One-pot synthesis of optically active cyanohydrin acetates from aldehydes via lipase-catalyzed kinetic resolution coupled with in situ formation and racemization of cyanohydrins

1992 ◽  
Vol 57 (21) ◽  
pp. 5643-5649 ◽  
Author(s):  
Minoru Inagaki ◽  
Jun Hiratake ◽  
Takaaki Nishioka ◽  
Junichi Oda
Keyword(s):  
Kinetic Resolution ◽  
Optically Active ◽  
One Pot ◽  
One Pot Synthesis ◽  
In Situ Formation

ChemInform Abstract: Lipase-Catalyzed Kinetic Resolution with in situ Racemization: One-Pot Synthesis of Optically Active Cyanohydrin Acetates from Aldehydes.

ChemInform ◽  
2010 ◽  
Vol 23 (12) ◽  
pp. no-no
Author(s):  
M. INAGAKI ◽  
J. HIRATAKE ◽  
T. NISHIOKA ◽  
J. ODA
Keyword(s):  
Kinetic Resolution ◽  
Optically Active ◽  
One Pot ◽  
One Pot Synthesis

Lipase-catalyzed kinetic resolution with in situ racemization: one-pot synthesis of optically active cyanohydrin acetates from aldehydes

1991 ◽  
Vol 113 (24) ◽  
pp. 9360-9361 ◽  
Author(s):  
Minoru Inagaki ◽  
Jun Hiratake ◽  
Takaaki Nishioka ◽  
Junichi Oda
Keyword(s):  
Kinetic Resolution ◽  
Optically Active ◽  
One Pot ◽  
One Pot Synthesis

One-Pot Synthesis of Optically Active Cyanohydrin Acetates from Aldehydes via Quinidine-Catalyzed Transhydrocyanation Coupled with Lipase-Catalyzed Kinetic Resolution in Organic Solvent

1992 ◽  
Vol 65 (1) ◽  
pp. 111-120 ◽  
Author(s):  
Minoru Inagaki ◽  
Akihiko Hatanaka ◽  
Mitsuo Mimura ◽  
Jun Hiratake ◽  
Takaaki Nishioka ◽  
...  
Keyword(s):  
Organic Solvent ◽  
Kinetic Resolution ◽  
Optically Active ◽  
One Pot ◽  
One Pot Synthesis

ChemInform Abstract: One-Pot Synthesis of Optically Active Cyanohydrin Acetates from Aldehydes via Quinidine-Catalyzed Transhydrocyanation Coupled with Lipase-Catalyzed Kinetic Resolution in Organic Solvent.

ChemInform ◽  
2010 ◽  
Vol 23 (17) ◽  
pp. no-no
Author(s):  
M. INAGAKI ◽  
A. HATANAKA ◽  
M. MIMURA ◽  
J. HIRATAKE ◽  
T. NISHIOKA ◽  
...  
Keyword(s):  
Organic Solvent ◽  
Kinetic Resolution ◽  
Optically Active ◽  
One Pot ◽  
One Pot Synthesis

Expeditious Scalable Catalyst-Free One-Pot Synthesis of 4-Alkoxy-5-amino-3-methylthiophene-2-carbonitriles via Sequential Reactions­ of Lithiated Alkoxyallenes with Isothiocyanates and 2-Bromoacetonitrile

Synthesis ◽  
2018 ◽  
Vol 50 (09) ◽  
pp. 1891-1900 ◽  
Author(s):  
Nina Nedolya ◽  
Boris Trofimov ◽  
Olga Tarasova ◽  
Alexander Albanov
Keyword(s):  
Intramolecular Cyclization ◽  
Thiophene Ring ◽  
One Pot ◽  
One Pot Synthesis ◽  
Convenient Approach ◽  
Reaction Proceeds ◽  
Sequential Addition ◽  
In Situ Formation ◽  
Cyano Groups

A synthetically simple and convenient approach to tetrasubstituted thiophenes with rare combination of the alkoxy, amino, and cyano groups has been developed. The assembly of polyfunctionalized thiophene ring is implemented in one preparative step by sequential addition of isothiocyanate and 2-bromoacetonitrile to the lithiated (with n-BuLi) alkoxyallene. The reaction proceeds through in situ formation and intramolecular cyclization of cyanomethyl 2-alkoxy-N-buta-2,3-dienimidothioate (1-aza-1,3,4-triene).

Lipase-Catalyzed Domino Kinetic Resolution/Intramolecular Diels—Alder Reaction: One-Pot Synthesis of Optically Active 7-Oxabicyclo[2.2.1]heptenes from Furfuryl Alcohols and β-Substituted Acrylic Acids.

ChemInform ◽  
2003 ◽  
Vol 34 (6) ◽  
Author(s):  
Shuji Akai ◽  
Tadaatsu Naka ◽  
Sohei Omura ◽  
Kouichi Tanimoto ◽  
Masashi Imanishi ◽  
...  
Keyword(s):  
Kinetic Resolution ◽  
Alder Reaction ◽  
Optically Active ◽  
Diels Alder ◽  
One Pot ◽  
One Pot Synthesis ◽  
Diels Alder Reaction ◽  
Acrylic Acids

One-pot synthesis of Ni(II) and Fe(III) complexes: In situ formation of 2-pyridinemethanol from 2-pyridinecarboxaldehyde

2011 ◽  
Vol 14 (6) ◽  
pp. 877-881 ◽  
Author(s):  
Ji-Ping Sun ◽  
Li-Cun Li ◽  
Xiang-Jun Zheng
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
In Situ Formation

scholarly journals One-Pot Synthesis of 2,5-Disubstituted Furans through In Situ Formation of Allenes and Enolization Cascade

2019 ◽  
Vol 2019 (48) ◽  
pp. 7870-7873 ◽  
Author(s):  
Yann Bernhard ◽  
Joachim Gilbert ◽  
Till Bousquet ◽  
Audrey Favrelle-Huret ◽  
Philippe Zinck ◽  
...  
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
In Situ Formation
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