Preparation and characterization of tris(trimethylsilyl)silyl derivatives of tin. X-ray crystal structure of Cl2Sn[Si(Si(CH3)3)3]2

1990 ◽  
Vol 29 (18) ◽  
pp. 3525-3528 ◽  
Author(s):  
S. P. Mallela ◽  
Russell A. Geanangel



1987 ◽  
Vol 26 (13) ◽  
pp. 2106-2109 ◽  
Author(s):  
John Arnold ◽  
T. Don Tilley ◽  
Arnold L. Rheingold ◽  
Steven J. Geib






2017 ◽  
Vol 18 (3) ◽  
pp. 195-201 ◽  
Author(s):  
Marina Z. Mijajlovic ◽  
Milos V. Nikolic ◽  
Dusan Lj. Tomovic ◽  
Andriana M. Bukonjic ◽  
Aleksandar Kocovic ◽  
...  

Abstract New platinum(IV)-complexes with S-alkyl derivatives of thiosalicylic acid (alkyl = benzyl-(L1), methyl-(L2), ethyl-(L3), propyl-(L4), butyl-(L5)) have been synthesized and characterized by microanalysis, infrared spectroscopy, and 1H and 13C NMR spectroscopy. Th e bidentate S,O ligand precursor, the S-butyl derivative of thiosalicylic acid (S-bu-thiosal), was prepared, and its crystal structure was determined. Single crystals suitable for X-ray measurements were obtained by slow crystallization from a DMSO-water system. S-bu-thiosal crystallized in a P21/c space group of a monoclinic crystal system with a = 8.0732 (3) Å, b = 19.6769 (4) Å, c = 8.2291 (3) Å and Z = 4. S-bu-thiosal also has a coplanar geometry.



Sign in / Sign up

Export Citation Format

Share Document