Exploiting 13C/14N solid-state NMR distance measurements to assign dihedral angles and locate neighboring molecules

2018 ◽  
Vol 54 (49) ◽  
pp. 6376-6379 ◽  
Author(s):  
Giovanna M. Pope ◽  
Ivan Hung ◽  
Zhehong Gan ◽  
Hani Mobarak ◽  
Göran Widmalm ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Natural Abundance ◽  
Dihedral Angles ◽  
Distance Measurements ◽  
Nmr Method

The RESPDOR NMR method rapidly provides multiple 13C/14N distance measurements in natural abundance solids.

scholarly journals Determining carbon–carbon connectivities in natural abundance organic powders using dipolar couplings

2016 ◽  
Vol 52 (55) ◽  
pp. 8565-8568 ◽  
Author(s):  
Myriam Dekhil ◽  
Giulia Mollica ◽  
Tristan Texier Bonniot ◽  
Fabio Ziarelli ◽  
Pierre Thureau ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Natural Abundance ◽  
Dipolar Couplings ◽  
Nmr Method

A solid-state NMR method to establish carbon–carbon connectivities in natural abundance powders.

Thermosetting Mechanism Study of Organosilicon Polymer Containing Carborane by Solid-State NMR Spectroscopy

1999 ◽  
Vol 576 ◽  
Author(s):  
H. Kimura ◽  
K. Okita ◽  
M. Ichitani ◽  
M. Yonezawa ◽  
T. Sugimoto
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Main Chain ◽  
Addition Reaction ◽  
Side Chain ◽  
Mechanism Study ◽  
Nmr Method ◽  
Organosilicon Polymer ◽  
Thermal Stable

ABSTRACTThe thermosetting mechanism of an organosilicon polymer containing carborane has been studied utilizing the 13and 29Si solid-state NMR method. The polymer having C≡C bonds in the main chain and CH═CH2, Si-H bonds, and carborane in the bulky side chain, shows a very highly thermal stability in air by curing. From 13C and 29Si NMR spectra of the polymer, it was found that the intermolecular cross-linking reactions of the polymer was due to (1) the diene reaction between Ph-C≡C and C≡C and (2) the addition reaction between side chain terminal and Ph-C≡C and between CH═CH2 and Si–H, and a very highly thermal stable structure is formed.

A solid-state NMR method to determine domain sizes in multi-component polymer formulations

2015 ◽  
Vol 261 ◽  
pp. 43-48 ◽  
Author(s):  
Judith Schlagnitweit ◽  
Mingxue Tang ◽  
Maria Baias ◽  
Sara Richardson ◽  
Staffan Schantz ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Method

scholarly journals Self-Assembly of E5/PDGFβR in Membranes Studied by Solid-State NMR Distance Measurements

2020 ◽  
Vol 118 (3) ◽  
pp. 210a
Author(s):  
Li Tian ◽  
Stephan L. Grage ◽  
Parvesh Wadhwani ◽  
Anne S. Ulrich
Keyword(s):  
Solid State ◽  
Self Assembly ◽  
Solid State Nmr ◽  
Distance Measurements

scholarly journals Distance Measurements in Multiply Labeled Crystalline Cytidines by Dipolar Recoupling Solid State NMR

1999 ◽  
Vol 103 (20) ◽  
pp. 3890-3903 ◽  
Author(s):  
S. R. Kiihne ◽  
K. B. Geahigan ◽  
N. A. Oyler ◽  
H. Zebroski ◽  
M. A. Mehta ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Distance Measurements ◽  
Dipolar Recoupling

Proton-Detected Solid-State NMR Spectroscopy of Natural-Abundance Peptide and Protein Pharmaceuticals

2009 ◽  
Vol 121 (7) ◽  
pp. 1279-1282 ◽  
Author(s):  
Donghua H. Zhou ◽  
Gautam Shah ◽  
Charles Mullen ◽  
Dennis Sandoz ◽  
Chad M. Rienstra
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Natural Abundance ◽  
Solid State Nmr Spectroscopy ◽  
Protein Pharmaceuticals
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