The preparation and characterization of seven-coordinate tin(IV) complexes of the 2,6-diacetylpyridine Schiff bases of S-alkyl/aryl-dithiocarbazates and the X-ray crystal structure of the [Sn(dapsme)I2] complex (dapsme=doubly deprotonated form of the 2,6-diacetylpyridine Schiff base of S-methyldithiocarbazate)

Polyhedron ◽  
2004 ◽  
Vol 23 (11) ◽  
pp. 2037-2043 ◽  
Author(s):  
Mohammad Akbar Ali ◽  
Aminul Huq Mirza ◽  
Ai Ling Tan ◽  
Lim Kok Wei ◽  
Paul V Bernhardt
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Schiff Bases ◽  
Deprotonated Form ◽  
Alkyl Aryl ◽  
X Ray

The Electrochemical Synthesis of Neutral Zinc(II) Complexes of Schiff Base Ligands: The Crystal Structure of Bis[N-(4-methylphenyl)salicylaldiminato]zinc(II)

1988 ◽  
Vol 43 (5) ◽  
pp. 611-615 ◽  
Author(s):  
T. Sogo ◽  
J. Romero ◽  
A. Sousa ◽  
A. de Blas ◽  
M. L. Durán ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Schiff Bases ◽  
Electrochemical Synthesis ◽  
Chemical Properties ◽  
Zinc Atom ◽  
Schiff Base Ligands ◽  
Space Group ◽  
X Ray ◽  
Physico Chemical

Abstract The electrochemical synthesis and physico-chemical properties of neutral zinc(II) complexes of bidentate Schiff bases derived from salicylaldehydes are presented together with the X-ray structure of bis[N-(4-methylphenyl)salicylaldiminato]zinc(II). The crystal is monoclinic, a = 21.877(3), b = 8.801(2), c = 12.027(5) Å, β = 96.55(3)°, space group C2/c. The complex is a monomer, and the zinc atom is tetrahedrally coordinated.

X-ray Crystal Structure of the N-(2-hydroxy-1-naphthalidene)phenylglycine Schiff Base. Synthesis and Characterization of its Transition Metal Complexes

2006 ◽  
Vol 31 (5) ◽  
pp. 580-585 ◽  
Author(s):  
Kalagouda B. Gudasi ◽  
Manjula S. Patil ◽  
Ramesh S. Vadavi ◽  
Rashmi V. Shenoy ◽  
Siddappa A. Patil ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Synthesis And Characterization ◽  
X Ray

Synthesis and characterization of ferrocene-containing new schiff base complexes. The X-ray crystal structure of (C10H6N2)CNNCHFc

Polyhedron ◽  
1992 ◽  
Vol 11 (15) ◽  
pp. 1917-1922 ◽  
Author(s):  
Xia Xu-Bing ◽  
Duan Chun-Ying ◽  
Zhu Long-Gen ◽  
You Xiao-Zeng ◽  
Yang Yao ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Schiff Base Complexes ◽  
Synthesis And Characterization ◽  
X Ray

Synthesis and structural characterization of m-terphenyl Schiff base ligands and their aluminum complexes

2004 ◽  
Vol 82 (9) ◽  
pp. 1346-1352 ◽  
Author(s):  
Diane A Dickie ◽  
Hanifa Jalali ◽  
Rahul G Samant ◽  
Michael C Jennings ◽  
Jason AC Clyburne
Keyword(s):  
Schiff Base ◽  
Schiff Bases ◽  
Structural Characterization ◽  
Condensation Reaction ◽  
Schiff Base Ligands ◽  
X Ray ◽  
X Ray Crystallography ◽  
Aluminum Complexes

2,4,6-Triphenylbenzaldehyde 1 undergoes a condensation reaction with 2-aminophenol to give N-(2′,4′,6′-triphenylbenzylidene)-2-iminophenol (TPIP) 2. The imine 2 can be reduced with NaBH4 in ethanol to form N-(2′,4′,6′-triphenylbenzyl)-2-aminophenol (TPAP) 3. Addition of trimethylaluminum to 2 or 3 results in the formation of the complexes TPIP-AlMe2·AlMe3 (4) or TPAP-AlMe2 (5). Compounds 2, 3, and 4 have been crystallographically characterized.Key words: N,O ligands, aluminum, m-terphenyl, Schiff bases, X-ray crystallography.

scholarly journals Synthesis and characterization of three new asymmetric Schiff bases and X-ray crystal structure of [H 2 cd3-OMesalen] ligand

2010 ◽  
Author(s):  
Saeed Menati ◽  
Hadi Rudbari ◽  
Giuseppe Bruno ◽  
A. Taeb ◽  
A. Kakanejadi ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Bases ◽  
Synthesis And Characterization ◽  
X Ray

Crystal structure and characterization of a co-product in the syntheses of a Schiff base give evidence of its zwitterionic nature in the solid state

2022 ◽  
Author(s):  
María Rosa Rodríguez ◽  
Gustavo Espino ◽  
Oscar E. Piro ◽  
Gustavo A. Echeverría ◽  
Beatriz Susana Parajón Costa ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Schiff Base ◽  
Solid State ◽  
X Ray

During the syntheses of the Schiff base 2-methoxy-6-{[(tiophen-2-methyl)imino]methylphenol (o-HVATPNH2), a co-´product was isolated and characterized. The crystal structure of this molecule, 4,10-dimethoxy-13-(thiophen-2-ylmethyl)-6,12-dihydro-6,12-epiminodibenzo[b,f][1,5]dioxocane, namely (o-VA)2TPNH2 for short, was determined by X-ray...

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