Methods of test for aluminium oxide

1986 ◽  
Keyword(s):  
Author(s):  
A.N. Sagredos ◽  
R. Moser

AbstractBased on previous work (7) a method to simultaneously determine vamidothion [I], vamidothion-sulfoxide [II] and vamidothion sulfone [III] in tobacco has been developed. The compounds are extracted with water/acetone/acetic acid from the tobacco, cleansed over an aluminium oxide column and then determined on the gas chromatograph with the specific sulphur detector. Rates of recovery are 70 % - 92 %, the determination level is 0.1 ppm. Mass spectrometry and nuclear magnetic resonance data of vamidothion [I], vamidothion-sulfoxide [ II ] and vamidothion-sulfone [III] are given.


2013 ◽  
Vol 10 (2) ◽  
pp. 26-28
Author(s):  
Ladislav Kyncl ◽  
Robert Cep ◽  
Pavel Novacek ◽  
Jiri Schreier

Abstract This article discusses the test removable ceramic plates during machining with interrupted cut. Tests were performed on a lathe, which was clamped preparation which simulated us the interrupted cut. By changing the number plates mounted in a preparation it was a regular or irregular cut. When with four plates it was regular interrupted cut, the remaining three variants were already irregular cut. It was examined whether it will have the irregular intermittent cutting effect on the insert and possibly how it will change life of inserts during irregular interrupted cut.


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