New nano stationary phase GC capillary columns for fast analysis of PAH by GC and GC/MS

2009 ◽  
Vol 89 (15) ◽  
pp. 1113-1123 ◽  
Author(s):  
Allen J. Britten ◽  
Krishnat P. Naikwadi
1981 ◽  
Vol 208 (2) ◽  
pp. 231-238 ◽  
Author(s):  
Lars Blomberg ◽  
Jan Buijtenjk ◽  
Karin Markides ◽  
Thomas Wännman

2008 ◽  
Vol 28 (3) ◽  
pp. 165-180 ◽  
Author(s):  
Allen J. Britten ◽  
Krishnat P. Naikwadi

2016 ◽  
Vol 89 (12) ◽  
pp. 1978-1984 ◽  
Author(s):  
A. Yu. Shmykov ◽  
A. N. Krasovskii ◽  
N. A. Bubis ◽  
A. L. Bulyanitsa ◽  
N. A. Esikova ◽  
...  

1988 ◽  
Vol 454 ◽  
pp. 65-71 ◽  
Author(s):  
E. Matisová ◽  
A. Moravcová ◽  
J. Krupčík ◽  
P. Čellár ◽  
P.A. Leclercq

2018 ◽  
Vol 46 (1) ◽  
pp. 39-42
Author(s):  
Dana Moravcová ◽  
Josef Planeta

Abstract The monolithic capillary columns (0.1 mm x 150 mm) prepared by the acidic hydrolysis of tetramethoxysilane (TMOS) in the presence of polyethylene glycol (PEG) and urea were modified by zwitterionic stationary phases and evaluated under HILIC separation conditions by employing a mixture containing nucleosides and nucleotides. The polymeric layer of zwitterions did not affect the high separation efficiency of the original silica monolith. The prepared zwitterionic columns exhibited high separation efficiencies in a range 61,000-289,000 theoretical plates/m for a 2- methacryloyloxyethyl phosphorylcholine-based stationary phase and in a range 59,000-135,000 theoretical plates/m for a [2-(methacryloyloxy)ethyl]dimethyl-(3-sulfopropyl)ammonium hydroxide-based stationary phase under optimal separation conditions. The grafted layer of zwitterions on the silica monolithic surface also significantly improved the separation selectivity to compounds of interest


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