Modelling and experimental validation of ultrasound assisted unseeded batch cooling crystallization ofl-asparagine monohydrate

CrystEngComm ◽  
2016 ◽  
Vol 18 (25) ◽  
pp. 4863-4874 ◽  
Author(s):  
Stutee Bhoi ◽  
Debasis Sarkar
Keyword(s):  
Experimental Validation ◽  
Cooling Crystallization ◽  
Ultrasound Assisted ◽  
Asparagine Monohydrate ◽  
Batch Cooling

Particle engineering by optimization for the unseeded batch cooling crystallization of l-asparagine monohydrate

CrystEngComm ◽  
2017 ◽  
Vol 19 (42) ◽  
pp. 6373-6382 ◽  
Author(s):  
Stutee Bhoi ◽  
Maheswata Lenka ◽  
Debasis Sarkar
Keyword(s):  
Crystallization Process ◽  
Optimization Approach ◽  
Temperature Profiles ◽  
Particle Engineering ◽  
Model Based ◽  
Cooling Crystallization ◽  
Asparagine Monohydrate ◽  
Batch Cooling

A model-based optimization approach is proposed to obtain temperature profiles to achieve the target CSD in a batch cooling crystallization process.

Process Control of Seeded Batch Cooling Crystallization of the Metastable α-Form Glycine Using an In-Situ ATR-FTIR Spectrometer and an In-Situ FBRM Particle Counter

2004 ◽  
Vol 4 (5) ◽  
pp. 949-953 ◽  
Author(s):  
Norihito Doki ◽  
Hiroya Seki ◽  
Kiyoteru Takano ◽  
Haruki Asatani ◽  
Masaaki Yokota ◽  
...  
Keyword(s):  
Process Control ◽  
Particle Counter ◽  
Cooling Crystallization ◽  
Ftir Spectrometer ◽  
Batch Cooling

Optimization of batch cooling crystallization

2004 ◽  
Vol 59 (2) ◽  
pp. 313-327 ◽  
Author(s):  
K.L. Choong ◽  
R. Smith
Keyword(s):  
Cooling Crystallization ◽  
Batch Cooling
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