Determination of microphase structure and scale and scale of mixing in poly-ɛ-caprolactone (PCL)/poly(vinyl chloride) (PVC) blend by high-resolution solid-state 13C-NMR spectroscopy with magic angle spinning and cross polarization

1994 ◽  
Vol 53 (13) ◽  
pp. 1823-1832 ◽  
Author(s):  
S.-Y. Kwak
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
13C Nmr Spectroscopy ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
Poly Vinyl Chloride ◽  
Angle Spinning ◽  
Solid State 13C Nmr

Structural Properties of a Dimeric Phenylcyanamidocopper(I) Complex, [{Cu(PPh3)2(C6H5NCN)}2]

2000 ◽  
Vol 53 (12) ◽  
pp. 971 ◽  
Author(s):  
Eric W. Ainscough ◽  
Andrew M. Brodie ◽  
Peter C. Healy ◽  
Joyce M. Waters
Keyword(s):  
Crystal Structure ◽  
Solid State ◽  
Structural Properties ◽  
Structure Determination ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
X Ray ◽  
Angle Spinning

The X-ray crystal structure determination of bis[-(phenylcyanamido)bis(triphenylphosphine)copper(I)], [{Cu(PPh3)2(C6H5NCN)}2], (1) is reported. The complex has a centrosymmetric dimeric structure with the phenylcyanamide ligands bridging the copper atoms in a -1,3-fashion. The structure is compared with that of the 4-methylphenylcyanamido complex, [{Cu(PPh3)2(4-MeC6H4NCN)}2] (2), and the differences observed in the Cu–P bond lengths compared with changes in the solid state 31P cross-polarization magic-angle spinning (CPMAS) spectra of the two complexes.

Band-Selective1H−13C Cross-Polarization in Fast Magic Angle Spinning Solid-State NMR Spectroscopy

2008 ◽  
Vol 130 (51) ◽  
pp. 17216-17217 ◽  
Author(s):  
Ségolène Laage ◽  
Alessandro Marchetti ◽  
Julien Sein ◽  
Roberta Pierattelli ◽  
Hans Juergen Sass ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

scholarly journals Facile Characterization of Polymer-Supported Reagents Using Cross Polarization Magic Angle Spinning Method in Solid State 13C-NMR

2004 ◽  
Vol 52 (7) ◽  
pp. 864-865
Author(s):  
Kazuaki Shikii ◽  
Hiroko Seki ◽  
Kentaro Yamaguchi ◽  
Wannaporn Disadee ◽  
Toshiko Watanabe ◽  
...  
Keyword(s):  
Solid State ◽  
13C Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
Polymer Supported ◽  
Angle Spinning ◽  
Solid State 13C Nmr
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