Antibacterial, antibiofilm and antioxidant screening of copper(II)-complexes with some S-alkyl derivatives of thiosalicylic acid. Crystal structure of the binuclear copper(II)-complex with S-propyl derivative of thiosalicylic acid

2017 ◽  
Vol 1128 ◽  
pp. 330-337 ◽  
Author(s):  
Andriana M. Bukonjić ◽  
Dušan Lj. Tomović ◽  
Miloš V. Nikolić ◽  
Marina Ž. Mijajlović ◽  
Verica V. Jevtić ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Binuclear Copper ◽  
Acid Crystal ◽  
Thiosalicylic Acid ◽  
Alkyl Derivatives ◽  
Derivatives Of

Cytotoxicity of copper(II)-complexes with some S-alkyl derivatives of thiosalicylic acid. Crystal structure of the binuclear copper(II)-complex with S-ethyl derivative of thiosalicylic acid

2016 ◽  
Vol 1116 ◽  
pp. 264-271 ◽  
Author(s):  
Miloš V. Nikolić ◽  
Marina Ž. Mijajlović ◽  
Verica V. Jevtić ◽  
Zoran R. Ratković ◽  
Slađana B. Novaković ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Binuclear Copper ◽  
Acid Crystal ◽  
Thiosalicylic Acid ◽  
Alkyl Derivatives ◽  
Derivatives Of

scholarly journals Synthesis and Characterization of Platinum (IV) complexes with S-alkyl Derivatives of Thiosalicylic Acid and the Crystal Structure of the S-butyl Derivative of Thiosalicylic Acid

2017 ◽  
Vol 18 (3) ◽  
pp. 195-201 ◽  
Author(s):  
Marina Z. Mijajlovic ◽  
Milos V. Nikolic ◽  
Dusan Lj. Tomovic ◽  
Andriana M. Bukonjic ◽  
Aleksandar Kocovic ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Water System ◽  
13C Nmr Spectroscopy ◽  
Monoclinic Crystal ◽  
1H And 13C Nmr ◽  
X Ray ◽  
Thiosalicylic Acid ◽  
Alkyl Derivatives ◽  
Derivatives Of

Abstract New platinum(IV)-complexes with S-alkyl derivatives of thiosalicylic acid (alkyl = benzyl-(L1), methyl-(L2), ethyl-(L3), propyl-(L4), butyl-(L5)) have been synthesized and characterized by microanalysis, infrared spectroscopy, and 1H and 13C NMR spectroscopy. Th e bidentate S,O ligand precursor, the S-butyl derivative of thiosalicylic acid (S-bu-thiosal), was prepared, and its crystal structure was determined. Single crystals suitable for X-ray measurements were obtained by slow crystallization from a DMSO-water system. S-bu-thiosal crystallized in a P21/c space group of a monoclinic crystal system with a = 8.0732 (3) Å, b = 19.6769 (4) Å, c = 8.2291 (3) Å and Z = 4. S-bu-thiosal also has a coplanar geometry.

2,3,4,6-tetra-O-Acetyl-D-Gluconic Acid: Crystal Structure and Application in the Synthesis of N-(D-gluconyl) Derivatives of D-Glucosamine

2014 ◽  
Vol 33 (1) ◽  
pp. 33-47 ◽  
Author(s):  
Monika Norkowska ◽  
Henryk Myszka ◽  
Magdalena Cyman ◽  
Daria Grzywacz ◽  
Damian Trzybiński ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Gluconic Acid ◽  
Acid Crystal ◽  
Derivatives Of

scholarly journals Alkyl chloro, dialkyl and mixed alkyl derivatives of imido(pentamethylcyclopentadienyl) tantalum(V). X-ray crystal structure of [TaCp*Cp′Cl{N(2,6-Me2C6H3)}], (Cp′=η5-C5H4SiMe3]

1998 ◽  
Vol 554 (2) ◽  
pp. 185-194 ◽  
Author(s):  
Aurora Castro ◽  
Mikhail V Galakhov ◽  
Manuel Gómez ◽  
Pilar Gómez-Sal ◽  
Avelino Martı́n ◽  
...  
Keyword(s):  
Crystal Structure ◽  
X Ray ◽  
Alkyl Derivatives ◽  
Derivatives Of

scholarly journals Synthesis and Characterization of Zinc(II)-Complexes with S-Alkyl Derivatives of Thiosalicylic Acid

2018 ◽  
Vol 19 (2) ◽  
pp. 113-117 ◽  
Author(s):  
Milos V. Nikolic ◽  
Marina Z. Mijajlovic ◽  
Dusan Lj. Tomovic ◽  
Andriana M. Bukonjic ◽  
Verica V. Jevtic ◽  
...  
Keyword(s):  
Nmr Spectra ◽  
Ethanol Solution ◽  
Alkyl Halides ◽  
Synthesis And Characterization ◽  
Direct Reaction ◽  
Thiosalicylic Acid ◽  
Alkyl Derivatives ◽  
Derivatives Of ◽  
C Nmr

Abstract New zinc(II)-complexes with S-alkyl derivatives of thiosalicylic acid (alkyl = benzyl-(L1), methyl-(L2), ethyl-(L3), propyl-(L4), butyl-(L5)) have been synthesized and characterized by elemental microanalysis, IR spectroscopy, and 1H and 13C NMR spectroscopy. The S-alkyl derivatives of thiosalicylic acid were prepared by alkylation of thiosalicylic acid by adding alkyl halides to an alkaline water-ethanol solution, while the corresponding zinc(II)-complexes were obtained via the direct reaction of ZnCl2 with S-alkyl derivatives of thiosalicylic acid in water. Based on the microanalysis results and the IR and NMR spectra of the S-alkyl derivatives of thiosalicylic acid and the corresponding zinc(II)-complexes, we concluded that the ligands are bidentately coordinated to the zinc(II)-ion.

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