Activation of an aliphatic carbon-hydrogen bond at room temperature. Conversion on a cluster of a stable .sigma.-bonded alkyl group to a .mu.2-alkylidene ligand. Synthesis and crystal structure determination of HOs3(6-CH2C5H3N-2-C(H):N-iso-Pr)(CO)9 and H2Os3(6-CHC5H3N-2-C(H):N-iso-Pr)(CO)8

1988 ◽  
Vol 7 (7) ◽  
pp. 1565-1572 ◽  
Author(s):  
Robert. Zoet ◽  
Gerard. Van Koten ◽  
Kees. Vrieze ◽  
Jacob. Jansen ◽  
Kees. Goubitz ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bond ◽  
Structure Determination ◽  
Alkyl Group ◽  
Room Temperature ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure ◽  
Aliphatic Carbon ◽  
Ligand Synthesis

First crystal-structure determination of natural lansfordite, MgCO3·5H2O

2017 ◽  
Vol 81 (5) ◽  
pp. 1063-1071 ◽  
Author(s):  
Fabrizio Nestola ◽  
Anatoly V. Kasatkin ◽  
Sergey S. Potapov ◽  
Olga YA. Chervyatsova ◽  
Arianna Lanza
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bond ◽  
Single Crystal ◽  
Structure Determination ◽  
Room Temperature ◽  
Crystal Structure Determination ◽  
Hydrogen Atoms ◽  
Synthetic Analogues ◽  
X Ray

AbstractThis study presents the first crystal-structure determination of natural MgCO3·5H2O, mineral lansfordite, in comparison with previous structural works performed on synthetic analogues. A new prototype single-crystal X-ray diffractometer allowed us to measure an extremely small crystal (i.e. 0.020 mm × 0.010 mm × 0.005 mm) and refine anisotropically all non-hydrogen atoms in the structure and provide a robust hydrogen-bond arrangement. Our new data confirm that natural lansfordite can be stable for several months at room temperature, in contrast with previous works, which reported that such a mineral could be stable only below 10°C.

Synthesis and crystal structure determination of a new misfit compound: [(EuS)1.5]1.15NbS2

1998 ◽  
Vol 1 (4) ◽  
pp. 269-276
Author(s):  
Laurent Cario ◽  
Alain Meerschaut ◽  
Catherine Deudon ◽  
Jean Rouxel
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure

ChemInform Abstract: Flux Synthesis and Crystal Structure Determination of the Colored Skutterudite Ir2Sn3Se3.

ChemInform ◽  
2015 ◽  
Vol 46 (22) ◽  
pp. no-no
Author(s):  
Wenjie Yan ◽  
Florian Pielnhofer ◽  
Samuel A. Tragl ◽  
Richard Weihrich
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure ◽  
Flux Synthesis

Synthesis and Crystal Structure Determination of Hydantoin-l-Proline

2012 ◽  
Vol 42 (9) ◽  
pp. 968-971 ◽  
Author(s):  
Gerzon E. Delgado ◽  
Luis E. Seijas ◽  
Asiloé J. Mora
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure

ChemInform Abstract: SYNTHESIS AND CRYSTAL STRUCTURE DETERMINATION OF A Λ3PΛ5P-PHOSPHORANE OF A NOVEL TYPE

1983 ◽  
Vol 14 (45) ◽  
Author(s):  
H.-M. SCHIEBEL ◽  
R. SCHMUTZLER ◽  
D. SCHOMBURG ◽  
U. WERMUTH
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure

scholarly journals Synthesis and Crystal Structure Determination of a Dimeric Complex of Dimethylammoniumbis(p-tert-butylcatecholato) borate

2020 ◽  
Vol 36 (0) ◽  
pp. 27-29
Author(s):  
Mustafa TOMBUL ◽  
Mutluhan BIYIKOGLU ◽  
Adnan BULUT ◽  
Kutalmis GÜVEN ◽  
Özer ISILAR
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Dimeric Complex ◽  
Synthesis And Crystal Structure

scholarly journals Synthesis and crystal structure determination of YCo1−x Fe x O3 (x = 0, 0.33, 0.5, 0.67 and 1) perovskites

2015 ◽  
Vol 127 (7) ◽  
pp. 1173-1181 ◽  
Author(s):  
S IMITROVSKA-LAZOVA ◽  
S ALEKSOVSKA ◽  
P TZVETKOV
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure

Synthesis and Crystal Structure Determination of (NH4)Ag2AsS4, a Further Chalcopyrite-Type Compound

1993 ◽  
Vol 106 (2) ◽  
pp. 421-426 ◽  
Author(s):  
M. Auernhammer ◽  
H. Effenberger ◽  
E. Irran ◽  
F. Pertlik ◽  
J. Rosenstingl
Keyword(s):  
Crystal Structure ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Synthesis And Crystal Structure ◽  
Type Compound
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