Single orientation in poly(diacetylene) films for nonlinear optics. Molecular epitaxy of 1,6-bis(9-carbazolyl)-2,4-hexadiyne on organic crystals

1991 ◽  
Vol 24 (9) ◽  
pp. 2622-2628 ◽  
Author(s):  
J. Le Moigne ◽  
F. Kajzar ◽  
A. Thierry
1990 ◽  
Vol 68 (1) ◽  
pp. 8-13 ◽  
Author(s):  
P. Andreazza ◽  
F. Lefaucheux ◽  
M. C. Robert ◽  
D. Josse ◽  
J. Zyss

ChemInform ◽  
1988 ◽  
Vol 19 (43) ◽  
Author(s):  
D. PUGH ◽  
J. N. SHERWOOD

Author(s):  
E. Knapek ◽  
H. Formanek ◽  
G. Lefranc ◽  
I. Dietrich

A few years ago results on cryoprotection of L-valine were reported, where the values of the critical fluence De i.e, the electron exposure which decreases the intensity of the diffraction reflections by a factor e, amounted to the order of 2000 + 1000 e/nm2. In the meantime a discrepancy arose, since several groups published De values between 100 e/nm2 and 1200 e/nm2 /1 - 4/. This disagreement and particularly the wide spread of the results induced us to investigate more thoroughly the behaviour of organic crystals at very low temperatures during electron irradiation.For this purpose large L-valine crystals with homogenuous thickness were deposited on holey carbon films, thin carbon films or Au-coated holey carbon films. These specimens were cooled down to nearly liquid helium temperature in an electron microscope with a superconducting lens system and irradiated with 200 keU-electrons. The progress of radiation damage under different preparation conditions has been observed with series of electron diffraction patterns and direct images of extinction contours.


Author(s):  
K. Shi rota ◽  
A. Yonezawa ◽  
K. Shibatomi ◽  
T. Yanaka

As is well known, it is not so easy to operate a conventional transmission electron microscope for observation of magnetic materials. The reason is that the instrument requires re-alignment of the axis and re-correction of astigmatism after each specimen shift, as the lens field is greatly disturbed by the specimen. With a conventional electron microscope, furthermore, it is impossible to observe magnetic domains, because the specimen is magnetized to single orientation by the lens field. The above mentioned facts are due to the specimen usually being in the lens field. Thus, special techniques or systems are usually required for magnetic material observation (especially magnetic domain observation), for example, the technique to switch off the objective lens current and Lorentz microscopy. But these cannot give high image quality and wide magnification range, and furthermore Lorentz microscopy is very complicated.


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