Fluorinated linkers for monitoring solid-phase synthesis using gel-phase 19F NMR spectroscopy

1998 ◽  
Vol 39 (39) ◽  
pp. 7193-7196 ◽  
Author(s):  
Anette Svensson ◽  
Karl-Erik Bergquist ◽  
Tomas Fex ◽  
Jan Kihlberg
2003 ◽  
Vol 2003 (8) ◽  
pp. 1529-2532 ◽  
Author(s):  
Marc S. Robillard ◽  
Jason S. Leith ◽  
Gijs A. van der Marel ◽  
Jacques H. van Boom ◽  
Jan Reedijk

ChemInform ◽  
2010 ◽  
Vol 24 (10) ◽  
pp. no-no
Author(s):  
E. GIRALT ◽  
F. ALBERICIO ◽  
F. BARDELLA ◽  
R. ERITJA ◽  
M. FELIZ ◽  
...  

2010 ◽  
Vol 8 (1) ◽  
pp. 28-33 ◽  
Author(s):  
Piotr Stefanowicz ◽  
Joanna Batorska ◽  
Monika Kijewska ◽  
Hubert Bartosz-Bechowski ◽  
Zbigniew Szewczuk ◽  
...  

AbstractWe established, that crystalline hydrate of 2,3:4,5-di-O-isopropylidene-β-D-arabino-hexos-2-ulo-2,6-pyranose is a new, convenient and stable reagent for solid phase synthesis of peptide derived Amadori products. The structure of the title compound was studied by X-ray analysis, NMR spectroscopy, and high resolution ESI-MS. The crystal structure indicated the existence of two symmetry-independent molecules that were not connected with hydrogen bonds. A comparison with previously reported 2,3:4,5-di-O-isopropylidene-β-D-fructopyranose revealed, that these two compounds are isostructural.


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