ChemInform Abstract: High-Pressure High-Temperature Synthesis and Crystal Structure of the Isotypic Rare Earth (RE)-Thioborate-Sulfides RE9[BS3]2 [BS4]3S3, (RE: Dy-Lu).

ChemInform ◽  
2011 ◽  
Vol 42 (22) ◽  
pp. no-no
Author(s):  
Marija Borna ◽  
Jens Hunger ◽  
Alim Ormeci ◽  
Dirk Zahn ◽  
Ulrich Burkhardt ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Rare Earth ◽  
High Temperature ◽  
Temperature Synthesis ◽  
Synthesis And Crystal Structure ◽  
High Temperature Synthesis ◽  
High Pressure High Temperature

scholarly journals High-pressure Synthesis and Crystal Structure of the Borate Sc3B5O12

2009 ◽  
Vol 64 (11-12) ◽  
pp. 1339-1344 ◽  
Author(s):  
Stephanie C. Neumair ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Rare Earth ◽  
High Temperature ◽  
Single Crystal ◽  
Structure Determination ◽  
Synthesis And Crystal Structure ◽  
High Pressure High Temperature ◽  
Rare Earth Borate ◽  
Pressure Synthesis

The rare-earth borate Sc3B5O12 was synthesized under high-pressure / high-temperature conditions of 6 GPa and 1100 °C in a Walker-type multianvil apparatus. The single-crystal structure determination revealed an isotypy to RE3B5O12 (RE = Er-Lu). Sc3B5O12 crystallizes in the rare space group Pmna (Z = 4) with the parameters a = 1245.4(3), b = 443.46(9), c = 1222.1(2) pm, V = 0.675(1) nm3, R1 = 0.0520, and wR2 = 0.0860 (all data). The structure of Sc3B5O12 is composed of layers of condensed BO4 tetrahedra, separated by eight-fold coordinated scandium ions

High-pressure/high-temperature synthesis, crystal structure, and electrical properties of CaCu3 − x Fe x V4O12

2011 ◽  
Vol 47 (12) ◽  
pp. 1396-1401 ◽  
Author(s):  
N. I. Kadyrova ◽  
Yu. G. Zainulin ◽  
A. P. Tyutyunnik ◽  
N. V. Mel’nikova ◽  
I. S. Ustinova
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Electrical Properties ◽  
Temperature Synthesis ◽  
High Temperature Synthesis ◽  
High Pressure High Temperature
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