scholarly journals Strategies for 1 H‐Detected Dynamic Nuclear Polarization Magic‐Angle Spinning NMR Spectroscopy

2020 ◽  
Vol 26 (68) ◽  
pp. 15852-15854
Author(s):  
Maria Concistré ◽  
Subhradip Paul ◽  
Marina Carravetta ◽  
Ilya Kuprov ◽  
Philip T. F. Williamson
Keyword(s):  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning

2018 ◽  
Vol 130 (25) ◽  
pp. 7580-7584 ◽  
Author(s):  
Kristaps Jaudzems ◽  
Andrea Bertarello ◽  
Sachin R. Chaudhari ◽  
Andrea Pica ◽  
Diane Cala-De Paepe ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Nmr Spectroscopy ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Biomolecular Nmr ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

19 F Magic Angle Spinning Dynamic Nuclear Polarization Enhanced NMR Spectroscopy

2019 ◽  
Vol 58 (22) ◽  
pp. 7249-7253 ◽  
Author(s):  
Jasmine Viger‐Gravel ◽  
Claudia E. Avalos ◽  
Dominik J. Kubicki ◽  
David Gajan ◽  
Moreno Lelli ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

scholarly journals Natural Abundance Oxygen-17 Solid-State NMR of Metal Organic Frameworks Enhanced by Dynamic Nuclear Polarization

2021 ◽  
Author(s):  
Diego Carnevale ◽  
Georges Mouchaham ◽  
Sujing WANG ◽  
Mathieu Baudin ◽  
Christian SERRE ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Metal Organic Frameworks ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Metal Organic ◽  
Angle Spinning

The 17O resonances of Zirconium-oxo clusters in porous Zr carboxylate metal-organic frameworks (MOFs) have been investigated by magic-angle spinning (MAS) NMR spectroscopy enhanced by dynamic nuclear polarization (DNP) at natural...

19 F Magic Angle Spinning Dynamic Nuclear Polarization Enhanced NMR Spectroscopy

2019 ◽  
Vol 131 (22) ◽  
pp. 7327-7331
Author(s):  
Jasmine Viger‐Gravel ◽  
Claudia E. Avalos ◽  
Dominik J. Kubicki ◽  
David Gajan ◽  
Moreno Lelli ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

scholarly journals Dynamic nuclear polarization at 40 kHz magic angle spinning

2016 ◽  
Vol 18 (15) ◽  
pp. 10616-10622 ◽  
Author(s):  
Sachin R. Chaudhari ◽  
Pierrick Berruyer ◽  
David Gajan ◽  
Christian Reiter ◽  
Frank Engelke ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Wide Range ◽  
Angle Spinning

DNP-enhanced solid-state NMR spectroscopy is shown to maintain performance over a wide range of sample spinning rates up to 40 kHz.

scholarly journals Instrumentation for cryogenic magic angle spinning dynamic nuclear polarization using 90 L of liquid nitrogen per day

2017 ◽  
Vol 283 ◽  
pp. 71-78 ◽  
Author(s):  
Brice J. Albert ◽  
Seong Ho Pahng ◽  
Nicholas Alaniva ◽  
Erika L. Sesti ◽  
Peter W. Rand ◽  
...  
Keyword(s):  
Liquid Nitrogen ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

2016 ◽  
Vol 52 (32) ◽  
pp. 5531-5533 ◽  
Author(s):  
Eric Besson ◽  
Fabio Ziarelli ◽  
Emily Bloch ◽  
Guillaume Gerbaud ◽  
Séverine Queyroy ◽  
...  
Keyword(s):  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
High Field ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Hybrid Silica ◽  
Silica Materials ◽  
Field Dynamic ◽  
Angle Spinning

Hybrid silica materials with wall-embedded nitroxides efficiently polarize impregnated substrates in high-field dynamic nuclear polarization magic-angle spinning solid-state NMR experiments.

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