Detailed analysis of the S-RESPDOR solid-state NMR method for inter-nuclear distance measurement between spin-1/2 and quadrupolar nuclei

2012 ◽  
Vol 215 ◽  
pp. 34-49 ◽  
Author(s):  
Xingyu Lu ◽  
Olivier Lafon ◽  
Julien Trébosc ◽  
Jean-Paul Amoureux
Keyword(s):  
Solid State ◽  
Detailed Analysis ◽  
Solid State Nmr ◽  
Distance Measurement ◽  
Quadrupolar Nuclei ◽  
Nmr Method

I-STMAS, a new high-resolution solid-state NMR method for half-integer quadrupolar nuclei

2003 ◽  
Vol 23 (4) ◽  
pp. 213-223 ◽  
Author(s):  
Jean-Paul Amoureux ◽  
Cláudia Morais ◽  
Julien Trebosc ◽  
João Rocha ◽  
Christian Fernandez
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Quadrupolar Nuclei ◽  
Nmr Method ◽  
Half Integer

Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions

2010 ◽  
Vol 206 (2) ◽  
pp. 269-273 ◽  
Author(s):  
Lei Chen ◽  
Xingyu Lu ◽  
Qiang Wang ◽  
Olivier Lafon ◽  
Julien Trébosc ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Distance Measurement ◽  
Quadrupolar Nuclei ◽  
Half Integer ◽  
Analytical Expressions

Modern solid-state NMR of quadrupolar nuclei

2010 ◽  
Vol 51 (S1) ◽  
pp. 28-46 ◽  
Author(s):  
O. B. Lapina ◽  
D. F. Khabibulin ◽  
A. A. Shubin
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Quadrupolar Nuclei

Thermosetting Mechanism Study of Organosilicon Polymer Containing Carborane by Solid-State NMR Spectroscopy

1999 ◽  
Vol 576 ◽  
Author(s):  
H. Kimura ◽  
K. Okita ◽  
M. Ichitani ◽  
M. Yonezawa ◽  
T. Sugimoto
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Main Chain ◽  
Addition Reaction ◽  
Side Chain ◽  
Mechanism Study ◽  
Nmr Method ◽  
Organosilicon Polymer ◽  
Thermal Stable

ABSTRACTThe thermosetting mechanism of an organosilicon polymer containing carborane has been studied utilizing the 13and 29Si solid-state NMR method. The polymer having C≡C bonds in the main chain and CH═CH2, Si-H bonds, and carborane in the bulky side chain, shows a very highly thermal stability in air by curing. From 13C and 29Si NMR spectra of the polymer, it was found that the intermolecular cross-linking reactions of the polymer was due to (1) the diene reaction between Ph-C≡C and C≡C and (2) the addition reaction between side chain terminal and Ph-C≡C and between CH═CH2 and Si–H, and a very highly thermal stable structure is formed.

A solid-state NMR method to determine domain sizes in multi-component polymer formulations

2015 ◽  
Vol 261 ◽  
pp. 43-48 ◽  
Author(s):  
Judith Schlagnitweit ◽  
Mingxue Tang ◽  
Maria Baias ◽  
Sara Richardson ◽  
Staffan Schantz ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Method

Signal enhancement in solid-state NMR of quadrupolar nuclei

2013 ◽  
Vol 51-52 ◽  
pp. 1-15 ◽  
Author(s):  
Frédéric A. Perras ◽  
Jasmine Viger-Gravel ◽  
Kevin M.N. Burgess ◽  
David L. Bryce
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Signal Enhancement ◽  
Quadrupolar Nuclei
Sign in / Sign up

Export Citation Format

Share Document