One-pot synthesis of 4-ethyl 2,3-dimethyl 1-(5-aryl-1,3,4-thiadiazol-2-yl)-5-oxo-2,5-dihydro-1H-pyrrole-2,3,4-tricarboxylate derivatives via intramolecular Wittig reaction

2020 ◽  
Vol 44 (7-8) ◽  
pp. 403-409
Author(s):  
Samin Iravani ◽  
Abbas Ali Esmaeili
Keyword(s):  
Wittig Reaction ◽  
Spectroscopic Methods ◽  
Acetylenic Esters ◽  
One Pot ◽  
Intramolecular Wittig Reaction ◽  
One Pot Synthesis

A facile one-pot synthesis of highly functionalized dialkyl 1-(5-aryl-1,3,4-thiadiazol-2-yl)-4-ethoxy-5-oxo-2,5-dihydro-1 H-pyrrole-2,3-dicarboxylate derivatives via the reaction between acetylenic esters, triphenylphosphine, and ethyl 2-[(5-aryl-1,3,4-thiadiazol-2-yl)amino]-2-oxoacetate is developed. The structure of the products is confirmed by spectroscopic methods.

A facile and regioselective one-pot synthesis of novel pyrazolo[1 $$'$$ ′ ,5 $$'$$ ′ :1,2]pyrrolo[3,4-b]quinoline-2,3-dicarboxylate hybrids via intramolecular Wittig reaction

2017 ◽  
Vol 22 (1) ◽  
pp. 37-46 ◽  
Author(s):  
Tahere Hosseyni Largani ◽  
Gholamhasan Imanzadeh ◽  
Nader Noroozi Pesyan ◽  
Ertan Şahin ◽  
Amir Nasser Shamkhali ◽  
...  
Keyword(s):  
Wittig Reaction ◽  
One Pot ◽  
Intramolecular Wittig Reaction ◽  
One Pot Synthesis

A practical one-pot synthesis of coumarins in aqueous sodium bicarbonate via intramolecular Wittig reaction at room temperature

RSC Advances ◽  
2014 ◽  
Vol 4 (75) ◽  
pp. 39667 ◽  
Author(s):  
Ningaraddi S. Belavagi ◽  
Narahari Deshapande ◽  
Manjunath G. Sunagar ◽  
Imtiyaz Ahmed M. Khazi
Keyword(s):  
Sodium Bicarbonate ◽  
Room Temperature ◽  
Wittig Reaction ◽  
One Pot ◽  
Aqueous Sodium ◽  
Intramolecular Wittig Reaction ◽  
Aqueous Sodium Bicarbonate ◽  
One Pot Synthesis

A one-pot synthesis of trichloromethylated pyrimidines from trichloroacetimidamides and acetylenic esters

2016 ◽  
Vol 57 (16) ◽  
pp. 1733-1735 ◽  
Author(s):  
Issa Yavari ◽  
Alaleh Malekafzali ◽  
Reza Eivazzadeh-Keihan ◽  
Stavroula Skoulika ◽  
Rahman Alivaisi
Keyword(s):  
Acetylenic Esters ◽  
One Pot ◽  
One Pot Synthesis

One-Pot Synthesis of 3-(1,2,3,4-Tetrahydroisoquinolin-1-yl)-isoquinolin-1(2H)-ones by Sequential DEAD-Promoted Oxidative Ugi/Wittig Reaction Starting from Phosphonium Salt Precursors

Synlett ◽  
2021 ◽  
Author(s):  
Long Zhao ◽  
Mao-Lin Yang ◽  
Mei Sun ◽  
Ming-Wu Ding
Keyword(s):  
Wittig Reaction ◽  
Phosphonium Salt ◽  
One Pot ◽  
One Pot Synthesis ◽  
Sequential Reactions

A new one-pot Synthesis of 3-(1,2,3,4-tetrahydroisoquinolin-1-yl)- isoquinolin-1(2H)-ones by DEAD-promoted oxidative Ugi/Wittig reaction was developed. The sequential reactions of (2-carboxybenzyl)triphenylphosphonium salts, isocyanides and N-aryl-1,2,3,4-tetrahydroisoquinolines produced 3-(1,2,3,4-tetrahydroisoquinolin-1-yl)- isoquinolin-1(2H)-ones in moderate to good overall yields in the presence of DEAD and Et3N.

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