Evaluation of Mechanical and Wear Properties of Ceramic and Inorganic compounds based Composite via PM route and Optimization through Robust design technique

The present research study investigates the Mechanical, Physical, and Tribological properties of powder metallurgy (PM) produced AA6063 alloy reinforced with silicon nitride (Si3N4) and copper nitrate (CuN2O6). Incorporation of Si3N4 & CuN2O6 reinforcement in matrix material ranged from 6 to 12 % Si3N4 in a 6-step interval and 2 to 6 %CuN2O6 in a two-step interval. The characterizations were made on the PM-produced specimens using OM, EDS, XRD, and Hardness. The reinforcement particles were uniformly distributed, which was attributed to a homogeneous mixer of matrix and reinforcements. The test findings show that as the reinforcing percentage of the ceramic and inorganic compound increases, properties such as hardness and density rise considerably and monolithically. The existence of phases such as Si3N4 and CuN2O6 reinforcement in the AA6063 matrix was ensured by X-ray diffraction. The hardness of AA6063/12%Si3N4/6%CuN2O6 increased by 88% over the base alloy due to a mismatch in thermal expansion between the Al matrix and reinforcement, which causes massive internal stress, causing the aluminium matrix to plastically deform to accommodate the reduced volume expansion of Si3N4 and CuN2O6 particles. The dry sliding wear test was determined using the Pin-on-Disc method, and the results show that the composite is more wear-resistant. An orthogonal array and analysis of variance were utilized to evaluate the solution, including parameters using the Taguchi robust design technique. The weight percentage of the Si3N4/CuN2O6 compound and the relationship between weight % of reinforcement and applied load had the most significant impact on composite wear resistance. The produced composite's wear morphology was studied using images from a scanning electron microscope and energy dispersive spectroscopy.

Study of the Possibilities of Obtaining Powder Materials by Rotational Turning with Multi-Faceted Cutters

Composite materials obtained through powder metallurgy methods are increasingly applied in various industries, particularly in aviation and rocket and space equipment which use their high specific strength, resistance to high temperatures and other properties. Producers of composite materials use various metallic and non-metallic materials (fibres and powders) as fillers [1-2]. For example, the high plasticity (moldability) of aluminium powders allows utilizing them as a matrix material in moulding of composites using various methods of rolling, extrusion, and intense plastic deformation [3-5]. However, the widespread use of chip as a raw material for the production of composites is hampered by the complexities in obtaining powders with granules of the necessary shape and size.

PENGGUNAAN MODUL MATRIKS UNTUK MENINGKATKAN HASIL BELAJAR MATEMATIKA PESERTA DIDIK KELAS XI SMK

This research is a class action research (Classroom Action Research) which was carried out at SMK Muhammadiyah Watansoppeng and aims to improve mathematics learning outcomes through the use of matrix modules in class XI students of SMK Muhammadiyah Watansoppeng. The subjects of this study were 15 students of class XI SMK Muhammadiyah Watansoppeng in the 2021/2022 academic year. Data collection techniques used are learning outcomes tests and observations. The data collected were analyzed using descriptive analysis using quantitative and qualitative analysis. The results of the analysis showed an increase in mathematics learning outcomes. The results of quantitative analysis show that the average score of mastery of students in the first cycle of 70.53 is in the high category with the percentage of completeness reaching 60%, this indicates that students have not achieved classical mastery. And the average score of mastery of students in cycle II of 78.27 is in the high category with the percentage of completeness reaching 87%, this shows that students have achieved classical mastery. The results of qualitative analysis based on observations showed an increase in student activity in accordance with learning, namely the increase in students attending the learning process, who actively asked questions about material that was not clear in the matrix module, who exchanged opinions with other students in solving problems in the matrix module, which actively respond to other friends' questions, who are working on practice questions in the module given by the teacher, and there is a decrease in student activity that is not in accordance with learning. Based on the results of the analysis, it appears that there is a change that the use of the module is quite effective in improving mathematics learning outcomes in class XI students of SMK Muhammadiyah Watansoppeng on matrix material. ABSTRAKPenelitian ini adalah penelitian tindakan kelas (Classroom Action Reseach) yang dilaksanakan di SMK Muhammadiyah Watansoppeng dan bertujuan untuk meningkatkan hasil belajar matematika melalui penggunaan modul matriks pada peserta didik kelas XI SMK Muhammadiyah Watansoppeng. Subjek penelitian ini adalah siswa kelas XI SMK Muhammadiyah Watansoppeng pada tahun pelajaran 2021/2022 sebanyak 15 siswa. Teknik pengumpulan data yang digunakan adalah tes hasil belajar dan observasi. Data yang terkumpul dianalisis dengan menggunakan analisis deskriptif dengan menggunakan analisis secara kuantitatif dan kualitatif. Hasil analisis menunjukkan adanya peningkatan hasil belajar matematika. Hasil analisis kuantitatif menunjukkan bahwa skor rata-rata penguasaan peserta didik pada siklus I sebesar 70,53 berada dalam kategori tinggi dengan persentase ketuntasan mencapai 60%, hal ini menunjukkan bahwa peserta didik belum mencapai ketuntasan kelasikal. Dan skor rata-rata penguasaan peserta didik pada siksus II sebesar 78,27 berada dalam kategori tinggi dengan persentase ketuntasan mencapai 87%, hal ini menunjukkan bahwa peserta didik sudah mencapai ketuntasan kelasikal. Hasil analisis kualitatif berdasarkan observasi menunjukkan peningkatan aktivitas peserta didik yang sesuai dengan pembelajaran yakni meningkatnya peserta didik hadir dalam proses belajar, yang aktif bertanya tentang materi yang belum jelas pada modul matriks, yang bertukar pendapat dengan peserta didik lain dalam menyelesaikan permasalahan pada modul matriks, yang aktif memberikan tanggapan terhadap pertanyaan teman yang lain, yang mengerjakan soal latihan dalam modul yang diberikan oleh guru, dan terjadi penurunan aktivitas peserta didik yang tidak sesuai dengan pembelajaran. Berdasarkan hasil analisis tersebut, nampak adanya perubahan bahwa penggunaan modul cukup efektif untuk meningkatkan hasil belajar matematika pada peserta didik kelas XI SMK Muhammadiyah Watansoppeng pada materi matriks.

Natural Fiber-Reinforced Polylactic Acid, Polylactic Acid Blends and Their Composites for Advanced Applications

Polylactic acid (PLA) is a thermoplastic polymer produced from lactic acid that has been chiefly utilized in biodegradable material and as a composite matrix material. PLA is a prominent biomaterial that is widely used to replace traditional petrochemical-based polymers in various applications owing environmental concerns. Green composites have gained greater attention as ecological consciousness has grown since they have the potential to be more appealing than conventional petroleum-based composites, which are toxic and nonbiodegradable. PLA-based composites with natural fiber have been extensively utilized in a variety of applications, from packaging to medicine, due to their biodegradable, recyclable, high mechanical strength, low toxicity, good barrier properties, friendly processing, and excellent characteristics. A summary of natural fibers, green composites, and PLA, along with their respective properties, classification, functionality, and different processing methods, are discussed to discover the natural fiber-reinforced PLA composite material development for a wide range of applications. This work also emphasizes the research and properties of PLA-based green composites, PLA blend composites, and PLA hybrid composites over the past few years. PLA’s potential as a strong material in engineering applications areas is addressed. This review also covers issues, challenges, opportunities, and perspectives in developing and characterizing PLA-based green composites.

Fabrication and characterization of SiC-reinforced Al-4032 metal matrix composites

Aluminium metal matrix composites (AMCs) have become quite popular for light weight, low cost, and good workability. The present work reports the impact of silicon carbide (SiC) reinforcement on the physical, microstructural, and mechanical characteristics of Al-4032/SiC composites with 4, 6, 8% of SiC (particle size 54μm) fabricated through bottom pouring stir casting. Density and porosity measurements of all three AMCs have been performed using the rule of mixture. The microstructure of the AMC samples has been analyzed using an optical microscope (OM), x-ray diffraction analysis (XRD), and scanning electron microscopy (SEM) equipped with energy dispersive spectroscopy (EDS). The mechanical properties, in terms of the ultimate tensile strength (UTS), elongation, micro-hardness, and impact toughness of the AMCs have also been obtained according to American society for testing and materials (ASTM) standards. A maximum 1.52% increase in theoretical density, while a maximum 2.92% decrease in experimental density has been recorded for 8% reinforcement. The UTS, microhardness, and impact toughness of the AMC have been found to improve significantly owing to the addition of ceramic particles. The uniform distribution of SiC particles all over base Al-4032 matrix material has been noticed by SEM and OM for AMCs up to 6% reinforcement.

The Study of Enhanced Mechanical Properties for Cu/Gr/2024Al Composite

2024Al alloy powder as matrix material with nanocopper-modified graphene as reinforcement was studied to explore the effects of graphene on the tissue, hardness, friction performance of the composite. The Cu/Gr/2024Al composites were prepared via three-dimensional mixed powder and vacuum hot press sintering. The results found that the nanocopper-modified graphene could be uniformly distributed in the aluminum alloy matrix, and formed a good binding interface with the matrix material. When the graphene content was 0.75 wt.% and 1.0wt%, the impact yield strength and the hardness reached the maximum of 434.8 MPa and 118.4 HV5, which were 27.24% and 43.11% higher than that of 2024Al respectively. Furthermore, with the increase of nanocopper-modified graphene content, the corrosion resistance of composite materials in 3.5%Cl-concentration solution was improved.

INFLUENCE OF IPNS (VINYLESTER/EPOXY/POLYURETHANE) ON THE MECHANICAL PROPERTIES OF GLASS/CARBON FIBER REINFORCED HYBRID COMPOSITES

The main objective of this study is to compare the interpenetrating polymer networks’ (IPNs) physical strengths with different variants of fibers. In this study, E-glass, carbon, and a combination of E-glass and carbon fiber (hybrid) have been taken as the reinforcement. Similarly, three combinations of the IPNs were chosen as the matrix material, namely epoxy / polyurethane (EP), vinyl ester / polyurethane (VP) and epoxy/vinyl ester (EV) as IPN blends. In order to thoroughly understand the physical characteristics of the combination of blends and fibers, nine variants (laminates) were fabricated: combinations of epoxy / polyurethane / E-glass (EPG), epoxy / polyurethane / carbon (EPC), epoxy / vinyl ester / glass / carbon (EPGC-hybrid), vinyl ester / polyurethane / glass (VPG), vinyl ester / polyurethane / carbon (VPC), vinyl ester / polyurethane / glass / carbon (VPGC), epoxy / vinyl ester / glass (EVG), epoxy / vinyl ester / carbon (EVC), and epoxy / vinyl ester / glass / carbon (EVGC-hybrid), all with help of a hand-layup technique. Furthermore, mechanical tests such as tensile, flexural, impact, and HDT (heat distortion temperature) were performed on all the variants as per the ASTM standards. Results shows that carbon fiber reinforcement with all IPN combinations has shown extraordinary performance (double fold) over the E-glass fiber reinforcement, whereas the hybrid (combination of E-glass/carbon) laminates have shown excellent characteristics over E-glass fiber reinforcement, irrespective of IPN matrix material. All the results were compared with each other and their corresponding variations were plotted as bar charts. ABSTRAK: Objektif utama kajian ini adalah bagi membandingkan kekuatan fizikal rangkaian polimer saling menusuk (IPN) dengan pelbagai jenis gentian berbeza. Kajian ini mengguna pakai gentian kaca-E, karbon dan gabungan kaca-E dan gentian karbon (hibrid) sebagai penguat. Begitu juga, tiga kombinasi IPN dipilih sebagai bahan matrik, iaitu epoksi / poliuretan (EP), ester vinil / poliuretan (VP) dan epoksi / ester vinil (EV) sebagai campuran IPN. Bagi tujuan memahami secara mendalam ciri-ciri fizikal gabungan campuran dan gentian, sembilan varian (lamina) dihasilkan, malaui kombinasi seperti epoksi / poliuretan / kaca-E (EPG), epoksi / poliuretan / karbon (EPC), epoksi / ester vinil / kaca / karbon (EPGC-hibrid), ester vinil / poliuretan / kaca (VPG), ester vinil / poliuretan / karbon (VPC), ester vinil / poliuretan / kaca / karbon (VPGC), epoksi / ester vinil / kaca (EVG), epoksi / ester vinil / karbon (EVC), epoksi / ester vinil / kaca / karbon (EVGC-hibrid) dengan teknik susun atur lapisan menggunakan tangan. Selain itu, ujian mekanikal seperti tegangan, lenturan, hentaman dan HDT (suhu kelenturan panas) dilakukan pada semua varian mengikut piawaian ASTM. Dapatan kajian menunjukkan bahawa, penguat gentian karbon dengan semua kombinasi IPN telah menunjukkan prestasi luar biasa (dua kali ganda) daripada penguat gentian kaca-E, manakala lamina hibrid (campuran kaca-E / karbon) telah menunjukkan ciri-ciri sangat baik berbanding penguat gentian kaca-E tanpa mengira bahan matrik IPN. Semua hasil dapatan dibandingkan antara satu sama lain dan padanan variasi diplot sebagai carta bar.

Investigation of the Biocidal Performance of Multi-Functional Resin/Copper Nanocomposites with Superior Mechanical Response in SLA 3D Printing

Metals, such as silver, gold, and copper are known for their biocidal properties, mimicking the host defense peptides (HDPs) of the immune system. Developing materials with such properties has great importance in medicine, especially when combined with 3D printing technology, which is an additional asset for various applications. In this work, copper nanoparticles were used as filler in stereolithography (SLA) ultraviolet (UV) cured commercial resin to induce such biocidal properties in the material. The nanocomposites developed featured enhanced mechanical responses when compared with the neat material. The prepared nanocomposites were employed to manufacture specimens with the SLA process, to be tested for their mechanical response according to international standards. The process followed was evaluated with Scanning Electron Microscopy (SEM), Atomic Force Microscopy (AFM), energy-dispersive X-ray spectroscopy (EDS), and thermogravimetric analysis (TGA). The antibacterial activity of the fabricated nanocomposites was evaluated using the agar-well diffusion method. Results showed enhanced mechanical performance of approximately 33.7% in the tensile tests for the nanocomposites filled with 1.0 wt.%. ratios, when compared to the neat matrix material, while this loading showed sufficient antibacterial performance when compared to lower filler loadings, providing an added value for the fabrication of effective nanocomposites in medical applications with the SLA process.

Study on Mechanical and Wear Behaviour of AA7075/TaC/Si3N4/Ti Hybrid Metal Matrix Composites

This research article focuses on the development of AA7075 alloy reinforced with different wt% of Tantalum Carbide (TaC), Silicon Nitride (Si3N4) and Titanium (Ti) particulates using stir casting. Mechanical characteristics like tensile, compression and microhardness of the developed composites were analysed. High temperature tribological properties of the hybrid MMCs were studied for various input control factors like sliding speed, load and temperature. Design analysis has been executed by Taguchi orthogonal array and ANOVA (Analysis of Variance). The incorporated reinforcements exhibited improved wear resistance at ambient temperature along with elevated temperatures. Monolithic dissemination of reinforcement’s in the prepared composites magnifies the mechanical and tribological characteristics for composites compared to matrix material. From the optimization technique, it was witnessed that Wear Rate and Frictional Coefficient are afflicted by temperature go after load & sliding speed. The optimal amalgamation of control parameters of distinct tribo-responses has been detected.

Experimental Investigation on Aquatic Waste Water Hyacinth (Eichhorniacrassipes) Plant into Natural Fibre Polymer Composite – Biological Waste into Commercial Product

Present work dealt with evaluating the aquatic wastewater hyacinth plant long fibre reinforced withepoxy polymer composite mechanical strength, absorption, characterization, thermal degradation and stability, surface morphology studies. This research work water hyacinth long fibre is used as a reinforcement material and epoxy polymer matrix material is used as a matrix phase material. By utilizing the compression moulding hot press machine the different weight percentages (20, 25, 30, and 35%) of the hyacinth composite samples areproduced.Converting the biological waste into zero waste and useful product concept is achieved in this research. In this work hyacinth, long fibre is extracted with a new novel mechanical way (fabricated machine) of the extraction process. Hyacinth long fibre composite tensile strength (mechanical strength) is varied from 36.42 to 44.62MPa, flexural strength varied from 47.86 to 59.684MPa, and impact strength varied from 0.5 to 3.5J. After the 8th hour of monitoring the composite samples are attained constant values on both water and chemical absorption studies. By utilizing thermogravimetric analysis, x-ray diffraction method, Fourier transform infrared spectroscopy method the essential functional groups present in the hyacinth composites are identified. Based on the final experiment results the hyacinth fibre composite is highly recommended to the usage of profit oriented products.