Synthesis, Structure and Characterization of a Series of Transition Metal Complexes with Tripodal Polyimidazole Ligand

2005 ◽  
Vol 23 (2) ◽  
pp. 132-136 ◽  
Author(s):  
Ren Yan-Wei ◽  
Wu Ai-Zhi ◽  
Li Jun ◽  
Zhang Feng-Xing ◽  
Zhang Jin-Hua
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes

scholarly journals Synthesis and Characterization of Transition Metal Complexes with 2,2'-[(Propylene-1,3-diyldioxy)bis(nitrilomethylidyne)]diphenol

2013 ◽  
Vol 25 (16) ◽  
pp. 9362-9364
Author(s):  
Feng-Ying Chai ◽  
Xin-Ying Zhang ◽  
Meng-Meng Zhao ◽  
Zheng-Kun Wang ◽  
Jiao-Long Meng ◽  
...  
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Synthesis And Characterization

scholarly journals Characterization of reactive organometallic species via MicroED

2019 ◽  
Author(s):  
Christopher Jones ◽  
Matthew Asay ◽  
Lee Joon Kim ◽  
Jack Kleinsasser ◽  
Ambarneil Saha ◽  
...  
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Cryogenic Cooling ◽  
Structural Determination ◽  
X Ray ◽  
X Ray Crystallography ◽  
Diamagnetic Transition

Here we apply microcrystal electron diffraction (MicroED) to the structural determination of transition metal complexes. We find that the simultaneous use of 300 keV electrons, very low electron doses, and an ultra-sensitive camera allows for the collection of data without cryogenic cooling of the stage. This technique reveals the first crystal structures of the classic zirconocene hydride, colloquially known as “Schwartz’s reagent”, a novel Pd(II) complex not amenable to solution-state NMR or X-ray crystallography, and five other paramagnetic or diamagnetic transition metal complexes.

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