An Automatic Sample Changer for Nuclear Activation Analysis

Author(s):  
F. Cosmi ◽  
V. F. Romano ◽  
L. F. Bellido
2006 ◽  
Vol 71 (7) ◽  
pp. 1042-1050
Author(s):  
Manju Tandon ◽  
Piyush Kumar ◽  
Haiyan Xia ◽  
Lili Wang ◽  
Leonard I. Wiebe

A rapid PCB-screening protocol, based on a combination of extraction techniques and instrumental nuclear activation analysis (INAA), required water soluble brominated internal standard that undergoes facile hydrolysis to a lipophilic brominated counterpart. Bromophenyl glucuronic acids 2, 3, 7 were synthesized for this application. Glucuronic acids 2 and 3 were prepared by bromination of phenyl β-D-glucopyranosiduronic acid in 81 and 54%, respectively, whereas compound 7 was prepared by coupling methyl 2,3,4-tri-O-acetyl-α-D-glucopyranosyluronate bromide (5) with 2,4,6-tribromophenol. Incubation with β-glucuronidase indicated that tribromophenyl derivative 7 is an excellent substrate, with near quantitative conversion to tribromophenol within seconds of incubation with the enzyme.


Maturitas ◽  
1992 ◽  
Vol 15 (3) ◽  
pp. 256
Author(s):  
J. Kalef-Ezra ◽  
D. Glaros ◽  
G. Klouvas ◽  
J. Hatzikonstantinou ◽  
A. Karantanas ◽  
...  

1992 ◽  
Vol 65 (773) ◽  
pp. 417-420 ◽  
Author(s):  
J. Kalef-Ezra ◽  
D. Glaros ◽  
G. Klouvas ◽  
J. Hatzikonstantinou ◽  
A. Karantanas ◽  
...  

2018 ◽  
Vol 315 (3) ◽  
pp. 689-694
Author(s):  
Aimoré Dutra Neto ◽  
Maria Angela de B. C. Menezes ◽  
Ana Clara Oliveira Pelaes ◽  
Radojko Jaćimović

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