Regulation on the synthesis temperature and optical properties of SmBO3 prepared by chloride fluxes assisted the solid state reaction method

The synthesis of aluminum titanate solid solution (Al2(1-x)MgxTi1+xO5, x=0, 0.1, 0.2) powders was realized by solid state reaction method using fine commercial α-Al2O3, TiO2 and MgO powders as raw materials. The effect of the introduced amount of MgO on the phase formation of aluminum titanate solid solution was investigated by XRD following the phase evolution. It was revealed that the introduction of MgO strongly affects the formation of Al2(1-x)MgxTi(1+x)O5 solid solution. The easily formed MgTi2O5 acts as the nucleus prompting the formation and lowering the synthesis temperature. The microstructure and properties of the solid solution ceramics were also studied by SEM and measuring the fracture strength and the thermal expansion coefficient.

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Structural and optical properties of BaSnO3 ceramics by solid state reaction method

Materials Today Proceedings ◽

10.1016/j.matpr.2021.04.429 ◽

2021 ◽

Author(s):

M. Asisi Janifer ◽

S. Anand ◽

C. Joseph Prabagar ◽

S. Pauline

Keyword(s):

Optical Properties ◽

Solid State ◽

Solid State Reaction ◽

Solid State Reaction Method ◽

Structural And Optical Properties ◽

Reaction Method

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Studies on structural, dielectric and optical properties of (Ba0.95Ca0.05)1−x(Ti0.8Sn0.2)1−xNaxNbxO3 lead-free ceramics

RSC Advances ◽

10.1039/d1ra00952d ◽

2021 ◽

Vol 11 (24) ◽

pp. 14504-14512

Author(s):

H. Slimi ◽

A. Oueslati ◽

A. Aydi

Keyword(s):

Optical Properties ◽

Solid State ◽

Solid State Reaction ◽

Solid State Reaction Method ◽

Lead Free ◽

Reaction Method ◽

Lead Free Ceramics ◽

Dielectric And Optical Properties

(Ba0.95Ca0.05)1−x(Ti0.8Sn0.2)1−xNaxNbxO3 (BCNTSNO3) lead-free ceramics with compositions (x = 0.75, 0.8 and 0.85) were synthesized through the traditional solid-state reaction method.

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Effect of La addition on structural, magnetic and optical properties of multiferroic YFeO3 nanopowders fabricated by low-temperature solid-state reaction method

2020 6th International Conference on Mechanical Engineering and Automation Science (ICMEAS) ◽

10.1109/icmeas51739.2020.00052 ◽

2020 ◽

Author(s):

Meng Wang ◽

Shengsheng Zhao ◽

Xiaolong Zhang ◽

Changwei Huang ◽

Yi Zhu

Keyword(s):

Optical Properties ◽

Solid State ◽

Low Temperature ◽

Solid State Reaction ◽

Solid State Reaction Method ◽

Reaction Method ◽

La Addition

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Solid-State Reaction Synthesis and Mechanism of Lithium Silicates

Materials Science Forum ◽

10.4028/www.scientific.net/msf.654-656.2006 ◽

2010 ◽

Vol 654-656 ◽

pp. 2006-2009 ◽

Cited By ~ 1

Author(s):

Tao Tang ◽

Huo Gen Huang ◽

De Li Luo

Keyword(s):

Solid State ◽

Solid State Reaction ◽

Solid State Reaction Method ◽

Synthesis Temperature ◽

Molar Ratio ◽

Lithium Silicate ◽

Reaction Method ◽

Lithium Silicates ◽

Selection For ◽

Tritium Breeding Materials

Lithium-based ceramics have been recognized as promising tritium breeding-materials for D-T fusion reactor blankets. Lithium silicates, Li4SiO4 and Li2SiO3, are recommended by many ITER research teams as the first selection for the solid tritium breeder. The solid-state reaction method is the most important way to synthesize lithium silicates. In present study, the processes of solid-sate reaction between amorphous silica and Li2CO3 powders was investigaed by TGA/DSC; the lithium silicate powders were synthesized at 700~900°C with different Li:Si molar ratio using solid-state reaction method. The optimized synthesis temperature and the solid-state reaction mechanism were derived on the base of experimental results.

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