Determination of physiological noble metals in human urine using liquid-liquid extraction and Zeeman electrothermal atomic absorption spectrometry

1997 ◽  
Vol 340 (1-3) ◽  
pp. 277-283 ◽  
Author(s):  
Jutta Begerow ◽  
Martina Turfeid ◽  
Lothar Dunemann
2003 ◽  
Vol 491 (2) ◽  
pp. 231-237 ◽  
Author(s):  
Cláudio José de Castro Maciel ◽  
Gilmar Machado Miranda ◽  
Danielle Palma de Oliveira ◽  
Maria Elisa P.B. de Siqueira ◽  
Josianne Nicácio Silveira ◽  
...  

1983 ◽  
Vol 66 (4) ◽  
pp. 850-852
Author(s):  
Earle E Cary ◽  
Michael Rutzke

Abstract This method involves sample digestion in nitric, perchloric, and sulfuric acids. Chromium is concentrated by coprecipitation with ferric hydroxide. Redissolved iron is removed by liquid-liquid extraction, remaining silica is dissolved with hydrofluoric acid, and chromium is determined by electrothermal atomic absorption spectrometry. The sensitivity and detection limits for chromium approach those given by the manufacturers of the various instruments. Recovery studies and analysis of standard materials show that this method is reliable.


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