Synthesis of 13C/19F/2H Labeled Indoles for Use as Tryptophan Precursors for Protein NMR Spectroscopy

2021 ◽  
Author(s):  
Ansis Maleckis ◽  
Iresha Herath ◽  
Gottfried Otting
Keyword(s):  
Nmr Spectroscopy ◽  
Protein Nmr ◽  
Ring Closing Metathesis ◽  
13C Isotope ◽  
Protein Nmr Spectroscopy ◽  
Spin Pairs

Synthesis of indoles labeled with 13C-1H and 13C-19F spin pairs is described. All syntheses utilize inexpensive carbon-13C dioxide as the 13C isotope source. Ruthenium-mediated ring-closing metathesis is the key step...

Recent Developments in Protein NMR Spectroscopy

1996 ◽  
pp. 117-120
Author(s):  
Stephan Grzesiek ◽  
Geerten W. Vuister ◽  
Andy C. Wang ◽  
Frank Delaglio ◽  
Ad Bax
Keyword(s):  
Nmr Spectroscopy ◽  
Protein Nmr ◽  
Recent Developments ◽  
Protein Nmr Spectroscopy

scholarly journals PCR-based gene synthesis and protein NMR spectroscopy

Structure ◽  
1997 ◽  
Vol 5 (11) ◽  
pp. 1407-1412 ◽  
Author(s):  
Danilo R Casimiro ◽  
Peter E Wright ◽  
H Jane Dyson
Keyword(s):  
Nmr Spectroscopy ◽  
Protein Nmr ◽  
Gene Synthesis ◽  
Protein Nmr Spectroscopy

Simple and inexpensive incorporation of 19F-Tryptophan for protein NMR spectroscopy

2012 ◽  
Vol 48 (86) ◽  
pp. 10681 ◽  
Author(s):  
Peter B. Crowley ◽  
Ciara Kyne ◽  
William B. Monteith
Keyword(s):  
Nmr Spectroscopy ◽  
Protein Nmr ◽  
Protein Nmr Spectroscopy

Recent advances in protein NMR spectroscopy and their implications in protein therapeutics research

2013 ◽  
Vol 406 (9-10) ◽  
pp. 2279-2288 ◽  
Author(s):  
Guifang Wang ◽  
Ze-Ting Zhang ◽  
Bin Jiang ◽  
Xu Zhang ◽  
Conggang Li ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Protein Nmr ◽  
Protein Therapeutics ◽  
Recent Advances ◽  
Protein Nmr Spectroscopy
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