layer-by-layer technique as opposed to subtractive manufacturing. However, many challenges arise in the FDM-printed part such as warping, first layer problem and elephant food that was led to an error in dimensional accuracy of the printed parts especially for the overhanging parts. Hence, in order to investigate the manufacturability of the FDM printed part, various geometrical and manufacturing features were developed using the benchmarking artifacts. Therefore, in this study, new benchmarking artifacts containing multiple overhang lengths were proposed. After the benchmarking artifacts were developed, each of the features were inspected using 3D laser scanner to measure the dimensional accuracy and tolerances. Based on 3D scanned parts, 80% of the fabricated parts were fabricated within ±0.5 mm of dimensional accuracy as compared with the CAD data. In addition, the multiple overhang lengths were also successfully fabricated with a very significant of filament sagging observed.

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