Synthesis and characterization of a new zero-dimensional organic-inorganic hybrid material based on antimony

2021 ◽  
pp. 132012
Author(s):  
Imen Tlili ◽  
Rim Essalhi ◽  
George Mousdi ◽  
Mohammed S.M. Abdelbaky ◽  
Slaheddine Chaabouni
2011 ◽  
Vol 130-134 ◽  
pp. 410-413 ◽  
Author(s):  
Bao Hui Li ◽  
Bao Juan Tian

In this paper a novel hybrid organic–inorganic amino hybrid material monolithic column for capillary electro chromatography (CEC) is preparation and characterization. The amido hybrid material monolithic column was prepared in situ co-condensation of tetraethoxysilane (TEOS) with 3-aminoproplytriethoxysilane (3-APTES) via sol-gel procedure. The all kinds of factors that effect the morphology of monolith column were investigated. The results showed that the structure of monolithic column could be adjusted easily through altering the composition of sol solution.


2018 ◽  
Vol 1155 ◽  
pp. 536-547 ◽  
Author(s):  
Mohamed Saber Lassoued ◽  
Mohammed S.M. Abdelbaky ◽  
Abdelmajid Lassoued ◽  
Salah Ammar ◽  
Abdellatif Gadri ◽  
...  

2003 ◽  
Vol 15 (25) ◽  
pp. 4705-4708 ◽  
Author(s):  
Z. Y. Cheng ◽  
B. X. Gao ◽  
M. L. Pang ◽  
S. Y. Wang ◽  
Y. C. Han ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
Hela Ferjani ◽  
Habib Boughzala ◽  
Ahmed Driss

The title compound is an organic-inorganic hybrid material. The single crystal X-ray diffraction investigation reveals that the studied compound crystallizes in the orthorhombic system, space group Pbca with the following lattice parameters:  (4) Å,  (3) Å,  (6) Å, and . The crystal lattice is composed of a discrete anion surrounded by piperazinium cations, chlorine anions, and water molecules. Complex hydrogen bonding interactions between , , organic cations, and water molecules form a three-dimensional network. Room temperature IR, Raman spectroscopy, and optical absorption of the title compound were recorded and analysed. The observed crystal morphology was compared to the simulated one using the Bravais-Friedel, Donnay-Harker model.


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