Faculty Opinions recommendation of Large scale preparation of silicon-functionalized SynPhase Polystyrene lanterns for solid-phase synthesis.

2009 ◽  
Author(s):  
Anthony Czarnik
Keyword(s):  
Large Scale ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Phase Synthesis ◽  
Large Scale Preparation ◽  
Scale Preparation

Criteria for the economic large scale solid-phase synthesis of oligonucleotides

Tetrahedron ◽  
1994 ◽  
Vol 50 (8) ◽  
pp. 2617-2622 ◽  
Author(s):  
F.Xavier Montserrat ◽  
Anna Grandas ◽  
Ramon Eritja ◽  
Enrique Pedroso
Keyword(s):  
Large Scale ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Phase Synthesis

scholarly journals Synthesis by extrusion: continuous, large-scale preparation of MOFs using little or no solvent

2015 ◽  
Vol 6 (3) ◽  
pp. 1645-1649 ◽  
Author(s):  
Deborah Crawford ◽  
José Casaban ◽  
Robert Haydon ◽  
Nicola Giri ◽  
Tony McNally ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Large Scale ◽  
Phase Synthesis ◽  
Large Scale Preparation ◽  
Scale Preparation ◽  
Melt Phase

Continuous flow mechanochemical and melt-phase synthesis at kg h−1 rates from solid reagents and either no solvent, or only minimal solvent, is reported.

A Facile Template-Free Approach for the Large-Scale Solid-Phase Synthesis of CdS Nanostructures and Their Excellent Photocatalytic Performance

Small ◽  
2011 ◽  
Vol 7 (7) ◽  
pp. 957-964 ◽  
Author(s):  
Sanjay K. Apte ◽  
Sunil N. Garaje ◽  
Gurudas P. Mane ◽  
Ajayan Vinu ◽  
Sonali D. Naik ◽  
...  
Keyword(s):  
Large Scale ◽  
Photocatalytic Performance ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Phase Synthesis ◽  
Cds Nanostructures ◽  
Template Free

scholarly journals Optimal Method for Disulfide Bond Closure in the Synthesis of Atosiban—Antagonist of Oxytocin Receptors

2021 ◽  
Vol 47 (6) ◽  
pp. 1241-1248
Author(s):  
D. V. Avdeev ◽  
M. V. Ovchinnikov ◽  
Y. S. Dudkina ◽  
A. S. Molokoedov ◽  
A. A. Azmuko ◽  
...  
Keyword(s):  
Disulfide Bond ◽  
Large Scale ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Comparative Assessment ◽  
Polymer Support ◽  
Optimal Method ◽  
Phase Synthesis ◽  
Oxytocin Receptors ◽  
By Products

Abstract This work is devoted to the large-scale solid-phase synthesis (SPS) of Atosiban, Mpa1-D-Tyr(OEt)-Ile-Thr-Asn-Cys6-Pro-Orn-Gly-NH2 cyclic 1,6 disulfide, the only clinically used oxytocin receptor antagonist. The conditions have been selected for the closure of the disulfide bond (S–S) in the Atosiban molecule both in the solution and solid phase with the minimal formation of by-products. A comparative assessment of the formation of the S–S bond was carried out under various conditions. The formation of by-products during the closure of the disulfide bond has been studied both in solution and on the polymer support. The developed technique allows for the synthesis of Atosiban on an enlarged scale (10–20 mmol) involving the cyclization of a protected intermediate with the formation of the S–S bond during solid-phase synthesis with the minimal formation of by-products.

Facile template free approach for the large-scale solid phase synthesis of nanocrystalline XIn2S4 (X = Cd/Zn) and its photocatalytic performance for H2 evolution

2020 ◽  
Vol 44 (23) ◽  
pp. 9634-9646 ◽  
Author(s):  
Sonali D. Naik ◽  
Sanjay K. Apte ◽  
Sunil N. Garaje ◽  
Yogesh A. Sethi ◽  
Manish D. Shinde ◽  
...  
Keyword(s):  
Large Scale ◽  
Photocatalytic Performance ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
H2 Evolution ◽  
Phase Synthesis ◽  
Template Free

Nanostructured CdIn2S4 and ZnIn2S4 with unique morphologies can be synthesized using this method which is simple and easy to operate.

Design, construction and application of an automated large scale solid phase peptide synthesizer: Large scale preparation of vasopressin analogs

Peptides ◽  
1988 ◽  
pp. 204-207
Author(s):  
Martin S. Edelstein ◽  
John L. Hughes ◽  
Pradip K. Bhatnagar ◽  
Jonathan E. Foster ◽  
Kenneth D. Tubman ◽  
...  
Keyword(s):  
Large Scale ◽  
Solid Phase ◽  
Large Scale Preparation ◽  
Scale Preparation ◽  
Design Construction
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